一种含Ti奥氏体不锈钢的热变形行为

采用Gleeble3500热模拟机研究一种含Ti奥氏体不锈钢在温度850～1250℃、应变速率0.01～10s-1条件下的热变形行为。确定其热变形方程为ε=6.516×1015[sinh(α·σ)]4.33exp(-453000/RT),由计算得到的能量消耗效率η建立了热加工图,该奥氏体不锈钢的热变形激活能为453kJ/mol,不同真应变下的热加工图相似,随着变形温度的升高及应变速率的降低,能量消耗效率η逐渐升高。     

Ti—6Al—2Zr—1Mo—1V合金的热压变形特性及塑性流动方程

在 Gleeble- 15 0 0热模拟机上对 Ti- 6 Al- 2 Zr- 1Mo- 1V钛合金铸态材料进行了恒温和恒应变速率下的热压缩变形试验 .在试验温度 70 0～ 10 0 0℃、应变速率 5× 10 -3～ 5 0 s-1条件下 ,测试了材料的稳态变形抗力 ,并绘制成 lnσ- lnε和 lnσ- 1/ T关系曲线 ,从而确定合金的变形激活能 Q和应力指数 n.观察热变形后的组织表明 :合金在 80 0℃热变形为不完全动态再结晶组织 ,变形机制受动态回复与动态再结晶共同影响 ;90 0℃为完全动态再结晶组织 ,变形机制完全受动态再结晶影响 .合金在 90 0℃以上具有较好的工艺塑性 ,并且应力指数 n随变形温度的升高而减小 .     

Cu-0.58Sn合金热变形行为和热加工图研究

利用Gleeble-3180热模拟试验机,对Cu-0.58Sn合金在400～700 ℃,应变速率0.01～10 s?1条件下的热变形行为进行了研究。结果表明：该合金具有正的应变速率敏感性和热敏性,其流动应力随应变速率的增大而增大,随变形温度的升高而减小。建立了本构方程及热加工图,计算得出CuSn合金的热变形激活能为239.928 kJ/mol,同时优化出合金的最佳热加工参数为：变形温度500～700 ℃,应变速率3.16～10 s-1。     

铸态Ti–44Al–4Nb–(Mo, Cr, B)合金的热变形行为及热加工图

利用Gleeble热模拟机研究了铸态Ti-44Al-4Nb-(Mo,Cr,B)合金在1 050～1 200℃、0.005～0.5s-1下的热变形行为,并基于所得的真应力-真应变曲线绘制了热加工图。另外,通过透射电子显微镜(TEM)研究了片层和γ相的变形机制。结果表明,该合金是典型的应变速率和温度敏感材料,它的热加工性能较好,在1 100、1 150℃温度下的低应变速率区域以及1 200℃温度下高应变速率区域比较适合热加工。再结晶是流变软化的主要原因,较高的变形温度和较低应变速率有利于再结晶晶粒的进行。片层结构的变形机制为片层扭折,而γ相的主要变形机制为位错滑移和变形孪晶。     

5A30铝合金热变形的流变应力及材料常数

在Gleeble-1500热模拟试验机上,采用高温等温压缩试验,研究了5A30铝合金在300～500℃温度范围及应变速率在0.001～1s-1内压缩变形的流变应力变化规律,采用数学回归及最小偏差法求出了该合金的材料常数,建立了该合金流变应力与Zener-Hollomon参数的线性关系式.结果表明,该合金为正应变速率敏感材料,流变应力随变形温度升高而降低,随应变速率升高而增大;该合金的材料常数包括变形激活能Q为160.94kJ/mol,应力水平参数α为0.0184mm2/N,应力指数n为3.314,结构因子A为3.058×109s-1;合金流变应力模型可表达为σ=54.31ln{(Z/3.058×109)1/3.314+[(Z/3.058×109)2/3.314+1]1/2}.     

AZ31镁合金高温热压缩流变应力行为的研究

在Gleeble 1500D型热模拟试验机上,在应变速率为0.01～1s-1、变形温度为573～723K条件下,对AZ31合金的流变应力行为进行了研究.结果表明:AZ31镁合金在热压缩变形时,当应变速率一定时,流变应力随着变形温度的升高而减小;而当变形温度一定时,流变应力随着应变速率的增大而增大;该合金的热压缩流变应力行为可用双曲正弦形式的本构方程来描述,在本实验条件下AZ31镁合金热变形应力指数n=8.34,其热变形激活能Q=196kJ/mol.     

00Cr22Ni5Mo3N双相不锈钢的高温软化机理

采用热/力模拟实验方法对热轧态00Cr22Ni5Mo3N双相不锈钢(DSS)进行低应变高温平面变形试验.结果表明,在应变速率分别为0.1s-1和2s-1,变形温度900 ～ 1200℃条件下,双相不锈钢的峰值变形抗力随变形温度升高而降低,随应变速率的增大而增加,在各变形温度下,其差值达到30～80MPa.在1000 ～ 1200℃变形温度区间,铁素体组织发生完全的动态回复以及再结晶软化,部分奥氏体主要通过孪生变形及亚晶的形成进行软化.     

粉末冶金工艺参数对新型医用TiMoTaNbZr合金热变形行为的影响

以各合金元素粉末为原料,通过混料、冷等静压及真空烧结制备了新型医用Ti-14Mo-2. 1Ta-0. 9Nb-7Zr合金。通过改变压制压力、烧结保温时间等工艺参数制备合金,然后在变形量为60%、变形温度为900℃、变形速率为0. 01 s-1的条件下对合金进行高温热变形处理。利用X射线衍射(XRD)、光学显微镜(OM)及真应力-真应变曲线,表征分析了粉末冶金制备工艺参数对合金热变形行为的影响。结果表明,合金热变形后组织沿变形方向成纤维状,形成流线;粉末冶金法制备的合金强塑性好,且保温时间越长、制备压力越大,合金强塑性越好;合金在高温变形的条件下,发生动态回复和动态再结晶。动态回复阶段流变应力随着应变量的增加而增加,动态再结晶阶段则相反,再结晶完成后,合金进入稳态流变阶段。     

超轻镁锂合金LZ91热变形行为探究：本构方程及热加工图

本文以挤压态Mg-9Li-1Zn镁锂合金为材料在Gleeble3500热模拟实验机上做热压缩变形实验,变形温度范围为150℃-350℃,应变速率范围为0.001s-1-10s-1。基于所采集实验数据绘制流变应力应变曲线,建立了双曲线正弦函数的本构方程及真应变为0.916时热加工图,结合变形后微观组织观测分析了动态再结晶的产生情况,表明了适宜加工的安全区域和在加工中应该避免的失稳区域,预测温度范围为250-300℃,应变速率0.01s-1时为较理想的变形参数,峰值耗散系数值大于38.55%,热变形激活能Q=112.066kJ/mol,应力指数n=3.60273。     

Mg-8Gd-3Y-0.5Zr耐热镁合金的热压缩变形行为

对Mg-8Gd-3Y-0.5Zr(质量分数, %)稀土镁合金在温度为250～450 ℃、应变速率为0.001～0.1 s^-1、最大变形程度为50%的条件下, 进行了恒应变速率高温压缩模拟实验研究, 分析了实验合金高温变形时流变应力与应变速率及变形温度之间的关系以及组织变化, 计算了塑性变形表观激活能及相应的应力指数, 结果表明: 合金的稳态流变应力随应变速率的增大而增大, 在恒应变速率条件下, 合金的真应力水平随温度的升高而降低; 在给定的变形条件下, 计算得出的塑性变形表观激活能和应力指数分别为220 kJ/mol和5.6。根据实验分析, 合金的热加工宜在350 ℃左右进行。     

Current situation and future trend of China rare earth luminescent material industry

<正>Rare earth luminescent material is one of the most important application sectors of rare earths.China enjoys the exceptional advantage to develop rare earth luminescent material for its abundant rare earth resources.After several decades'endeavor,China's rare earth luminescent material industry,headed by rare earth phosphor for lamp and LED and high efficient rare earth energy-saving light source,has been gradually developed into a scale industry.China has become a major production base of rare earth phosphor for lamps and rare earth     

China rare earth market review

正June 1~10,2014Rare earth market remained weak.Quoted price of rare earth products was similar to that in May.There was no sign of recovery in downstream market.The market of NdFeB magnetic materials and phosphor was depressed.Catalyst,polishing powder and ceramic industries remained inactive.Demand from downstream industry was soft.Consumers purchased on their needs.Suppliers had strong intention to sell.Prices of rare earth products     

Annual Report analysis of Chinese rare earth-related listed companies in 2013

<正>Chinese rare earth-related listed companies have published their 2013 annual reports.It can be understood from their reports that production and operation activities of Chinese rare earth-related companies were still heavily affected by macro economy and industrial policies.They basically followed the steps of national economy.In 2013,world economy recovered slowly but the economy     

Market opportunities and challenges for rare earth polishing powder

正1.Status of rare earth polishing powder Rare earth polishing powder with high content of cerium oxide began to replace iron oxide for glass polishing and became one of the key materials in glass polishing process since 1940.Compared with traditional iron oxide,rare earth polishing powder has many advantages,such as fast polishing rate,high polishing quality and long service life.It can achieve good surface quality and improve operation conditions.For example,in lens polishing,the polishing work that cerium     

Baotou Research Institute of Rare Earths developed a new RE alloy preparation technology

正Pyrometallurgy Laboratory of Baotou Research Institute of Rare Earths had independently developed a new preparation technology of rare earth alloy for NdFeB.The alloy can remarkably enhance the coercivity of NdFeB magnet but also evidently reduce the production cost of the magnet.The new master alloy was prepared in the kA pilot-scale electrolytic cell by the independent technology.The rare earth master alloy can be used as the raw material for NdFeB.Compared     

矿用防爆轴流对旋主要通风机叶片ANSYS模态分析及应用

高效节能矿用防爆对旋主要通风机的叶片是主要通风机运行的关键部件,叶片在运行时不断受到气流的作用力,从而使叶片产生振动,当叶片振动的频率与叶片的固有频率接近时,容易产生共振从而导致叶片的断裂。一旦叶片断裂时,对主要通风机的安全运行产生致命的影响,从而导致矿山、化工等企业发生重大事故,将会产生不可估量的损失。基于有限元分析软件ANSYS,对高效节能矿用防爆轴流对旋主要通风机叶片进行模态分析及产生对应的六阶模态频率,对主要通风机叶片的运行频率、固有频率及产生的共振问题进行了原理分析,并且解决了叶片频率共振的问题,从而为主要通风机叶片结构设计提供理论依据,并对主要通风机叶片的安全运行提供保障。     

2013 NdFeB export analysis

<正>China totally exported nearly 24,000 tonsof NdFeB products during 201 3,including 18,825 tons of permanent magnet,valued USD 1.34 billion at an average price of 71.4 USD/kg;3,277 tons of NdFeB magnetic powder,valued USD 1 01 million at an average price of 30.9 USD/kg;1,334 tons of strip casting ribbon,with total export value of USD 74million at an average price of 55.3 USD/kg;and 586     

Market and recycling of NiMH battery

<正>Market status and future trend of NiMH battery1.Global market of small NiMH battery Global market size of small NiMH batteries declined year on year since 2011.The trend will continue to 2018,at the rate of 5%to 10%annually.Demand for small NiMH batteries will be stable gradually.Many electrical apparatuses are powered by the built-in lithium battery today,which is the main reason for the shrunk market of small NiMH batteries.But,for some products,small NiMH     

China rare earth market review

正September 1-10,2014 Affected by the National Day holiday,rare earth transaction was stagnant and the market showed a weak steady state.As there was no good news for downstream market,some products with flat demand would likely rally slightly for some time to     

唐口煤矿深部复杂开采工作面瓦斯分源涌出规律研究

研究工作面瓦斯涌出规律对工作面瓦斯治理有重要意义。为了得到唐口煤矿深部3号煤层复杂开采条件下工作面回采时期瓦斯涌出时空演化规律,选取6304工作面作为对象,采用实测方法研究6304工作面瓦斯涌出规律。结果表明:6304工作面瓦斯涌出量为6.534 m³/min,其中煤壁占34.27%,落煤占29.62%,采空区占36.11%;沿工作面倾向由低到高,瓦斯浓度整体为上升趋势,其中1—76号架工作面瓦斯浓度小于0.20%,76—102号架瓦斯浓度上升明显,最大为0.387%;上隅角的后部采空区是工作面的瓦斯主要涌出源,上隅角1号测点瓦斯浓度0.78%,上隅角周边3号、5号、7号、8号、9号测点瓦斯浓度平均为0.643%;周期来压时,上隅角瓦斯相对平时较高。研究为针对性的瓦斯分源监控与灾害防治提供基础。