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排序方式: 共有179条查询结果,搜索用时 343 毫秒
1.
A new and efficient method for preparation of optically active poly(styrene–divinylbenzene) copolymers (PS-DVB) is presented here. This is carried out by Friedel–Crafts acylation reaction of chiral N-phthaloyl
-leucine acid chloride with PS-DVB beads in the presence of aluminum chloride as Lewis acid catalyst and 1,2-dichloroethane as the solvent at ambient temperature. Reagents’ amounts and reaction conditions are mentioned and four samples with different amounts of functionality have been prepared. Final products were characterized by FT-IR and elemental analysis. The results obtained confirm that the above modification in preparation of chiral supported PS-DVB has been achieved well and in moderate yield. 相似文献
2.
Alireza Pourshahid Daniel Amyot Liam Peyton Sepideh Ghanavati Pengfei Chen Michael Weiss Alan J. Forster 《Electronic Commerce Research》2009,9(4):269-316
A number of recent initiatives in both academia and industry have sought to achieve improvements in e-businesses through the
utilization of Business Process Management (BPM) methodologies and tools. However there are still some inadequacies that need
to be addressed when it comes to achieving alignment between business goals and business processes. The User Requirements
Notation (URN), recently standardized by ITU-T, has some unique features and capabilities beyond what is available in other
notations that can help address alignment issues. In this paper, a URN-based framework and its supporting toolset are introduced
which provide business process monitoring and performance management capabilities integrated across the BPM lifecycle. The
framework extends the URN notation with Key Performance Indicators (KPIs) and other concepts to measure and align processes
and goals. An example process for controlling access to a healthcare data warehouse is used to illustrate and evaluate the
framework. Early results indicate the feasibility of the approach. 相似文献
3.
Sepideh Hamedi Seyed Abbas Shojaosadati Soheila Shokrollahzadeh Sameereh HashemiNajafabadi 《IET nanobiotechnology / IET》2017,11(2):157
Elucidation of the molecular mechanism of silver nanoparticle (AgNP) synthesis is necessary to control nanoparticle size, shape, and monodispersity. In this study, the mechanism of AgNP formation by Neurospora intermedia was investigated. The higher production rate of AgNP formation using a culture supernatant heat‐treated at 100° and 121°C relative to that with an un‐treated culture supernatant indicated that the native form of the molecular species is not essential. The effect of the protein molecular weight (MW) on the nanoparticle size distribution and average size was studied by means of ultraviolet–visible spectroscopy and dynamic light scattering. Using un‐treated and concentrated cell‐free filtrate passed through 10 and 20 kDa cut‐off filters led to the production of AgNPs with average sizes of 25, 30, and 34 nm, respectively. Also, using the permeate fraction of cell‐free filtrate passed through a 100 kDa cut‐off filter led to the formation of the smallest nanoparticles with the narrowest size distribution (average size of 16 nm and polydispersity index of 0.18). Sodium dodecyl sulphate polyacrylamide gel electrophoresis analysis of the fungal extracellular proteins showed two notable bands with the MWs of 15 and 23 kDa that are involved in the reduction and stabilisation of the nanoparticles, respectively.Inspec keywords: silver, nanoparticles, nanofabrication, proteins, molecular weight, ultraviolet spectra, visible spectra, cellular biophysics, electrophoresis, molecular biophysicsOther keywords: Neurospora intermedia, molecular mechanism, silver nanoparticle synthesis, nanoparticle shape, nanoparticle monodispersity, AgNP formation, untreated culture supernatant, molecular species, protein molecular weight, MW, nanoparticle size distribution, ultraviolet‐visible spectroscopy, dynamic light scattering, untreated cell‐free filtrate, concentrated cell‐free filtrate, cut‐off filters, permeate fraction, polydispersity index, Sodium dodecyl sulphate polyacrylamide gel electrophoresis analysis, fungal extracellular proteins, nanoparticle reduction, nanoparticle stabilisation, temperature 100 degC, temperature 121 degC, size 25 nm, size 30 nm, size 34 nm, size 16 nm, Ag 相似文献
4.
5.
Soudeh Ghafouri-Fard Tayyebeh Khoshbakht Bashdar Mahmud Hussen Sepideh Kadkhoda Mohammad Taheri Arash Tafrishinejad 《International journal of molecular sciences》2022,23(1)
miR-149 is an miRNA with essential roles in carcinogenesis. This miRNA is encoded by the MIR149 gene on 2q37.3. The miR-149 hairpin produces miR-149-5p and miR-149-3p, which are the “guide” and the sister “passenger” strands, respectively. Deep sequencing experiments have shown higher prevalence of miR-149-5p compared with miR-149-3p. Notably, both oncogenic and tumor suppressive roles have been reported for miR-149-5p. In this review, we summarize the impact of miR-149-5p in the tumorigenesis and elaborate mechanisms of its involvement in this process in a variety of neoplastic conditions based on three lines of evidence, i.e., in vitro, in vivo and clinical settings. 相似文献
6.
Application of the Electrodiffusion Method to Measure Wall Shear Stress: Integrating Theory and Practice 下载免费PDF全文
Lutz Böhm Sepideh Jankhah Jaroslav Tihon Pierre R. Bérubé Matthias Kraume 《化学工程与技术》2014,37(6):938-950
The electrodiffusion method has been used in fluid dynamic research for the past 50 years. It allows the measurement of wall shear stress, a crucial parameter, e.g., for the cleaning of membrane modules used in water filtration. Various authors have published articles dealing with the theory behind this technique. But no paper collects all the knowledge assembled over five decades of application. Here, comprehensive summary of the theory of steady flow, unsteady flow, and transient voltage step experiments is given. Factors influencing the accuracy of the measurements are discussed. Furthermore, a new approach to calibrate the system from voltage step experiments is introduced, and practical issues related to its application in flow measurements are discussed for an exemplary signal response to a near‐wall flow. 相似文献
7.
M Lauwereys M Arbabi Ghahroudi A Desmyter J Kinne W H?lzer E De Genst L Wyns S Muyldermans 《Canadian Metallurgical Quarterly》1998,17(13):3512-3520
Evidence is provided that dromedary heavy-chain antibodies, in vivo-matured in the absence of light chains, are a unique source of inhibitory antibodies. After immunization of a dromedary with bovine erythrocyte carbonic anhydrase and porcine pancreatic alpha-amylase, it was demonstrated that a considerable amount of heavy-chain antibodies, acting as true competitive inhibitors, circulate in the bloodstream. In contrast, the conventional antibodies apparently do not interact with the enzyme's active site. Next we illustrated that peripheral blood lymphocytes are suitable for one-step cloning of the variable domain fragments in a phage-display vector. By bio-panning, several antigen-specific single-domain fragments are readily isolated for both enzymes. In addition we show that among those isolated fragments active site binders are well represented. When produced as recombinant protein in Escherichia coli, these active site binders appear to be potent enzyme inhibitors when tested in chromogenic assays. The low complexity of the antigen-binding site of these single-domain antibodies composed of only three loops could be valuable for designing smaller synthetic inhibitors. 相似文献
8.
Freydoon Arbabi 《Computers & Structures》1982,15(2):103-108
The ease of erection of bolted frames has caused an increase in their application in recent years. The safe design of such frames requires the inclusion of joint flexibility in the analysis. The behavior of such connections is generally nonlinear. Since in optimization and nonlinear analysis the solution is carried out as a collection of elastic problems, efficient techniques are required for the analysis of the frame.In this paper a method is developed for such purposes. The method gives exact results for symmetric multi-story single-bay frames. For multi-bay frames the results are approximate and the degree of accuracy varies with the problem. A procedure for obtaining the exact solution of multi-bay frames is discussed. 相似文献
9.
Attenuation and phase coefficients are evaluated for microwave radio propagation through oblate spheroidal raindrops on slant radio paths. From these coefficients, it is evident that the resultant crosspolarisation for linearly or circularly polarised waves should be significantly less on satellite radio paths than on horizontal radio paths. 相似文献
10.
Sepideh Adabi Ali Movaghar Amir Masoud Rahmani Hamid Beigy 《The Journal of supercomputing》2013,66(3):1350-1389
Providing an efficient resource allocation mechanism is a challenge to computational grid due to large-scale resource sharing and the fact that Grid Resource Owners (GROs) and Grid Resource Consumers (GRCs) may have different goals, policies, and preferences. In a real world market, various economic models exist for setting the price of grid resources, based on supply-and-demand and their value to the consumers. In this paper, we discuss the use of multiagent-based negotiation model for interaction between GROs and GRCs. For realizing this approach, we designed the Market- and Behavior-driven Negotiation Agents (MBDNAs). Negotiation strategies that adopt MBDNAs take into account the following factors: Competition, Opportunity, Deadline and Negotiator’s Trading Partner’s Previous Concession Behavior. In our experiments, we compare MBDNAs with MDAs (Market-Driven Agent), NDF (Negotiation Decision Function) and Kasbah in terms of the following metrics: total tasks complementation and budget spent. The results show that by taking the proposed negotiation model into account, MBDNAs outperform MDAs, NDF and Kasbah. 相似文献