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A nuclear microprobe with high spatial resolution and high analytical sensitivity was applied to analyze trace elements,especially lead,in vehicle exhaust of Shanghai city.The result shows that the chemical composition and its corresponding x-ray relative intensity are different among different vehicle exhausts.There are many kinds of metal elements in particles of vehicle exhaust.most are harmful to people,such as Ti,Cr,Mn,Pb,etc.We found that the lead concentration was 6820μg/g and the bromine concentration was 5300μg/g in the exhaust from Santana using leaded gasoline(SULG).which is higher than any other kinds of vehicle exhausts.We have also detected the minimum lead in the particles of unleaded gasoline and its content varies from one to another.Its mean concentration was 450μg/g and the highest reached 6210μg/g.The unleaded gasoline‘s Pb existed in the whole particle while the leaded gasoline‘s enriched in the surface of the particle and was more harmful to the human beings. 相似文献
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The bonding of β'-Al2O3 and pyrex glass to Al matrix composites by anodic bonding process is achieved. The microstructure of the bonded interface and the joining mechanisms are analyzed with scanning electron microscope (SEM), energy dispersive X-ray fluorescence spectrometer (EDX). It is observed that the bonding region across the interface consists of the metal layer, oxide transitional layer and the ceramic layer, with the transitional layer composed of surface region and sub-surface region. The bonding process can mainly be categorized into anodic bonding process and solid state diffusing process. The pile-up of the ions and its drift in the interface area are the main reasons for anode oxidation and joining of the interface. The temperature, voltage and the drift ions in the ceramic or glass during the bonding process are the essential conditions to solid state diffusing and oxide bonding at the interface. The voltages, temperature, pressure as well as the surface state are the main factors that influence the anodic bonding. 相似文献
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用己二酸二酰肼(ADH)对透明质酸(HA)进行化学修饰,制备交联透明质酸(HA-ADH)薄膜。粘度法测试表明HA-ADH是一种可降解的生物材料,并且与HA相比,HA.ADH的降解速率减慢。在此基础上,研究了以疏水性的替硝唑(TDZ)和亲水性的头孢唑啉钠(CEZ)为模拟药物的HA-ADH药物载体薄膜的释药性能。紫外-可见(UV-Vis)吸收光谱检测表明,HA-ADH是一种疏水性药物TDZ的优良缓释制荆,这是由于TDZ的疏水性和HA-ADH薄膜的缓慢溶胀和降解性能的结合而得到的,药物的释放主要受扩散机制控制。 相似文献
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Transglutaminase (TGase) was separated from the culture broth of an isolated strain of Streptoverticillium mobaraense. The crude enzyme was prepared by centrifugation, ultrafiltration, precipitation by alcohol, centrifugation and freeze‐drying. The yield after these processes was 65–70%. Then the enzyme was purified to homogeneity by chromatography on CM‐cellulose and Sephadex G‐75 on which the yields were about 70% and 80%, respectively; the purified folds reached 2.5–4.7 and 1.08–2.06, respectively. The molecular weight of this TGase was 39,500–40,100 Da by gel filtration chromatography. Optimum enzyme activity was observed in the pH range of 5.0–7.0, and it was maintained stable at 20–40C. The optimal temperature and pH was 52C and 6.0, respectively. At 1 mM and 5 mM metal ion or inhibitors concentration, TGase activity was strongly inhibited by Zn2+ and NEM, and not affected obviously by Ba2+, Ca2+, Co2+, Cu2+, Fe2+, Fe3+, Mg2+, Mn2+, Na+ as well as PMSF and EDTA. The effects of these additions on this TGase were compared with those of other microbial TGases. 相似文献
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分析了当前对于从固定背景下的特征符号与背景符号相粘连的图表中提取信息所存在的问题,设计了适用于此类问题的方法模型。提出了一种在固定背景下通过背景符号检测和背景符号擦除来实现随机波形提取的方法。 相似文献
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单轴-平面W型复合锶铁氧体的制备及其吸波特性研究 总被引:3,自引:0,他引:3
用草酸盐共沉淀和微量掺杂法研制六角晶系W型Ni,Zn,Co,Al多元复合锶铁氧体,通过调节Ni2W同Co2W的摩尔比例,可使该种铁氧体易磁化方向从C单轴型向垂于C轴的平面型转化,控制置换锶铁氧体中部分Fe3 的微量掺杂Al3 ,可以调整4πMs值,提高磁晶各向异性场,测试分析了5种不同含Co量的W型复合锶铁氧体粉料涂层的吸波特性,发现其自然共振吸收峰随Co含量增加向低频方向偏移,最高吸收峰可达32.8dB,是适用于电子隐形技术的高品位的微波吸收剂。 相似文献
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