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排序方式: 共有689条查询结果,搜索用时 15 毫秒
1.
Haliza Abdul Aziz Noor Azeerah Abas Bonnie Tay Yen Ping Zainab Idris 《Journal of surfactants and detergents》2020,23(2):251-262
The technology for transesterification reactions between methyl esters and alcohols is well established by using classical homogeneous alkaline catalysts, which provide high conversion of methyl esters to specialty or nonindigenous esters. However, in certain products where the purity of the esters is of concern, the removal of homogeneous catalysts after the completion of the reaction is a challenge in terms of production cost and water footprint. Therefore, a study to investigate the potential of heterogeneous catalysts was conducted on reactions between methyl palmitate and triethanolamine. The degree of basicity and active surface area of calcium oxide (CaO), zinc oxide (ZnO), and magnesium oxide (MgO) were first characterized by using temperature-programmed desorption (TPD-CO2) and Brunauere–Emmett–Teller (BET), respectively. Among the metal oxides investigated, the CaO catalyst showed the best catalytic activity toward the transesterification process as it gave the highest conversion of methyl palmitate and yielded fatty esteramine compositions similar to the conventional homogeneous catalyst. The optimum transesterification condition by using the CaO catalyst utilized a lower vacuum system of approximately 200 mbar, which could minimize a considerable amount of energy consumption. Furthermore, low CaO dosage of 0.1% was able to give a conversion of 94.5% methyl ester and formed esteramine at 170 °C for 2 h. Therefore, the production of esterquats from esteramine may become more economically feasible through the methyl ester route by using the CaO catalyst, which can be recycled three times. 相似文献
2.
This paper derives the governing equations for the thermomechanical behaviour of composites. When the basic equations for the thermoelastic behaviour of solids were first derived in the nineteenth century several approximations were made. The effect of these assumptions are discussed and illustrated by the results of a simple laboratory test. The implications of this work on the analysis of impact damaged laminates are then discussed. 相似文献
3.
4.
Rajoo R. Lim S.S. Wong E.H. Hnin W.Y. Seah S.K.W. Tay A.A.O. Iyer M. Tummala R.R. 《Advanced Packaging, IEEE Transactions on》2008,31(2):377-385
A wafer level packaging technique has been developed with an inherent advantage of good solder joint co-planarity suitable for wafer level testing. A suitable weak metallization scheme has also been established for the detachment process. During the fabrication process, the compliancy of the solder joint is enhanced through stretching to achieve a small shape factor. Thermal cycling reliability of these hourglass-shaped, stretch solder interconnections has been found to be considerably better than that of the conventional spherical-shaped solder bumps. 相似文献
5.
Analysis of composite laminates with transverse cracks 总被引:1,自引:0,他引:1
The analysis of the behaviour of composite laminates with general balanced lay-up sequences and containing distributed transverse cracks is discussed and demonstrated in this paper. It is shown that a constitutive model of damage for composites, which has been successfully used to analyse the effects of uniformly distributed transverse cracks in cross-ply laminates, can be readily extended to the analysis of uniformly distributed transverse cracks in more general symmetric laminates. The further extension of the theory to non-uniformly distributed damage can be achieved by finite element analysis. It is shown that the finite element implementation of the theory is particularly simple since the contribution of the damage to the overall behaviour can be incorporated into the force vectors. 相似文献
6.
A Dielectrophoretic Chip With a 3-D Electric Field Gradient 总被引:1,自引:0,他引:1
7.
In this study, the diffusion of various types of solvent in oil palm empty fruit bunch/polyurethane composites, produced from chemically modified empty fruit bunches, was investigated. The solubility parameters and polymer–solvent interaction parameters of the produced composites were determined. The void contents of the composites were also determined before swelling tests to eliminate the free solvent present in the system. From the results obtained, we found that the diffusion of the solvents was dependent on the compatible group available and the voids present in the system. The solubility parameters of the empty fruit bunch/polyurethane composites with different degrees of chemical modification were 11.6 and 11.7 (cal/cm?3)1/2. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
8.
This paper illustrates the application of two fracture criteria, Atluri's T*-integral and Sih's strain energy density factor S for estimating the residual strength of an impact damaged fastener hole in a composite laminate. Finite element analyses are performed, and the magnitude and distribution of T* and S are determined around the delamination. It is found that the profiles of these distributions are extremely complex and sensitive to the modelling of the stress fields close to the delamination. The effects of local closure, shear moduli and cracktip singularity are investigated. It is also shown that the representation of the stress singularity in the finite element model has a strong effect on the distribution of T* and S. The distribution of both T* and S is such that three local maxima occur and are situated at the same locations around the delamination. These locations approximately coincide with the points of maximum growth as revealed by ultrasonic C-scan of the damage growth of several specimens. The T*-integral is shown to be more sensitive to the values of interlaminar shear moduli than S. The results of the analyses suggest that both the T*-integral and S criteria may be successfully employed in the prediction of residual strength. However, S is better at predicting the direction of damage growth provided the stress fields near the delamination can be accurately modelled. 相似文献
9.
David B.H. Tay 《Digital Signal Processing》1997,7(4):229-238
The design problem of multirate filter banks can be divided into two parts. The first part involves the issue of reconstruction error of the signal which consists of three components—aliasing, magnitude, and phase. The second part of the design problem involves the issue of designing good-quality subband filters. There has been a lot of research addressing the first part but there are relatively few good and simple design techniques for the second part. There is a class of techniques which we will refer to as TROV (TRansformation Of Variables) which satisfactorily addresses the two parts of the design problem. Techniques which fall under this class include the McClellan Transformation, Generalized Transformation of Variables, and Frequency Rotation. A survey of the design techniques proposed by different authors in the literature which falls under this class is presented here. First, the similarity and differences of the approaches adopted by different authors is studied. Second, it is shown that the different approaches can be unified. An extension to the design technique is presented which will enhance its flexibility and effectiveness. 相似文献
10.
Francis E. H. Tay Sumit Kanti Sikdar M. A. Mannan 《Journal of Materials Processing Technology》2002,120(1-3)
In many applications, topography represents the main external features of a surface. This paper describes the topography of the flank wear surface and also presents the relationship between the maximum flank wear and the topography parameters (roughness parameters) of the flank wear surface during the turning operation. A modern CNC lathe machine (Okuma LH35-N) was used for the machine turning operation. Three-dimensional surface roughness parameters of the flank wear surface were measured by a surface texture instrument (from Talysurf series) using surface topography software (Talymap). Based on the resulting experimental data, it is found that as the flank wear increases, the roughness parameters (sRa, sRq, and sRt) on the flank surface increase significantly. The greater the roughness value of the flank wear surface, the higher the friction of the tool on the workpiece and the greater the heat generation that will occur, thus ultimately causing tool failure. On the other hand, positive skewness (sRsk) indicates the presence of a small number of spikes on the flank surface of the cutting tool, which could quickly wear off during the machining process. 相似文献