Influence of the pulse shape on the EDM performance of Si3N4-TiN ceramic composite

This paper describes the influence of the EDM discharge pulse shape on the machining performances and material removal mechanisms of Si₃N₄-TiN. Dramatic differences of material removal, ranging from classical melting to chemical decomposition, are observed by applying different pulse shapes such as the iso-energetic or relaxation type discharge pulses. It not just leads to the change of surface texture and machining performances, but also has influences on the ceramic properties. An EDM strategy is developed for the production of ceramic components in Si₃N₄-TiN and validated through the fabrication of a high temperature mesoscopic gas turbine.     

Examination of wire electrical discharge machining of Al2O3p/6061Al composites

Alumina particle reinforced 6061 aluminum matrix composites (Al₂O₃p/6061Al) have excellent physical and chemical properties than those of a traditional metal; however, their poor machinability lead to worse surface quality and serious cutting tool wear. In this study, wire electrical discharge machining (WEDM) is adopted in machining Al₂O₃p/6061Al composite. In the experiments, machining parameters of pulse-on time were changed to explore their effects on machining performance, including the cutting speed, the width of slit and surface roughness. Moreover, the wire electrode is easily broken during the machining Al₂O₃p/6061Al composite, so this work comprehensively investigates into the locations of the broken wire and the reason of wire breaking.The experimental results indicate that the cutting speed (material removal rate), the surface roughness and the width of the slit of cutting test material significantly depend on volume fraction of reinforcement (Al₂O₃ particles). Furthermore, bands on the machined surface for cutting 20 vol.% Al₂O₃p/6061Al composite are easily formed, basically due to some embedded reinforcing Al₂O₃ particles on the surface of 6061 aluminum matrix, interrupt the machining process. Test results reveal that in machining Al₂O₃p/6061Al composites a very low wire tension, a high flushing rate and a high wire speed are required to prevent wire breakage; an appropriate servo voltage, a short pulse-on time, and a short pulse-off time, which are normally associated with a high cutting speed, have little effect on the surface roughness.     

Surface modification of Al–Zn–Mg alloy by combined electrical discharge machining with ball burnish machining

The study investigated the feasibility of modifying the surface of Al–Zn–Mg alloy by a combined process of electric discharge machining (EDM) with ball burnish machining (BBM). A novel process that integrates EDM and BBM is also developed to conduct experiments on an electric discharge machine. Machining parameters of the combined process, including machining polarity, peak current, power supply voltage, and the protruding of ZrO₂, are chosen to determine their effects on material removal rate, surface roughness and the improvement ratio of surface roughness. In addition, the extent to which the combined process affects surface modification is also evaluated by microhardness and corrosion resistance tests. Experimental results indicate that the combined process of EDM with BBM can effectively improve the surface roughness to obtain a fine-finishing and flat surface. The micropores and cracks caused from EDM are eliminated during the process as well. Furthermore, such a process can reinforce and increase the corrosion resistance of the machined surface after machining.     

Scratching of Al2O3 under pre-stressing

Pre-stressing scratching tests have been preformed on polished surfaces of Al₂O₃ ceramic under a Rockwell diamond indenter which moved with uniform speed and constant normal load to investigate how the pre-stress contributes to the material removal mechanism. With the measurement of acoustic emission signals as well as indenter tangential forces, surface damages and cross-section of grooves of Al₂O₃ ceramic were evaluated under the action of different values of pre-stress. It was found that the scratched groove width was increased with the increasing of pre-stress when same normal loads were applied. The existence of pre-stress tends to restrain the crack propagation along the direction of pre-stress, and obvious plastic deformation at the bottom of scratched groove has been observed. Moreover, the fluctuation of tangential force was obviously enhanced, and the magnitude of tangential force in the test of pre-stress was higher than that of without pre-stress. The acoustic emission signals showed that fewer damages were produced in the process of scratching with an appropriate pre-stress. However, the continuing increase of pre-stress would aggravate the machining process.     

Surface integrity of finished turned Ti–6Al–4V alloy with PCD tools using conventional and high pressure coolant supplies

 Surfaces generated when machining Ti–6Al–4V alloy with PCD tools using conventional and high pressure coolant supplies was investigated. Longer tool life was recorded when machining Ti–6Al–4V with high-pressure coolant supplies and the recorded surface roughness R_a values were well below the tool rejection criterion (1.6 μm) for all cutting conditions investigated. The micro-structure of the machined surfaces were examined on a scanning electron microscope. Micrographs of the machined surfaces show that micro-pits and re-deposited work material were the main damages to the surfaces. Micro-hardness analysis showed hardening of the top machined surfaces when machining with conventional coolant while softening of the subsurface layer was observed when machining under high-pressure coolant supplies. The later is probably due to lower heat generated, with the consequent tempering action when machining with PCD tools with high-pressure coolant supplies. The microstructure below the machined surfaces had minimal or no plastic deformation when machining with conventional and high-pressure coolant supplies.     

EDM performance of Cr/Cu-based composite electrodes

Electrode materials for electrical discharge machining (EDM) are usually graphite, copper and copper alloys because these materials have high melting temperature, and excellent electrical and thermal conductivity. The electrodes made by using powder metallurgy technology from special powders have been used to modify EDM surfaces in recent years, to improve wear and corrosion resistance. However, electrodes are normally fabricated at high temperatures and pressures, such that fabrication is expensive. This paper proposes a new method of blending the copper powders contained resin with chromium powders to form tool electrodes. Such electrodes are made at low pressure (20 MPa) and temperature (200 °C) in a hot mounting machine. The results showed that using such electrodes facilitated the formation of a modified surface layer on the work piece after EDM, with remarkable corrosion resistant properties. The optimal mixing ratio, appropriate pressure, and proper machining parameters (such as polarity, peak current, and pulse duration) were used to investigate the effect of the material removal rate (MRR), electrode wear rate (EWR), surface roughness, and thickness of the recast layer on the usability of these electrodes. According to the experimental results, a mixing ratio of Cu–0wt%Cr and a sinter pressure of 20 MPa obtained an excellent MRR. Moreover, this work also reveals that the composite electrodes obtained a higher MRR than Cu metal electrodes; the recast layer was thinner and fewer cracks were present on the machined surface. Furthermore, the Cr elements in the composite electrode migrated to the work piece, resulting in good corrosion resistance of the machined surface after EDM.     

Study of electrical discharge grinding using metal matrix composite electrodes

An investigation was made into the combined technologies of electrical discharge machining and grinding (EDMG). A metal matrix (Cu/SiC_p) electrode with a rotating device was made and employed to study the EDMG technology. It was found that 3–7 times the normal electrical discharge machining (EDM) material removal rate (MRR) could be achieved in EDMG under suitable conditions of electrode rotating speed, SiC_p particle size and current. This novel achievement is attributed to the fact that, under appropriate conditions, the hump-shaped melted material created by the EDM mechanism is vulnerable to attack by the grinding mechanism during the EDMG operation, greatly increasing the removal rate. Conversely, under inappropriate conditions, in which hump-shaped material solidifies prior to the non-conductive ceramic particle grinding, the above function becomes negligible and results in much lower MRR.     

Probability of precision micro-machining of insulating Si3N4 ceramics by EDM

Electrical discharge machining (EDM) is used as a precision machining method for the electrically conductive hard materials with a soft electrode material. But recently we succeeded to machine on insulating material by EDM. The technology is named as an assisting electrode method. The EDMed surface is covered with the electrical conductive layer during discharge. The layer holds the electrical conductivity during discharge. For micro-EDM, the wear of tool electrode becomes lager ratio than the normal machining. So the micro-machining is extremely difficult to get the precision sample.

In this paper to obtain a fine and precise ceramics sample, some trials were carried out considering the EDM conditions, tool electrodes material and assisting electrode materials. Insulating Si₃N₄ ceramics were used for workpiece. The machining properties were estimated by the removal rate and tool wear ratio. To confirm the change of micro-machining process, the discharge waveforms were observed. The micro-machining of the Ø0.05 mm hole could be machined with the commercial sinking electrical discharge machine.     

Improvement of Dry EDM Characteristics Using Piezoelectric Actuator

This paper describes improvement of the machining characteristics of dry electrical discharge machining (dry EDM) by controlling the discharge gap distance using a piezoelectric actuator. Dry EDM is a new process characterized by small tool electrode wear, negligible damage generated on the machined surface, and significantly high material removal rate especially when oxygen gas is used. However, the narrow discharge gap length compared with conventional EDM using oil as the dielectric working fluid results in frequent occurrence of short circuiting which lowers material removal rate. A piezoelectric actuator with high frequency response was thus introduced to help control gap length of the EDM machine. To elucidate the effects of the piezoelectric actuator, an EDM performance simulator was newly developed to evaluate the machining stability and material removal rate of dry EDM.     

Structure and electrochemical performance of FeF3/V2O5 composite cathode material for lithium-ion battery

Orthorhombic structure FeF₃ was synthesized by a liquid-phase method using FeCl₃, NaOH and HF solution as starting materials, and the FeF₃/V₂O₅ composites were prepared by milling the mixture of as-prepared FeF₃ and the conductive V₂O₅ powder. The properties of FeF₃/V₂O₅ composites were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), galvanostatic charge/discharge and cyclic voltammetry measurements. Results showed that the FeF₃/V₂O₅ composites can be used as cathode material for lithium-ion battery. Electrochemical measurements in a voltage range of 2.0–4.5 V reveal that the addition of conductive V₂O₅ improves significantly the electrochemical performance of FeF₃, and the FeF₃/V₂O₅ composite prepared by milling for 3 h exhibits high discharge capacity and good cycle performance, and its discharge capacity maintains about 209 mAh g⁻¹ at 0.1 C (23.7 mA g⁻¹) after 30 cycles.     

Preparation and characteristic of spherical Li3V2(PO4)3

Spherical Li₃V₂(PO₄)₃ was synthesized by using N₂H₄ as reducer. The products were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results show that single-phase, spherical and well-dispersed Li₃V₂(PO₄)₃ has been successfully synthesized in our experimental process. Electrochemical behaviors have been characterized by charge/discharge measurements. The initial discharge capacities of Li₃V₂(PO₄)₃ were 123 mAh g⁻¹ in the voltage range of 3.0–4.3 V and 132 mAh g⁻¹ in the voltage range of 3.0–4.8 V.     

Material removal mechanisms of cemented carbides machined by ultrasonic vibration assisted EDM in gas medium

A new electrical discharge machining (EDM) technology named tool electrode ultrasonic vibration assisted electrical discharge machining in gas medium (UEDM in gas) is proposed and its principle is introduced. Relevant experimental equipment was designed by which a series of machining experiments of cemented carbide material were carried out. The mechanisms of cemented carbide material removal are discussed in detail through observing and analyzing the microstructures of machined surface. Five material removal mechanisms of cemented carbides machined by UEDM in gas were proposed, which are melting and evaporation, oxidation and decomposition, spalling, the force of high-pressure gas and the affection of ultrasonic vibration.     

Experimental investigation of surface/subsurface damage formation and material removal mechanisms in SiC grinding

The difficulty and cost involved in the abrasive machining of hard and brittle ceramics are among the major impediments to the widespread use of advanced ceramics in industries these days. It is often desired to increase the machining rate while maintaining the desired surface integrity. The success of this approach, however, relies in the understanding of mechanism of material removal on the microstructural scale and the relationship between the grinding characteristics and formation of surface/subsurface machining-induced damage. In this paper, grinding characteristics, surface integrity and material removal mechanisms of SiC ground with diamond wheel on surface grinding machine have been investigated. The surface and subsurface damages have been studied with scanning electron microscope (SEM). The effects of grinding conditions on surface/subsurface damage have been discussed. This research links the surface roughness, surface and subsurface damages to grinding parameters and provides valuable insights into the material removal mechanism and the dependence of grinding-induced damage on grinding conditions.     

Electrochemical hydrogen storage of NdMg12–Ni composites modified with carbon nanotubes and BN particles

In this work, the electrochemical performance of NdMg₁₂–Ni composite electrode in alkaline solution and the effect of the surface modification with carbon nanotubes (CNTs) and boron nitride (BN) particles on the NdMg₁₂–Ni composite were investigated. The NdMg₁₂ alloy was synthesized by a salt-cover-melting and a subsequent quenching process. The NdMg₁₂–Ni–BN and NdMg₁₂–Ni–CNTs composites were prepared by ball-milling NdMg₁₂ alloy, Ni powders and CNTs or BN particles. It is found that CNTs or BN particles are mainly attached onto the surface of the NdMg₁₂–Ni composite after the ball-milling process. The electrochemical experiment results indicate that the NdMg₁₂–Ni composites modified with CNTs or BN particles have the improved electrochemical performance. In particular, the NdMg₁₂–Ni–5 wt.% CNTs and NdMg₁₂–Ni–3 wt.% BN composites have the higher initial discharge capacity of 416.6 mAh/g and 442.9 mAh/g, respectively, larger than the original NdMg₁₂–Ni composite. The large amount of grain boundaries and crystalline defects, induced during the ball-milling process, can accelerate the bulk hydrogen diffusion and provide more surface active sites for the electrochemical reaction of the composites. However, the cycle stability of the composites modified by CNTs or BN particles is still not satisfactory for the practical application.     

Micro-EDM process investigation and comparison performance of Al3O2 and ZrO2 based ceramic composites

This paper investigates the micro-EDM behaviour of an Al₃O₂ and ZrO₂ based electrically conductive ceramic composites. The influence of the generator parameters on material removal rate, relative tool wear, surface quality and material removal mechanism is investigated towards the definition of suitable micro-EDM technologies. The study is based on a design of experiments, supported by a fundamental investigation of the generator parameters. Similar variations trends to the machining of steel are observed within the investigated process window, for exception of the tool wear performance. The developed EDM technologies are finally validated through the fabrication of industrial demonstrators.     

Experimental characterization of material removal in dry electrical discharge drilling

Dry electrical discharge machining is one of the novel EDM variants, which uses gas as dielectric fluid. Experimental characterization of material removal in dry electrical discharge drilling technique is presented in this paper. It is based on six-factor, three-level experiment using L₂₇ orthogonal array. All the experiments were performed in a ‘quasi-explosion’ mode by controlling pulse ‘off-time’ so as to maximize the material removal rate (MRR). Furthermore, an enclosure was provided around the electrodes with the aim to create a back pressure thereby restricting expansion of the plasma in the dry EDM process. The main response variables analyzed in this work were MRR, tool wear rate (TWR), oversize and compositional variation across the machined cross-sections. Statistical analysis of the results show that discharge current (I), gap voltage (V) and rotational speed (N) significantly influence MRR. TWR was found close to zero in most of the experiments. A predominant deposition of melted and eroded work material on the electrode surface instead of tool wear was evident. Compositional variation in the machined surface has been analyzed using EDAX; it showed migration of tool and shielding material into the work material. The study also analyzed erosion characteristics of a single-discharge in the dry EDM process vis-á-vis the conventional liquid dielectric EDM. It was observed that at low discharge energies, single-discharge in dry EDM could give larger MRR and crater radius as compared to that of the conventional liquid dielectric EDM.     

A new apparatus for finishing large size/large batch silicon nitride (Si3N4) balls for hybrid bearing applications by magnetic float polishing (MFP)

A new apparatus was designed and built for the finishing of large size/large batch silicon nitride (Si₃N₄) balls by magnetic float polishing (MFP) technology for hybrid bearing applications. The polishing chamber is so designed that during polishing it can self-align with the upper part of the polishing chamber connected to the spindle. In situ machining of the upper part of the chamber is performed on the machine tool in which the apparatus is located, in order to achieve high accuracy and geometric alignment of the system. The finishing methodology consists of mechanical polishing followed by chemo-mechanical polishing. Boron carbide (B₄C), silicon carbide (SiC), and cerium oxide (CeO₂) are the three abrasives used in this investigation. Three stages are involved in polishing, namely, 1. a roughing stage to remove maximum material without imparting any damage to the surface, 2. an intermediate stage of semi-finishing to control the size and improve sphericity, and 3. a final finishing stage to obtain best surface finish and sphericity while maintaining the final diameter. Taguchi method was applied for the roughing stage to optimize the polishing conditions for the best material removal rate. Level average response analysis has indicated that a load of 1.5 N/ball, an abrasive concentration of 20%, and a speed of 400 rpm would give a high material removal rate using B₄C (500 grit) abrasive. A groove is formed on the bevel of the upper part of the chamber which plays different roles, some beneficial and other not so beneficial, in each stage. In the roughing stage, it is preferable, though not essential, to machine the groove after each run to maintain high material removal rates. It is, however, necessary to remove the groove formed at the end of the roughing stage. In the intermediate or semifinishing stage, sphericity can be significantly improved by not machining the groove. Thus groove, in this case, facilitates in the improvement of sphericity. Before the beginning of the final finishing stage, machining the groove is necessary for rapid improvement in the surface finish. A batch of 46, 3/4 in. Si₃N₄ balls was finished to a final diameter of 0.7500 in. with an average sphericity of 0.25 μm (best value of 0.15 μm) and an average surface finish, Ra of 8 nm (best value of 6.7 nm) with an actual polishing time of <30 h. This technology is easy to implement in industry and does not entile high capital investment.     

Servo scanning 3D micro-EDM based on macro/micro-dual-feed spindle

Using the end discharge of micro-rod-shaped electrode to scan layer by layer, micro-electrical discharge machining (EDM) can fabricate complex 3D micro-structures. During the machining process, the discharge state is broken frequently due to the wear of the tool electrode and the relative scanning motion. To keep a favorable discharge gap, the feed spindle of the tool electrode needs the characteristics of high-frequency response and high resolution. In this study, an experimental system with a macro/micro-dual-feed spindle was designed to improve the machining performance of servo scanning 3D micro-EDM (3D SSMEDM), which integrates an ultrasonic linear motor as the macro-drive and a piezoelectric (PZT) actuator as micro-feeding mechanism. Based on LabVIEW and Visual C++ software platform, a real-time control system was developed to control coordinately the dual-feed spindle to drive the tool electrode. The micro-feed motor controls the tool electrode to keep the favorable discharge gap, and the macro-drive motor realizes long working range by a macro/micro-feed conversion. The emphasis is paid on the process control of the 3D SSMEDM based on macro/micro-dual-feed spindle for higher machining accuracy and efficiency. A number of experiments were carried out to study the machining performance. According to the numerical control (NC) code, several typical 3D micro-structures have been machined on the P-doped silicon chips. Our study results show that the machining process is stable and the regular discharge ratio is higher. Based on our fundamental machining experiments, some better-machined effects have been gained as follows. By machining a micro-rectangle cavity (960 μm×660 μm), the machined depth error can be controlled within 2%, the XY dimensional error is within 1%, the surface roughness R_a reaches 0.37 μm, and the material removal rate is about 1.58×10⁴ μm³/s by using a tool electrode of Φ=100 μm in diameter. By machining multi-micro-triangle cavities (side length 700 μm), it is known that the machining repeatability error is <0.7%.     

陶瓷基复合材料加工技术及其表面亚表面损伤机制研究进展

综述了陶瓷基复合材料的传统机械加工、超声辅助加工、激光加工、多能场复合加工等加工方式的研究进展,并简述了几种加工方式的优缺点.对陶瓷基复合材料的表面及亚表面损伤机制进行了总结和分析,包括材料表面亚表面损伤形式、材料表面亚表面理论及模型研究.提出了传统的陶瓷基复合材料加工技术需要进一步优化刀具材料、开发新的刀具结构、优化工艺参数等,以减少加工缺陷.研究了复合加工中材料去除率最大条件下的损伤容限条件、材料加工后的性能保持性等,同时探究了高效高质量的多能场复合加工新方法及其应用理论,以及研究探索了在复杂载荷及动载荷(如动态切削力、高温切削及超声动态冲击载荷)耦合作用下陶瓷基复合材料的内在损伤机理及演化问题.     

Trepanning of Al2O3 by electro-chemical discharge machining (ECDM) process using abrasive electrode with pulsed DC supply

Electro-chemical discharge machining (ECDM) of electrically non-conductive high-strength–high-temperature-resistant ceramics such as aluminium oxide (Al₂O₃) by trepanning method (i.e. orbital motion of tool) has shown the possibility of drilling large size holes by comparatively smaller electrodes efficiently and economically. However, at greater machined depth, the conventional electrode configurations and machining parameters show that machining performance gradually deteriorates with increase in tool depth and finally cause micro cracks on the machined surface due to thermal shocks at high voltage. To reduce this problem and to enhance the machining performance during trepanning operation of Al₂O₃, a spring fed cylindrical abrasive electrode of 1.5 mm diameter has been used under the effect of the three most influential parameters, namely, pulsed DC supply voltage, duty factor and electrolyte conductivity, each at five different levels to assess the volume of material removed, machined depth and diameteral overcut. The results obtained from this study revealed that pulsed DC has reduced the tendency of cracking at high supply voltage compared to smooth DC and the machining ability of the abrasive electrode was better than copper electrode as it would enhance the cutting ability due to the presence of abrasive grains during machining. In addition to this, trepanning provides the scope for drilling bigger holes.