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1.
Hidemitsu Hojo Wataru Toyoshima Masayasu Tamura Noriyuki Kawamura 《Polymer Engineering and Science》1974,14(9):604-609
Particulate-filled thermosetting composites are widely used, yet little systematic work has been done on their long-term strength characteristics. In this study short-term tensile, flexural, and impact tests as well as tensile creep-rupture tests were made for unfilled and filled epoxy to clarify the effects of filler size, filler content, and temperature. Fillers used were silica, alumina particles, and glass beads. Test temperatures were varied from 25 to 110°C. As a result of short-term testing, it was found that the Petch relation held between strength and filler size if brittle fracture occurred, while a strength and filler size if brittle fracture occurred, while a strengthening effect existed when ductile fracture occurred. On creeprupture testing, a strengthening is observed with filler size and content for silica and glass beads. The Arrhenius plot of rupture time for various filler sizes and contents converges to a characteristic point corresponding to the glass transition temperature of the material. Using this relation, a modified Larson-Miller master rupture curve is proposed which can predict the long-term strength of particulate-filled thermosetting composites as functions of rupture time, temperature, filler size, and content. 相似文献
2.
3.
Image blurring of MeV transmission electrons for gold nanoparticles on the top surface of micrometer-thick specimens has been investigated using the Monte Carlo simulation. Both the simulated line density profile and therefore image blurring were in good agreement with the experimental ones in the ultrahigh voltage electron microscope. Quantitative effects of specimen thickness and electron energy on image blurring were presented, in which the specimen thickness had a greater influence. Image blurring was demonstrated to be caused mainly by multiple elastic scattering, but it could be reduced to several nanometers for a 5?μm thick epoxy-resin specimen at the electron energy of 2?MeV. 相似文献
4.
Md Sazzadur Rahman MD Nahin Islam Shiblee Kumkum Ahmed Ajit Khosla Jun Ogawa Masaru Kawakami Hidemitsu Furukawa 《大分子材料与工程》2020,305(9)
In this work, 3D printable gel polymer electrolytes (GPEs) based on N,N‐dimethylacrylamide (DMAAm) and polyvinylidene fluoride (PVDF) in lithium chloride containing ethylene glycol solution are synthesized and their physicochemical properties are investigated. 3D printing is carried out with a customized stereolithography type 3D gel printer named “Soft and Wet Intelligent Matter‐Easy Realizer” and free forming GPE samples having variable shapes and sizes are obtained. Printed PVDF/PDMAAm‐based GPEs exhibit tunable mechanical properties and favorable thermal stability. Electrochemical proprieties of the printed GPEs are carried out via impedance spectroscopy in the temperature range of 25–90 °C by varying PVDF content. Ionic conductivity as high as 6.5 × 10?4 S cm?1 is achieved at room temperature for GPE containing low PVDF content (5 wt%) and conductivity of the GPEs is increased as temperature rises. 相似文献
5.
Size-dependent separation of graphene oxide by deformation of packed-gel in a chromatographic column
Yuji Takaoka Shohei Esaki Koichi Sakaguchi Tomotsumi Fujisawa Masashi Unno Shintaro Morisada 《分离科学与技术》2020,55(7):1356-1363
ABSTRACTA deformable gel-packed chromatographic column was used to separate as-synthesized graphite oxide with different sizes. The synthesized gel (56 µm) was deformed by pressure of the fluid flow and the gaps in the gels showed a range of sizes. A suspension of graphene oxide (0.1 g/L, 10 mL) was injected, and graphene oxide in the elution had a size at 0.56 μm and 0.14 μm, whereas in half upper and bottom domain of the gel layer graphene oxide had a size at 33 µm and 2.9 µm, respectively, demonstrating that graphene oxide suspension was separated by size through gel layer. 相似文献
6.
Fuminori Adachi Takashi Washio Atsushi Fujimoto Hiroshi Motoda Hidemitsu Hanafusa 《New Generation Computing》2005,23(4):291-313
The needs of efficient and flexible information retrieval on multi-structural data stored in database and network are significantly
growing. Especially, its flexibility plays one of the key roles to acquire relevant information desired by users in retrieval
process. However, most of the existing approaches are dedicated to a single content and data structure respectively, e.g.,
relational database and natural text. In this work, we propose “Multi-Structure Information Retrieval” (MSIR) approach applicable
to various types of contents and data structures by adapting a small part of the approach to data structures. The power of
this approach comes from the use of the invariant feature information obtained from byte patterns in the files through some
mathematical transformation. The experimental evaluation of the proposed approach for both artificial and real data indicates
its high feasibility.
Fuminori Adachi: He received his Master of engineering from Osaka University in ’03. He is enrolled in the doctoral course of Osaka University
from ’03. His current research interest includes scientific discovery, data mining and machine learning techniques.
Takashi Washio, Ph.D.: He received his Ph.D. from Tohoku University in ’88. In ’88, he became a visiting reseacher in Massachusetts Institute of
Technology. In ’90, he joined Mitsubishi Research Institute Inc., and is working for Osaka University from ’96. His current
research interest includes scientific discovery, data mining and machine learning techniques.
Atsushi Fujimoto: He is enrolled in the master cource of Osaka University from ’03. His Current research interest includes correlation analysis,
data mining and machine learning techniques.
Hiroshi Motoda, Ph.D.: He received his Ph.D. from University of Tokyo in ’72. In ’67, he joined Hitachi Ltd. and has been working for Osaka University
since ’96. His current research interest includes scientific discovery, data mining and machine learning.
Hidemitsu Hanafusa: He received Master of Engineering from Keio University in ’83. In ’83, he joined The Kansai Electric Power Co. Ins. (KEPCO).
He researched on Maintenance Support System at INSS from ’97 to ’02. Now, he is working in KEPCO. 相似文献
7.
K Takada Y Matsumura S Dohmen N Mitsutomi M Takaoka S Morimoto 《Canadian Metallurgical Quarterly》1996,59(9):PL111-PL116
The profile of endothelin-1 (ET-1) release from cultured vascular endothelial cells (ECs) obtained from deoxycorticosterone acetate (DOCA)-salt hypertensive rats, was examined and compared with that from normotensive sham rats. ET-1 release from ECs was increased in a time-dependent manner, and the level of DOCA-salt hypertensive rats was higher than that of sham rats. Incubation of ECs with transforming growth factor (TGF)-beta 1 or thrombin resulted in a significant increase in the ET-1 release, while FK409, a novel nitric oxide donor, produced a dose-dependent decrease in the release. In the case of ECs from DOCA-salt hypertensive rats, the potencies of TGF-beta 1- or thrombin-induced action was much less than that seen with sham rats, while the difference of reactivity to FK409 was not observed between ECs of DOCA-salt rats and sham rats. Thus, ET-1 production in ECs appears to be up-regulated in DOCA-salt hypertensive rats. In addition, there seems to be an abnormalities in the signaling pathway via TGF-beta 1- or thrombin-induced enhancement of ET-1 production in ECs of DOCA-salt hypertensive rats. 相似文献
8.
Influence of the image quality deterioration of a tilted thick specimen on electron tomography 总被引:1,自引:0,他引:1
In electron tomography (ET) based on a transmission electron microscope, the effective thickness of a specimen increases with the tilt angle and, therefore, the projection quality may deteriorate because of electron scattering. The information-missing region, however, can be reduced by broadening the specimen tilt range. To clarify the general influence of these effects on ET, the projection quality varying with the tilt angle was quantitatively evaluated for a 5-microm thick specimen observed with a 3 MV ultrahigh-voltage electron microscope. Simulations of three-dimensional reconstruction were then performed for different specimen thicknesses and tilt ranges. As a result, the ET accuracy was shown to decrease as the specimen thickness increased. However, an optimum specimen-tilt range, at which ET could reach its highest accuracy, was found to exist and become small with the increase of the specimen thickness. The presented results are helpful for determining the specimen thickness limitation on the ET resolution and improving the ET fidelity of thick specimens. 相似文献
9.
Shortest path problems can be solved very efficiently when a directed graph is nearly acyclic. Earlier results defined a graph decomposition, now called the 1-dominator set, which consists of a unique collection of acyclic structures with each single acyclic structure dominated by a single associated trigger vertex. In this framework, a specialised shortest path algorithm only spends delete-min operations on trigger vertices, thereby making the computation of shortest paths through non-trigger vertices easier. A previously presented algorithm computed the 1-dominator set in O(mn) worst-case time, which allowed it to be integrated as part of an O(mn+nrlogr) time all-pairs algorithm. Here m and n respectively denote the number of edges and vertices in the graph, while r denotes the number of trigger vertices. A new algorithm presented in this paper computes the 1-dominator set in just O(m) time. This can be integrated as part of the O(m+rlogr) time spent solving single-source, improving on the value of r obtained by the earlier tree-decomposition single-source algorithm. In addition, a new bidirectional form of 1-dominator set is presented, which further improves the value of r by defining acyclic structures in both directions over edges in the graph. The bidirectional 1-dominator set can similarly be computed in O(m) time and included as part of the O(m+rlogr) time spent computing single-source. This paper also presents a new all-pairs algorithm under the more general framework where r is defined as the size of any predetermined feedback vertex set of the graph, improving the previous all-pairs time complexity from O(mn+nr2) to O(mn+r3). 相似文献
10.
Influence of the methyl group on the dielectric constant of boron carbon nitride films containing it
Hidemitsu Aoki Takuro Masuzumi Makoto Hara Zhiming Lu Daisuke Watanebe Chiharu Kimura Takashi Sugino 《Diamond and Related Materials》2010,19(12):1437-1440
LSI interconnect insulators made using low dielectric constant (low-k) materials are required for high performance devices with a small RC delay. We investigated a boron carbon nitride film containing the methyl group (Me–BCN) using tris-di-methyl-amino-boron (TMAB: B[N(CH3)2]3) gas as a low-k material. In addition, we studied the influence of the methyl group on the dielectric constant (k-value) and the properties of the Me–BCN films. It was found that the k-value of the Me–BCN films decreases with increasing number of C–H bonds due to the methyl group (CH3). The number of O–H bonds due to water incorporation is suppressed by increasing the number of C–H bonds. Consequently, we suggested that a lower k-value can be realized by the suppression of water invasion by a hydrophobic surface due to methyl bonds. Thus, the control of the methyl group is important to achieve a low-k material using Me–BCN films. 相似文献