Reliability issues for flip-chip packages

In this article, we review the reliability issues for plastic flip-chip packages, which have become an enabling technology for future packaging development. The evolution of area-array interconnects with high I/O counts and power dissipation has made thermal deformation an important reliability concern for flip-chip packages. Significant advances have been made in understanding the thermo-mechanical behavior of flip-chip packages based on recent studies using moiré interferometry. Results from moiré studies are reviewed by focusing on the role of the underfill to show how it reduces the shear strains of the solder balls but shifts the reliability concern to delamination of the underfill interfaces. The development of the high-resolution moiré interferometry based on the phase-shift technique provided a powerful method for quantitative analysis of thermal deformation and strain distribution for high-density flip-chip packages. This method has been applied to study plastic flip-chip packages and the results and impacts on delamination at the die/underfill interface and in the underfill region above the plated through-hole via are discussed. Here a related reliability problem of die cracking during packaging assembly and test is also discussed. Finally, we discuss briefly two emerging reliability issues for advanced flip-chip packages, one on the packaging effect on Cu/low k interconnect reliability and the other on electromigration of solder balls in flip-chip packages.     

Effects of Different Kinds of Underfills and Temperature–Humidity Treatments on Drop Reliability of Board-Level Packages

The hygrothermal and mechanical reliability of board-level packages with various underfills under sequential temperature and humidity (TH) testing and drop testing were investigated. Board-level packages with underfill had greater resistance to drop shock than that without underfill, indicating that underfill protects the package from failure by absorption of the applied drop shock. The underfill, which was composed of polypropylene glycol epoxy resin and silane, exhibited good reliability for drop shock because of the improved adhesion of the underfill compared with that without the polypropylene glycol epoxy resin and silane. In addition, the drop reliability of board-level packages with underfill decreased with increasing TH test duration. Adhesion between the substrate and underfill or between the solder and underfill was decreased by moisture absorption. Components positioned at the board center were more susceptible to failure by drop shock than were corner components.     

Measurement of underfill interfacial and bulk fracture toughness in flip-chip packages

Flip-chip package reliability is greatly improved by encapsulating the solder interconnections between a polymeric encapsulant or underfill. However, thermo-mechanical stresses within such packages often lead to failures initiating in the vicinity of chip and underfill interface. In this study, we present experimental results geared towards measuring and understanding such failure mechanisms. We provide the bulk fracture toughness of the underfill material and interfacial fracture toughness between the underfill material and the silicon die. The bulk and interfacial fracture toughness measurements are performed as a function of temperature. We use the single edge notch bending test to calculate the bulk fracture toughness of the underfill and to measure the interfacial fracture toughness, we use a novel technique referred to as the wedge delamination method. The wedge delamination method provides substantial advantage in measuring the interfacial fracture toughness for brittle materials over traditional methods. Using the wedge delamination method we compare the fracture strength between the underfill and silicon at the front-face and side-wall interfaces. Additionally, the influence of dicing technique on fracture toughness is also investigated.     

Mechanical fatigue test method for chip/underfill delamination in flip-chip packages

Underfill resin between Si chips and printed circuit boards is useful for improving the reliability of flip-chip packages. Generally, thermal cycle tests (TCTs) are applied to electronic packages under development in order to prove their reliability. At the early stage of development, however, a more effective test method is desirable, because TCTs are time-consuming. A new mechanical fatigue test for the underfill resin in flip-chip packages, namely the four points support test method, is proposed in this paper. The validity of the mechanical test method could be verified from the results of stress analyses and experiments. Considering the chip/underfill delamination statistically based on the assumption of Markov process, it was shown that the delamination probability during cyclic loads could be estimated with equations of the displacement range and number of cycles.     

Wafer-applied underfill: flip-chip assembly and reliability

Manufacturers of consumer electronic products are continuously striving to confer greater functionality to smaller, lighter, and less expensive packages, and flip-chip is an important enabling technology for these product trends. Underfill between the die and an organic substrate is necessary to compensate for the coefficient of thermal expansion mismatch. The underfill dispense and cure step is not a typical process for a surface-mount technology (SMT) factory, and demands additional capital equipment, floor space, cycle time, and headcount. An alternate approach to traditional capillary underfill is wafer-applied underfill. The underfill is applied after wafer bumping and sawing, but prior to the picking of the individual die from the saw tape. This paper describes the coating and assembly processes. Liquid-to-liquid thermal cycle shock tests (-55 to +125/spl deg/C) have been performed on test vehicles assembled with the wafer-applied underfill. First failures were at over 1000 cycles. Weibull plots of the data and failure analysis are presented.     

Design and Fabrication of a Flip-Chip-on-Chip 3-D Packaging Structure With a Through-Silicon Via for Underfill Dispensing

This paper presents a new package design for multichip modules. The developed package has a flip-chip-on-chip structure. Four chips [simulating dynamic random access memory (DRAM) chips for demonstration purpose] are assembled on a silicon chip carrier with eutectic solder joints. The I/Os of the four chips are fanned-in on the silicon chip carrier to form an area array with larger solder balls. A through-silicon via (TSV) hole is made at the center of the silicon chip carrier for optional underfill dispensing. The whole multichip module is mounted on the printed circuit board by the standard surface mount reflow process. After the board level assembly and X-ray inspection, the underfill process is applied to some selected specimens for comparative study purpose. The underfill material is dispensed through the center TSV hole on the silicon chip carrier to encapsulate the solder joints and the four smaller chips. Subsequently, scanning acoustic microscopy (SAM) is performed to inspect the quality of underfill. After the board-level assembly, all specimens are subject to the accelerated temperature cycling (ATC) test. During the ATC test, the electrical resistance of all specimens is monitored. The experimental results show that the packages without underfill encapsulation may fail in less than 100 thermal cycles while those with underfill can last for more than 1200 cycles. From the dye ink analysis and the cross-section inspection, it is identified that the packages without underfill have failure in the silicon chip carrier, instead of solder joints. The features and merits of the present package design are discussed in details in this paper.     

Thermomechanical reliability of underfilled BGA packages

The effect of underfill on various thermomechanical reliability issues in super ball grid array (SBGA) packages is studied in this paper. Nonlinear finite element models with underfill and no underfill are developed taking into consideration the process-induced residual stresses. In this study, the solder is modeled as time and temperature-dependent, while other materials are modeled temperature and direction-dependent, as appropriate. The stress/strain variations in the package due to thermal cycling are analyzed. The effect of underfill is studied with respect to magnitude and location of time-independent plastic strain, time-dependent creep strain and total inelastic strain in solder balls. The effect of copper core on the solder ball strains is presented. The possibility of delamination at the interposer-underfill interface as well as substrate-underfill interface is studied with the help of qualitative interfacial stress analysis. Results on SBGA packages indicate that the underfill does not always enhance BGA reliability, and that the properties of the underfill have a significant role in the overall reliability of the BGA packages. The predicted number of thermal cycles to solder joint fatigue are compared with the existing experimental data on similar nonunderfilled BGA packages.     

Development of environmentally friendly nonanhydride no-flowunderfills

Most no-flow underfill materials are based on epoxy/anhydride chemistry. Due to the sensitizing nature, the use of anhydride is limited and there is a need for a no-flow underfill using nonanhydride curing system. This paper presents the development of novel no-flow underfill materials-based on epoxy/phenolic resin system. Epoxy and phenolic resins of different structures are evaluated in terms of their curing behavior, thermo-mechanical properties, viscosity, adhesion toward passivation, moisture absorption and the reliability in flip-chip underfill package. The influence of chemical structure and the crosslinking density of the resin on the material properties is investigated. The assembly with nonanhydride underfill shows high reliability from the thermal shock test. Solder wetting test has confirmed the sufficient fluxing capability of phenolic resins. Results show that epoxy/phenolic system has great potential for an environmentally friendly and highly reliable no-flow underfill     

Fatigue testing method for fine bond wires in an LQFP package

A mechanical testing setup was developed to study the fatigue response of fine thermo-sonic wire bond connection in low profile quad flat packages (LQFP). The testing set-up was designed to induce pre-defined multi-axial stresses in the wire bond loops of non-encapsulated packages in order to mimic their deformation behavior during the thermo-mechanical loading. Lifetime curves were obtained up to 1.0E7 loading cycles with fatigue failure occurring in the heat affected zone of the ball bond. The experimental fatigue data in combination with extended FEA provided the basis for a Coffin Manson lifetime model. The proposed fatigue testing procedure can be applied as a highly efficient method for evaluation of various wire bonded packages by using a limited number of test samples and simultaneous testing of several wire bonds.     

Investigation on flip chip solder joint fatigue with cure-dependent underfill properties

A cure-dependent viscoelastic constitutive relation is applied to describe the curing process of epoxy underfill in flip chip on board (FCOB). The chemical shrinkage of the epoxy underfill during the curing process is applied via incremental initial strains. Thus, the stress and strain build-up, caused by the simultaneous increase in stiffness and shrinkage during the curing process, are simulated. Accelerated fatigue experiments with thermal cycles from -55/spl deg/C to 80/spl deg/C are carried out for a specially designed flip chip configuration. Based on the obtained curing induced initial stress and strain fields, thermo-mechanical predictions are presented for the test carriers. The solder bumps are modeled with temperature dependent visco-plastic properties. A combination of a Coffin-Manson based fatigue relation and a creep fatigue model is used as fatigue failure criterion. The results show that the finite element method (FEM)-based fatigue life predictions match better with the experimental results, if the curing induced initial stress state is taken into account. The effect of cure-induced hydrostatic stress is qualitatively investigated by using a modified energy partitioning damage model with a correction factor in the creep damage formulation to take into account the effect of the hydrostatic stress.     

Measurement of the temperature dependent constitutive behavior of underfill encapsulants

Reliable, consistent, and comprehensive material property data are needed for microelectronic encapsulants for the purpose of mechanical design, reliability assessment, and process optimization of electronic packages. In our research efforts, the mechanical responses of several different capillary flow snap cure underfill encapsulants are being characterized. A microscale tension-torsion testing machine has been used to evaluate the uniaxial tensile stress-strain behavior of underfill materials as a function of temperature and strain rate. A critical step to achieving accurate experimental results has been the development of a sample preparation procedure that produces mechanical test specimens that reflect the properties of true underfill encapsulant layers. In the developed method, 75-125/spl mu/m (3-5 mil) thick underfill uniaxial tension specimens are dispensed and cured using production equipment and the same processing conditions as those used with actual flip chip assemblies. A three parameter hyperbolic tangent empirical model has been shown to provide accurate fits to the observed underfill nonlinear stress-strain behavior over a range of temperatures and strain rates. In addition, the first measurements of underfill mechanical behavior at cryogenic temperatures have been made.     

Lead-free chip scale packages: assembly and drop test reliability

Three underfill options compatible with lead-free assembly have been evaluated: capillary underfill, fluxing underfill, and corner bond underfill. Chip scale packages (CSPs) with eutectic Sn/Pb solder were used for control samples. Without underfill, lead-free and Sn/Pb eutectic drop test results were comparable. Capillary flow underfills, dispensed and cured after reflow, are commonly used in CSP assembly with eutectic Sn/Pb solder. With capillary flow underfill, the drop test results were significantly better with lead-free solder assembly than with Sn/Pb eutectic. Fluxing underfill is dispensed at the CSP site prior to CSP placement. No solder paste is printed at the site. The CSP is placed and reflowed in a standard reflow cycle. A new fluxing underfill developed for compatibility with the higher lead-free solder reflow profiles was investigated. The fluxing underfill with lead-free solder yielded the best drop test results. Corner bond underfill is dispensed as four dots corresponding to the four corners of the CSP after solder paste print, but before CSP placement. The corner bond material cures during the reflow cycle. It is a simpler process compared to capillary or fluxing underfill. The drop test results with corner bond were intermediate between no underfill and capillary underfill and similar for both lead-free and Sn/Pb eutectic solder assembly. The effect of aging on the drop test results with lead-free solder and either no underfill or corner bond underfill was studied. Tin/lead solder with no underfill was used for control. This test was to simulate drop performance after the product has been placed in service for some period of time. There was degradation in the drop test results in all cases after 100 and 250 h of storage at 125/spl deg/C prior to the drop test. The worst degradation occurred with the lead-free solder with no underfill.     

Novel reworkable fluxing underfill for board-level assembly

Underfills are traditionally applied for flip-chip applications. Recently, there has been increasing use of underfill for board-level assembly including ball grid arrays (BGAs) and chip scale packages (CSPs) to enhance reliability in harsh environments and impact resistance to mechanical shocks. The no-flow underfill process eliminates the need for capillary flow and combines fluxing and underfilling into one process step, which simplifies the assembly of underfilled BGAs and CSPs for SMT applications. However, the lack of reworkability decreases the final yield of assembled systems. In this paper, no-flow underfill formulations are developed to provide fluxing capability, reworkability, high impact resistance, and good reliability for the board-level components. The designed underfill materials are characterized with the differential scanning calorimeter (DSC), the thermal mechanical analyzer (TMA), and the dynamic mechanical analyzer (DMA). The potential reworkability of the underfills is evaluated using the die shear test at elevated temperatures. The 3-point bending test and the DMA frequency sweep indicate that the developed materials have high fracture toughness and good damping properties. CSP components are assembled on the board using developed underfill. High interconnect yield is achieved. Reworkability of the underfills is demonstrated. The reliability of the components is evaluated in air-to-air thermal shock (AATS). The developed formulations have potentially high reliability for board-level components.     

The effects of underfill and its material models onthermomechanical behaviors of a flip chip package

In this paper, the effects of underfill on thermomechanical behavior of two types of flip chip packages with different bumping size and stand-off height were investigated under thermal cycling both experimentally and two-dimensional (2-D) finite element simulation. The materials inelasticity, i.e., viscoelasticity of underfill U8437-3 and viscoplasticity of 60 Sn40 Pb solder, were considered in the simulations. The results show that the use of underfill encapsulant increases tremendously (~20 times) the thermal fatigue lifetime of SnPb solder joint, weakens the effects of stand-off height on the reliability, and changes the deformation mode of the package. It was found that the thermal fatigue crack occurs in the region with maximum plastic strain range, and the Coffin-Manson type equation could then be used for both packages with and without underfill. Solder joint crack initiation occurred before delamination when using underfill with good adhesion (75 MPa) and the underfill delamination may not be a dominant failure mode in the present study. The interfacial stresses at the underfill/chip interface were calculated to analyze delamination sites, which agree with the results from acoustic image. Moreover, the effects of material models of underfill, i.e., constant elasticity (EC) and temperature dependent elasticity (ET) as well as the viscoelasticity (VE), on the thermomechanical behaviors of flip chip package were also studied in the simulation. The VE model gives comparatively large plastic strain range and large displacements in the shear direction, as well as decreased solders joint lifetime. The ET model gives similar results as the VE model and could be used instead of VE in simulations for the purpose of simplicity     

Evaluating the material properties of underfill for a reliable 3D TSV integration package using numerical analysis

The effects of the material properties of the underfill layer on thermal stress and deformation in 3D through silicon via (TSV) integration packages were evaluated through numerical analysis. Sample TSV packages with underfill composed of different silica volume ratios were fabricated. The sample packages were used to measure thermal deformation using a Moiré interferometer. Also, a cross-section from these samples was used for 2D finite element modeling and numerical analysis to obtain its thermal deformation. The experimental and numerical results were compared to confirm the suitability of the numerical technique in this research. A four-chip-stacked TSV integration package, which includes underfill layers of four different silica volume ratios, was proposed and designed. The diagonal part of the TSV integration packages were three dimensionally modeled and adopted for numerical analysis. Among the underfill with different silica volume ratios in the designed packages, a silica volume ratio of around 20% shows the best performance for a reliable flip chip bonding process, effectively minimizing thermal stress and deformation in the package.     

An examination of the applicability of the DNP metric on first level reliability assessments in underfilled electronic packages

The notion of using the distance from neutral point (DNP)¹ as a metric to assess the criticality of first level package thermomechanical stresses is examined in this paper. This metric has been applied by assuming that testing of electronic package assemblies with largest applicable DNP is required to infer the quality of similar packages with smaller die dimensions. Through a review of complex thermomechanical analyses available in the literature together with finite element studies performed herein for representative package geometries, this simple yet commonly applied approach is shown to be an overly conservative methodology for packages with first level underfill. For the representative cases considered, the local edge stresses and strains presumed to cause first level failure are shown to increase with DNP to a point where they no longer increase. A new methodology is presented based on this information for estimating test vehicle configurations needed to confidently qualify similar packages with larger die sizes.     

Finite volume based CFD simulation of pressurized flip-chip underfill encapsulation process

This paper presents the simulation of pressurized underfill encapsulation process for high I/O flip chip package. 3D model of flip chip packages is built using GAMBIT and simulated using FLUENT software. Injection methods such as central point, one line, L-type and U-type are studied. Cross-viscosity model and volume of fluid (VOF) technique are applied for melt front tracking of the encapsulant. The melt front profiles and pressure field for all injection types are analyzed and presented. The pressure distribution within the flip-chip, fill volume versus filling time and viscosity versus shear rate are also plotted. The U-type injection is found to be faster in filling. The numerical results are compared with the previous experimental results and found in good conformity. The strength of CFD software in handling underfill encapsulation problems is proved to be excellent.     

Procedure for design optimization of a T-cap flip chip package

In this study, a 1/4 three-dimensional finite element model of a T-cap flip chip package containing the substrate, underfill, solder bump, silicon die, metal cap and cap attachment was established to conduct thermo-mechanical reliability study during the flip chip fabrication processes. The applied thermal load was cooled from 183 °C to ambience 25 °C to determine the thermal stress and warpage during the curing period of solder ball mounting process. Under fixed geometry, two levels of underfill, metal caps and cap attachments were used to conduct the 2³ factorial design for determining reliable material combinations. The statistical tests revealed that the significant effects affecting the thermal stress were the underfill, metal cap, cap attachment and the interaction between the underfill and cap attachment. The metal cap, cap attachment and their interaction significantly affected the warpage. The proposed regression models were used to perform the surface response simulations and were useful in selecting suitable materials for constructing the package. This study provides a powerful strategy to help the designer to easily determine reliable packaging structures under various reliability considerations.     

The effects of rheological and wetting properties on underfill filler settling and flow voids in flip chip packages

As the bump diameter and bump pitch of flip chip packages get smaller, the underfill becomes more resistant to flow. Therefore, low viscosity underfills are used in the process to increase the throughput. Problems associated with low viscosity underfills include filler settling and flow induced voids due to fast edge flow. In this paper, we will discuss how the rheological properties can affect underfill filler settling and flow voids. The effects of yield stress of underfill on filler settling and the effects of shear thickening of underfill at large shear rates on flow voids of underfill were investigated. It was shown that the underfills with small fillers have shear-thickening viscosity and yield stress. The filler settling of underfills with yield stress was greatly reduced. A video underfill flow metrology with quartz die packages was developed for flow void observation. The correlation between underfill, substrate properties, and flow voids formation based on the video underfill flow measurement will be discussed.     

Effects of Phase Change of Pb-Free Flip-Chip Solders During Board-Level Interconnect Reflow

The impact of phase change (from solid to liquid) on the reliability of Pb-free flip-chip solders during board-level interconnect reflow is investigated. Most of the current candidates for Pb-free solder are tin-based with similar melting temperatures near 230 degC. Thus, Pb-free flip-chip solders melt again during the subsequent board-level interconnect reflow cycle. Solder volume expands more than 4% during the phase change from solid to liquid. The volumetric expansion of solder in a volume constrained by chip, substrate, and underfill creates serious reliability issues. The issues include underfill fracture and delamination from chip or substrate. Besides decreasing flip-chip interconnect reliability in fatigue, bridging through underfill cracks or delamination between neighboring flip-chip interconnects by the interjected solder leads to failures. In this paper, the volume expansion ratio of tin is experimentally measured, and a Pb-free flip-chip chip-scale package (FC-CSP) is used to observe delamination and solder bridging after solder reflow. It is demonstrated that the presence of molten solder and the interfacial failure of underfill can occur during solder reflow. Accordingly, Pb-free flip-chip packages have an additional reliability issue that has not been a concern for Pb solder packages. To quantify the effect of phase change, a flip-chip chip-scale plastic ball grid array package is modeled for nonlinear finite-element analysis. A unit-cell model is used to quantify the elongation strain of underfill and stresses at the interfaces between underfill and chip or underfill and substrate generated by volume expansion of solder. In addition, the strain energy release rate of interfacial crack between chip and underfill is also calculated