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Finite element analysis (FEA) was used to model the joining of titanium grade 2 (Ti) to AISI 321 stainless steel (SS) transition joint of lap configuration with grooves at the interface on SS side. The hot forming of Ti for filling the grooves without defects was simulated. FEA involving large plastic flow with sticking friction condition was initially validated using compression test on cylindrical specimen at 900 °C. The barreled shape and a no-deformation zone in the sample predicted by FEA matched with those of the compression experiments. For the joining process, FEA computed the distribution of strain and hydrostatic stress in Ti and the minimum ram load required for a defect-free joint. The hot forming parameters for Ti to fill the grooves without defects and any geometrical distortion of the die were found to be 0.001 s?1 at 900 °C. Using these conditions a defect-free Ti-SS joint was experimentally produced.  相似文献   
3.
Anusuya  P  Kumar  Prashanth  Esakki  Papanasam  Agarwal  Lucky 《SILICON》2022,14(16):10187-10198
Silicon - In this review, we discussed highly sensitive biosensor devices which is having a more attractive, wide scope and development in the sensing field. Biosensor devices can detect the...  相似文献   
4.
Confinement and crowding have been shown to affect protein fates, including folding, functional stability, and their interactions with self and other proteins. Using both theoretical and experimental studies, researchers have established the independent effects of confinement or crowding, but only a few studies have explored their effects in combination; therefore, their combined impact on protein fates is still relatively unknown. Here, we investigated the combined effects of confinement and crowding on protein stability using the pores of agarose hydrogels as a confining agent and the biopolymer, dextran, as a crowding agent. The addition of dextran further stabilized the enzymes encapsulated in agarose; moreover, the observed increases in enhancements (due to the addition of dextran) exceeded the sum of the individual enhancements due to confinement and crowding. These results suggest that even though confinement and crowding may behave differently in how they influence protein fates, these conditions may be combined to provide synergistic benefits for protein stabilization. In summary, our study demonstrated the successful use of polymer-based platforms to advance our understanding of how in vivo like environments impact protein function and structure.  相似文献   
5.
A pulse tube cryocooler (PTC) for future metrological satellites has been developed at one of the lead centers of the Indian Space Research Organisation in Bangalore, India for cooling on-board Infrared (IR) detectors to 80 K.A study has been conducted on the coldfinger of PTC to understand the off-state heat loads on the cooler by varying the value of gravity numerically in ANSYS FLUENT and experimentally by orienting the setup with respect to gravity. The off-state parasitic losses represent a major heat load in on-board applications that include redundant, viz. nonoperating coolers. To find out the amount of off-state parasitic heat losses in a nonoperating coldfinger of the PTC experimentally, transient warm-up technique was used. Various heat loads were applied experimentally on the cryo-tip at temperatures ranging from 80 to 100 K for determining the parasitic losses. The effect of orientation of PTC on the off-state parasitic heat load with respect to gravity is studied and presented in this paper. Enhancement due to free convection heat flow normalized by gas molecular conduction in pulse tube is analyzed using computational fluid dynamics to verify and compare with experimental results. The best orientation angle where the parasitic is low is when the cold end of the coldfinger of pulse tube cryocooler faces down (0°) and high when the cold end of the coldfinger is oriented to 135°.  相似文献   
6.
To demonstrate the development of an oxygen atom microreactor in the form of liquid-helium-cooled solid argon matrix deposited on an infrared (IR) window, the oxidation of ethylene by mobile O atoms has been investigated. O atom diffusion through the argon matrix is confirmed and used to examine ethylene-oxygen atom reactions. In a bench-scale matrix isolation system probed with a Fourier transform infrared (FT-IR) spectrometer, matrices of solid Ar at 8-10 K doped with NO2 and ethylene have been prepared on a ZnSe window within an evacuated cryostat. The matrices have been photolyzed using 350-450 nm photons, and the reaction products resulting from the reaction of O(3P), one of the photolysis products of NO2, with ethylene have been identified using FT-IR and a Gaussian 98W simulation program. These products include oxirane, acetaldehyde, ethyl nitrite radical, and ketene. The temperature effect in the range of 10-30 K on the products formed has also been investigated. The reaction mechanisms are discussed and the viability of the solid Ar matrix being a low temperature microreactor to examine reaction mechanisms of mobile oxygen atoms is elaborated.  相似文献   
7.
In hydraulic fracturing of shale formations, compared to conventional reservoirs, the fracturing fluid injected is of low‐viscosity and hence during pumping the proppant settles significantly, forming a proppant bank. Motivated by this consideration, we initially develop a high‐fidelity process model of hydraulic fracturing to describe the dominant proppant settling behavior during hydraulic fracturing process. Second, a novel remeshing strategy is developed to handle the high computational requirement due to moving boundaries. Third, a section‐based optimization method is employed to obtain key fracture design parameters for enhanced productivity in shale formations subject to given fracturing resources. Fourth, a reduced‐order model is constructed to design a Kalman filter and to synthesize a real‐time model‐based feedback control system by explicitly taking into account actuator limitations, process safety and economic considerations. We demonstrate that the proposed control scheme can regulate the uniformity of proppant bank heights along the fracture at the end of pumping. © 2017 American Institute of Chemical Engineers AIChE J, 64: 1638–1650, 2018  相似文献   
8.
In the present study we made an effort to deploy eco-friendly synthesized reduced graphene oxide/Lanthanum Alluminate nanocomposites (RGO-LaAlO3) and Lanthanum Alluminate (LaAlO3) as adsorbents to remove dye from the synthetic media. XRD, SEM, BET surface area and EDX have been used to characterize the above-mentioned adsorbents. The impacts of different factors like adsorbent dosage, the concentration of adsorbate and PH on adsorption were studied. The best fit linear and nonlinear equations for the adsorption isotherms and kinetic models had been examined. The sum of the normalized errors and the coefficient of determination were used to determine the best fit model. The experimental data were more aptly fitted for nonlinear forms of isotherms and kinetic equations. Pseudo-second-order and Freundlich isotherm model fits the equilibrium data satisfactorily. Methyl orange (MO) has been used as model dye pollutant and maximum adsorption capacity was found to be 469.7 and 702.2 mg g?1 for LaAlO3 and RGO-LaAlO3, respectively.  相似文献   
9.
Kumar  Prashanth  Bhowmick  Brinda 《SILICON》2020,12(4):821-830
Silicon - In this paper, a new structure for a silicon on insulator Schottky barrier MOSFET (SOI SB-MOSFET) has been proposed. The simulated device is calibrated with experimental result. Here...  相似文献   
10.
Green tea is a rich source of catechins, which when purified have a high economic value as they can be used as a supplement in several products, to increase their health benefits. Catechins are regarded as desired components with several applications in a variety of areas such as foods, cosmetics and pharmaceuticals. A multicomponent sorption model has been developed for the separation of catechins from liquid tea streams, with macroporous resins in a packed bed column. Two commercially available food grade resins were considered: Amberlite XADHP and Diaion HP20. For the desorption step, two food grade solvents are used: water and ethanol. The adsorption and desorption behaviour is subsequently mathematically described with one-dimensional axial dispersed plug flow model that can accurately simulate the dynamics of the solvent swing sorption columns. The model parameters were regressed from experimental data. Five components are modelled in the competitive sorption: the main four catechins present in green tea and caffeine. The model was used for the process design and optimization for the recovery of catechins from green tea.  相似文献   
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