Hydrolysis of Fe(OH)SO4 in the presence of metallic iron

Hydrolysis of Fe(OH)SO₄ was carried out in the presence of metallic iron in order to prevent the formation of iron(III) oxides with strongly bonded sulphate. Under the conditions of the experiment, the products were found to be mixtures of ?-Fe₂O₃ and α-FeOOH. The occluded sulphate, if any, could be easily washed out with water. The hydrolysis reaction passes through an equilibrium state before coming to completion. The entropy with enthalpy of the hydrolysis corresponding to the equilibrium state were found to be 4 e.u. and 0·5 kJ/mol, respectively. The activation energy of the hydrolysis reaction was found to be 21 kJ/mol.     

Oxidation Behavior of Rh–30Ni–18Nb Refractory Superalloy

The isothermal-oxidation behavior of Rh–30Ni–18Nb refractory alloy was investigated up to a period of 312 hours in air from 1000 to 1350°C. A comparison of the oxidation behavior of this alloy with a conventional Ni-base superalloy (Inconel 713 C) shows an order-of-magnitude higher oxidation resistance. This experimental alloy oxidizes by forming alternate layers of Nb₂O₅ and RhO while NiO is on the surface in contact with air. Optical and scanning-electron microscopy (SEM) was used to study the microstructure and morphology for the characterization of the oxides. Thermal stability of the alloy for extended periods of exposure to air at 1400°C was studied using transmission-electron microscopy (TEM).     

Performance analysis of tool electrode prepared through laser sintering process during electrical discharge machining of titanium

The International Journal of Advanced Manufacturing Technology - It is of great significance for intelligent manufacturing to study condition monitoring and diagnosis methods to realize early...     

A comprehensive modeling framework for gate stack process dependence of DC and AC NBTI in SiON and HKMG p-MOSFETs

A comprehensive modeling framework involving mutually uncorrelated contribution from interface trap generation and hole trapping in pre-existing, process related gate insulator traps is used to study NBTI degradation in SiON and HKMG p-MOSFETs. The model can predict time evolution of degradation during DC and AC stress, time evolution of recovery after stress, impact of stress and recovery bias and temperature, and impact of several AC stress parameters such as pulse frequency, duty cycle, duration of last pulse cycle (half or full) and pulse low bias. The model can successfully explain experimental data measured using fast and ultra-fast methods in SiON and HKMG devices having different gate insulator processes. The trap generation and trapping sub components of the composite model have been verified by independent experiments. Data published by different groups are reconciled and explained. The model can successfully predict long time DC and AC stress data and has been used to determine device degradation at end of life as EOT is scaled for different HKMG devices.     

Explanation of P/E cycling impact on drain disturb in flash EEPROMs under CHE and CHISEL programming operation

The impact of program/erase (P/E) cycling on drain disturb in NOR Flash EEPROM cells under channel hot electron (CHE) and channel-initiated secondary electron (CHISEL) programming operation is studied. Charge gain disturb increases and charge loss disturb decreases after cycling under CHE and CHISEL operation. Carefully designed experiments and fullband Monte Carlo simulations were used to explain this behavior. P/E cycling induced degradation in gate coupling coefficient and the resulting increase in source/drain leakage, reduction in band-to-band tunneling and change in carrier injection area seems to explain well the behavior of CHE and CHISEL drain disturb after cycling.     

Adaptive enhancement of compressed SAR images

Synthetic aperture radar (SAR) imagery is an important global all-weather surveillance and mapping satellite imagery system. As space-borne systems have a limited storage capacity, it is imperative to heavily compress SAR images, possible with lossy compression schemes. As a result, SAR images need to be enhanced in earth stations. The work reported in this paper aims to address the issue of compression artefact removal of SAR images in an adaptive manner. The SAR images, compressed using the JPEG utility at significantly low bit rates, are enhanced by adaptively removing coding artefacts and speckle noise. As edges carry significant information in satellite imagery, a significant edge image is used for edge enhancement with selective removal of noisy edges. Further, an image sharpness metric is proposed in this work to serve as an objective no-reference metric for measuring the sharpness of SAR images.     

CL-AGKA: certificateless authenticated group key agreement protocol for mobile networks

Wireless Networks - Wireless group communication has gained much popularity recently due to the increase in portable, lightweight devices. These devices are capable of performing group...     

A policy based framework for quality of service management in software defined networks

Growth in multimedia traffic over the Internet increases congestion in the network architecture. Software-Defined Networking (SDN) is a novel paradigm that solves the congestion problem and allows the network to be dynamic, intelligent, and it centrally controls the network devices. SDN has many advantages in comparison to traditional networks, such as separation of forwarding and control plane from devices, global centralized control, management of network traffic. We design a policy-based framework to enhance the Quality of Service (QoS) of multimedia traffic flows in a potential SDN environment. We phrase a max-flow-min-cost routing problem to determine the routing paths and presented a heuristic method to route the traffic flows in the network in polynomial time. The framework monitors the QoS parameters of traffic flows and identifies policy violations due to link congestion in the network. The introduced approach dynamically implements policy rules to SDN switches upon detection of policy violations and reroutes the traffic flows. The results illustrate that the framework achieves a reduction in end-to-end delay, average jitter, and QoS violated flows by 24%, 37%, and 25%, respectively, as compared to the Delay Minimization method. Furthermore, the proposed approach has achieved better results when compared to SDN without policy-based framework and reduced end-to-end delay, average jitter, and QoS violated flows by 51%, 62%, and 28%, respectively.

     

Load Balancing Technique for Congestion Control Multipath Routing Protocol in MANETs

A mobile ad hoc network (MANET) is a collection of wireless mobile nodes that can communicate without a central controller or fixed infrastructure. Due to node mobility, designing a routing protocol to provide an efficient and suitable method to route the data with less energy consumption, packet drop and to prolong the network lifetime has become a challenging issue in MANETs. In MANETs, reducing energy consumption and packet loss involves congestion control and load balancing techniques. Thus, this paper introduces an efficient routing technique called the multipath load balancing technique for congestion control (MLBCC) in MANETs to efficiently balance the load among multiple paths by reducing the congestion. MLBCC introduces a congestion control mechanism and a load balancing mechanism during the data transmission process. The congestion control mechanism detects the congestion by using an arrival rate and an outgoing rate at a particular time interval T. The load balancing mechanism selects a gateway node by using the link cost and the path cost to efficiently distribute the load by selecting the most desirable paths. For an efficient flow of distribution, a node availability degree standard deviation parameter is introduced. Simulation results of MLBCC show the performance improvements in terms of the control overhead, packet delivery ratio, average delay and packet drop ratio in comparison with Fibonacci sequence multipath load balancing, stable backbone-based multipath routing protocol and ad hoc on demand multipath distance vector routing. In addition, the results show that MLBCC efficiently balances the load of the nodes in the network.

     

High performance 14-bit pipelined redundant signed digit ADC

A novel architecture of a pipelined redundant-signed-digit analog to digital converter(RSD-ADC) is presented featuring a high signal to noise ratio(SNR), spurious free dynamic range(SFDR) and signal to noise plus distortion(SNDR) with efficient background correction logic. The proposed ADC architecture shows high accuracy with a high speed circuit and efficient utilization of the hardware. This paper demonstrates the functionality of the digital correction logic of 14-bit pipelined ADC at each 1.5 bit/stage. This prototype of ADC architecture accounts for capacitor mismatch, comparator offset and finite Op-Amp gain error in the MDAC(residue amplification circuit) stages. With the proposed architecture of ADC, SNDR obtained is 85.89 dB, SNR is 85.9 dB and SFDR obtained is 102.8 dB at the sample rate of 100 MHz. This novel architecture of digital correction logic is transparent to the overall system, which is demonstrated by using 14-bit pipelined ADC. After a latency of 14 clocks, digital output will be available at every clock pulse. To describe the circuit behavior of the ADC, VHDL and MATLAB programs are used. The proposed architecture is also capable of reducing the digital hardware. Silicon area is also the complexity of the design.