Synthesis of amphiphilic magnetic microspheres by dispersion copolymerization of styrene and poly(ethylene oxide) macromonomer

Amphiphilic magnetic microspheres ranging in diameter from 5 to 100 µm were prepared by dispersion copolymerization of styrene and poly(ethylene oxide) vinylbenzyl (PEO‐VB) macromonomer (MPEO) in the presence of Fe₃O₄ magnetic fluid. The effects of various polymerization parameters on the average particle size were systematically investigated. The average particle size was found to increase with increasing styrene concentration and initiator concentration. It also increased with decreasing stabilizer concentration and molecular weight of MPEO. The content of the hydroxyl groups localized in the microspheres ranged from 0.01 to 0.2 mmol g^?1. © 2003 Society of Chemical Industry     

单光子时间分辨在线谱仪系统中的接口电路

本文介绍单光子时间分辨在线谱仪系统中的多道分析器与IBM PC/XT微型计算机接口的工作原理及控制程序。     

石油系油浆与煤系闪蒸油的焦化性能——I．热解条件的影响

通过偏光显微镜观察了石油系油浆（LH）与煤系闪蒸油（SN）焦化后所得焦块的光学结构。结果表明，在较宽条件下两种原料单独焦化均得不到取向度高的流线型结构。将两种原料以一定比例混合后先热解丙焦化所得焦块的光学结构明显好于二者混合后直接焦化所得焦块的光学结构，其中LH和SN以3：2的重量比混合后在440℃、1MPa下热解3．5h然后再在530℃、1MPa下焦化8h所得焦块为具有较高取向度的流线型结构，适合于作为针状焦的起始原料。     

Ultrasonic thin-walled tube wave structure for sensing devices

Theoretical and experimental investigations of thin-walled tube acoustic wave devices for gravimetric sensing applications are presented. Integrated sensor configurations have been demonstrated by employing a sol-gel processed thin piezoelectric lead zirconate titanate (PZT) film. This was coated coaxially on stainless steel tubes and interdigital transducers (IDT) fabricated as the transmitter and receiver on the curved tube surfaces. We have observed tube waves along both the axial and circumferential directions between 1 and 6.6 MHz. We have also analyzed the mass sensitivities of different modes propagating along the tubes and shown that high mass sensitivity can be achieved by keeping the tube wall thin     

Cast bulk ZrTiAlCuNi amorphous alloys

Cylindrical bulk amorphous samples with diameters up to 10 mm have been prepared by casting ZrTiAlCuNi alloys in a copper mould. In order to rank glass-forming ability as a function of alloy composition, alloys were also cast into wedge-shaped moulds; to a first approximation, the thickness of the amorphous region obtained can be taken as an indication of glass-forming ability. The compositions which lead to the production of bulk glasses all have reduced glass transition temperatures in excess of 0.65 and the extremely high glass-forming ability of these compositions is discussed. We suggest that both the Al and Ti contents are determining factors for the production of bulk amorphous samples and these are believed to reduce the driving force for, and hence the rate of, crystallisation. These amorphous alloys have been found to display high thermal stability and can be annealed for several minutes in the supercooled liquid region. They are ductile at room temperature and have a high value of yield stress.     

PARAMAGNETIC MEISSNER EFFECTS IN MELT-TEXTURED Y_(0.99)Nd_(0.01)Ba_2Cu_3O_(7-y)SUPERCONDUCTOR

The paramagnetic Meissner effect (PME) was observed on the field-cooled M-T curvesof melt-textured Y0.99Nd0.01Ba2Cu3O7-y in applied magnetic fields from 1kOe toJ0kOe. In the magnetic field below 1kOe, the sample undergoes the typical transi-tion from the normal state to the superconducting state when it was cooled down. Theapplied magnetic fields in which the PME occurs, are very high compared with thefields reported in literatures. We propose that the occurrence of the PME may be dueto a phase transition of flux vortices in the superconductors.     

扎实推进规划工作 培植绿色发展理念——湖北省中小河流水能资源开发规划工作情况介绍

本文介绍了湖北省中小河流水能资源开发规划工作进展,规划工作在树立绿色发展理念、摸清水能资源开发状况等方面取得的成效,以及湖北省为推动规划工作采取的主要做法。     

马来酸酐接枝聚丙烯增容聚丙烯/碳酸钙复合物力学性能与增容机理

用在50L固相接枝反应器中合成的马来酸酐接枝聚丙烯(PP-g-MAH)作界面改性剂，制备了马来酸酐接枝聚丙烯／聚丙烯／碳酸钙(i-PP／PP-g-MAH／CaCO3)复合材料。研究了i-PP／PP-g-MAH／CaCO3复合材料的力学性能和增容机理。结果表明，PP-g-MAH对i-PP／CaCO3复合物的缺口冲击强度、弯曲强度和拉伸强度均有提高；PP-g-MAH与CaCO3反应形成PP-g-MAH的钙盐，实现反应性增容。     

Seasonal evolution of the interannual variability of chlorophyll-a concentration and its forcing factors in the northwestern Pacific from 1998 to 2010

The northwestern Pacific Ocean is a complex region with significant biological spatial variations on a seasonal timescale. To investigate the joint variation patterns on both seasonal and interannual timescales, a season-reliant empirical orthogonal function (S-EOF) analysis was applied to seasonal mean chlorophyll-a concentration (chl-a) anomalies in the northwestern Pacific Ocean during the period 1998–2010. The first two dominant modes accounted for nearly 31% of the total interannual variance, with the second S-EOF mode (S-EOF2) lagging behind the first S-EOF mode (S-EOF1) by one year. S-EOF1 featured a strong variation pattern to the north of 30° N, with maximum chl-a in winter and minimum chl-a in summer. However, S-EOF2 indicated an opposite seasonally evolving pattern compared with S-EOF1, with chl-a increasing along the Kuroshio and extension current from boreal winter to autumn. Both these modes revealed significant relationships with climate-related indices. The two modes corresponded to the central Pacific (CP) La Niña developing episodes and the turnaround from eastern Pacific (EP) La Niña to CP El Niño, respectively. Both modes were associated with the cold phase of the Pacific Decadal Oscillation, which played an important role in prolonging the impact of the El Niño/Southern Oscillation on chl-a seasonal evolution from 1998 to 2010. In addition, we discuss the possible factors dominating chl-a seasonal variation, in terms of the subregions of the northwestern Pacific Ocean. In the subtropical northwestern Pacific Ocean (15° N – 30° N), the chl-a growth was primarily nutrient-limited, whereas in the mid-latitude northwestern Pacific Ocean (35° N – 50° N), the chl-a growth was mainly light-limited.     

基于JavaScript的HTML＋MathML通用方案的设计与实现

MathML是一个W3C推荐标准.目前,测览器对MathML的支持比较复杂,(X)HTML+MathML存在多种文档方案,这些方案对运行环境往往有一定的要求和限定,为适应多样化应用的需要,必须考虑保留多种文档方案,导致了数据的大量冗余.本文阐述了现有(X)HTML+MathML文档方案的局限性,提出了一种基于JavaScript的HTML+MathML通用方案.该方案使用JavaScript包含MathML,使得同一个HTML+MathML文档能够实现跨平台、跨浏览器、跨插件的应用,简洁实用,有效地解决了通用性的应用需求.