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排序方式: 共有931条查询结果,搜索用时 93 毫秒
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2.
Sintering and grain growth of nano-crystalline undoped ZnO has been studied in detail over a wide range of temperature and holding time. Below 800 °C, sintering of over 70% theoretical density is not observed, irrespective of particle size. At 900 °C for 6 h, the nano-crystalline sample sinters to 99% of theoretical density whereas the density for as received sample is 93% of theoretical density. However, at 1300 °C or higher, the densification is found to be much faster and after a few hours becomes independent of holding time. Grain growth studies reveal a similar feature of attaining saturation over holding time. The average saturated grain size is found to be ∼1.5 and ∼2.2 μm at 800 and 900 °C, respectively, while at 1300 °C or higher, it is in between 12 and 13 μm. 相似文献
3.
Anirban Chakraborty James C. Earthman 《Metallurgical and Materials Transactions A》1997,28(4):979-989
Finite element simulations of the high-temperature behavior of single-phase γ, dual-phase α2+γ, and fully lamellar (FL) α2+γTiAl intermetallic alloy microstructures have been performed. Nonlinear viscous primary creep deformation is modeled in
each phase based on published creep data. Models were also developed that incorporate grain boundary and lath boundary sliding
in addition to the dislocation creep flow within each phase. Overall strain rates are compared to gain an understanding of
the relative influence each of these localized deformation mechanisms has on the creep strength of the microstructures considered.
Facet stress enhancement factors were also determined for the transverse grain facets in each model to examine the relative
susceptibility to creep damage. The results indicate that a mechanism for unrestricted sliding of γ lath boundaries theorized
by Hazzledine and co-workers leads to unrealistically high strain rates. However, the results also suggest that the greater
creep strength observed experimentally for the lamellar microstructure is primarily due to inhibited former grain boundary
sliding (GBS) in this microstructure compared to relatively unimpeded GBS in the equiaxed microstructures. The serrated nature
of the former grain boundaries generally observed for lamellar TiAl alloys is consistent with this finding. 相似文献
4.
Animesh Chakrabarti Man Mohan Sharma 《Journal of the American Oil Chemists' Society》1992,69(12):1251-1253
Anhydrous esterification of myristic acid with propylene was carried out in the temperature range of 110–145°C and pressure
from 190–195 psig in the presence of Amberlyst-15 (cation exchange resin) and Filtrol-24 (acid-treated clay) as catalysts.
The product ester, isopropyl myristate finds use in cosmetic and topical medicinal preparations where good absorption through
the skin is desired. Filtrol-24 is the catalyst of choice, and the recommended operating temperature is 130°C with a pressure
of 190 psig. 相似文献
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Sample preparation for DNA and RNA assays is a prime candidate for laboratory automation. A novel, parallel processing device that performs the three separate liquid-handling functions necessary for such sample preparation-dispensing, pipetting, and pressurizing-is presented. The device comprises an array of fine nozzles connected by fluidic channels to automatically and precisely distribute flow between one source and an array of points. The design principles, as well as the experimental and computational methods used to develop the device, are described. Test results, including accuracy, uniformity, volume range, and timing, are presented. The functionality of the device is demonstrated by performing a solid-phase extraction of DNA with two types of microcolumns. 相似文献
8.
Semi1 and semi2 interpenetrating polymer networks (IPNs) of PVC and in situ formed PMMA have been synthesized using diallyl phthalate and ethylene glycol dimethacrylate as the crosslinkers of PVC and PMMA, respectively. These two types of IPNs have been compared w.r.t their physical, mechanical, and thermal properties and an endeavor has been made to find a correlation of these properties with the morphology generated in these systems. The semi1 IPNs displayed a decrease in their mechanical parameters and the physical properties as well, while in contrast, the semi2 IPNs exhibited a marginal increase in the corresponding values after an initial drop upto about 15% of crosslinked PMMA incorporation when compared to the crosslinked PVC in the case of semi1 IPN and linear PVC in the case of semi2 IPN. The various samples of semi1 and semi2 IPNs showed a two‐stage degradation typical of PVC, while confirming the increased stability with the samples having higher percentages of PMMA. The influence of crosslinking of the major matrix in semi1 IPN was almost counterbalanced by the influence of crosslinking in the dispersed PMMA phase in the case of semi2 IPN. The softening characteristics as detected by the extent of penetration of the probe, as has been detected by thermomechanical analysis, are in conformity with their mechanicals. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 97: 1725–1735, 2005 相似文献
9.
An Experimental Study to Evaluate the Effect of Ambient Temperature during Manual Lifting and Design of Optimal Task Parameters 下载免费PDF全文
Ravindra Pratap Singh Ajay Batish T. P. Singh Anirban Bhattacharya 《人机工程学与制造业中的人性因素》2014,24(1):54-70
In the present study, the effect of lifting task parameters on the heart rate and oxygen uptake of workers during manual lifting tasks in different ambient conditions was evaluated. The experiments conducted in two different temperature conditions showed a significantly higher oxygen uptake and heart rate in colder conditions as compared to warmer conditions. Three other factors, namely, load, lifting frequency, and vertical distance were found to significant affect the responses. Various combinations of significant factors were used to calculate oxygen uptake and heart rate. These were then compared with the safe limits as per the maximum aerobic capacity of workers. Based on these comparisons, the safe combinations were identified that can be used to design lifting tasks in varied ambient conditions. The study further concluded that lifting tasks performed in winter should have different relaxation or fatigue allowances built into the cycle time of the task to compensate for higher exertion. © 2011 Wiley Periodicals, Inc. 相似文献
10.
Anirban Sengupta Chandan Mazumdar Aditya Bagchi 《Journal of Network and Systems Management》2011,19(3):319-342
From information security point of view, an enterprise is considered as a collection of assets and their interrelationships.
These interrelationships may be built into the enterprise information infrastructure, as in the case of connection of hardware
elements in network architecture, or in the installation of software or in the information assets. As a result, access to
one element may enable access to another if they are connected. An enterprise may specify conditions on the access of certain
assets in certain mode (read, write etc.) as policies. The interconnection of assets, along with specified policies, may lead
to managerial vulnerabilities in the enterprise information system. These vulnerabilities, if exploited by threats, may cause
disruption to the normal functioning of information systems. This paper presents a formal methodology for detection of managerial
vulnerabilities of, and threats to, enterprise information systems in linear time. 相似文献