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1.
Polymer networks in which poly(propylene imine) dendrimers (Astramol?) are connected to each other by linear polytetrahydrofuran (polyTHF) segments, were prepared by two methods. The first method was a one‐step procedure in which bifunctionally living polyTHF, obtained by initiation of the THF polymerization with trifluoromethane sulfonic anhydride (triflic anhydride), was reacted with an amino‐dendrimer. This reaction was very fast but did not allow formation of the end products. The second method was a two‐step procedure. In a first step, living polyTHF, prepared with acryloyloxybutyl triflate as initiator, was grafted on an amino‐dendrimer, to form a star‐like, acrylate‐terminated polyTHF multi‐macromonomer with the dendrimer as core. In a second step, networks were obtained by Michael addition between the acrylate end‐groups and unreacted amino‐groups of the dendrimer. This cross‐linking reaction occurred spontaneously upon heating of the solution of the multi‐macromonomer with gelation times varying from a few minutes to a few hours, depending on the temperature and the composition of the prepolymers. With this method it was possible to prepare networks in the form of coatings or films. © 2003 Society of Chemical Industry 相似文献
2.
α,ω-Methacrylate-terminated poly(1,3-dioxolane)s (polyDXL) were synthesized by cationic ring-opening polymerization of DXL in the presence of methylene-bis(oxyethylmethacrylate) as transfer agent. If the initiator concentration is small compared with the transfer agent concentration, the molecular weights of the polymers are governed by the ratio of the reacted monomer to the reacted transfer agent. The α,ω-methacrylate-terminated polyDXLs obtained undergo free radical polymerization with formation of polyacetal networks. The properties of the networks as function of the molecular weight of the corresponding prepolymers are reported. 相似文献
3.
4.
Ackerman Steven J.; Hilsenroth Mark J.; Knowles Eric S. 《Canadian Metallurgical Quarterly》2005,42(2):225
The present study examines the concurrent and predictive relationships between therapist psychodynamic-interpersonal activity and therapist-rated alliance. Ratings from 45 patient and therapist dyads engaged in short term psychodynamic psychotherapy from a point early (3rd or 4th session) and late (the session at which 90% of the treatment was completed) in treatment were used. The results suggest that therapists who have positive views of the alliance early in treatment also have positive views of the alliance later in treatment. Therapists who used psychodynamic-interpersonal activities early in treatment also made use of psychodynamic-interpersonal activities later in treatment. Moreover, the use of psychodynamic-interpersonal activities early in treatment was positively related to both global and specific aspects of therapist-rated alliance late in treatment. (PsycINFO Database Record (c) 2011 APA, all rights reserved) 相似文献
5.
6.
Eric Pardede J. Wenny Rahayu David Taniar 《Journal of Computer and System Sciences》2008,74(2):170-195
With the increasing demand for a proper and efficient XML data storage, XML-Enabled Database (XEnDB) has emerged as one of the popular solutions. It claims to combine the pros and limit the cons of the traditional Database Management Systems (DBMS) and Native XML Database (NXD). In this paper, we focus on XML data update management in XEnDB. Our aim is to preserve the conceptual semantic constraints and to avoid inconsistencies in XML data during update operations. In this current era when XML data interchange mostly occurs in a commercial setting, it is highly critical that data exchanged be correct at all times, and hence data integrity in XML data is paramount. To achieve our goal, we firstly classify different constraints in XML documents. Secondly, we transform these constraints into XML Schema with embedded SQL annotations. Thirdly, we propose a generic update methodology that utilizes the proposed schema. We then implement the method in one of the current XEnDB products. Since XEnDB has a Relational Model as the underlying data model, our update method uses the SQL/XML as a standard language. Finally, we also analyze the processing performance. 相似文献
7.
8.
Eric P. Kvam Ph.D. Srikanth B. Samavedam B.Tech. 《JOM Journal of the Minerals, Metals and Materials Society》1994,46(3):47-51
The Ge-Si on Si epilayer system, besides being an interesting technological system in its own right, is a superb model for strained-layer studies. The point defect and symmetry defect structures associated with compound semiconductors can be avoided, allowing a focus on the mechanics of the system. Dislocation sources, glide behavior, and performance effects have been examined for strained-layer systems. Surprises have appeared along the way, but these materials are now becoming characterized well enough for industrial device applications. 相似文献
9.
M. Nyoka G. Akdogan R. H. Eric N. Sutcliffe 《Metallurgical and Materials Transactions B》2003,34(6):833-842
The process of mixing and solid-liquid mass transfer in a one-fifth scale water model of a 100-ton Creusot-Loire Uddeholm
(CLU) converter was investigated. The modified Froude number was used to relate gas flow rates between the model and its protoype.
The influences of gas flow rate between 0.010 and 0.018 m3/s and bath height from 0.50 to 0.70 m on mixing time were examined. The results indicated that mixing time decreased with
increasing gas flow rate and increased with increasing bath height. The mixing time results were evaluated in terms of specific
energy input and the following correlation was proposed for estimating mixing times in the model CLU converter: T
mix=1.08Q
−1.05
W
0.35, where Q (m3/s) is the gas flow rate and W (tons) is the model bath weight. Solid-liquid mass-transfer rates from benzoic acid specimens immersed in the gas-agitated
liquid phase were assessed by a weight loss measurement technique. The calculated mass-transfer coefficients were highest
at the bath surface reaching a value of 6.40 × 10−5 m/s in the sprout region. Mass-transfer coefficients and turbulence parameters decreased with depth, reaching minimum values
at the bottom of the vessel. 相似文献
10.
In this article, the authors seek to strengthen the theoretical foundation of team and cell formation through the inclusion of human factors. They distinguish three types of team characteristics: global, shared, and compositional attributes. In this last category, they also deal with diversity in teams by addressing three types of variables: demographic characteristics, skills and knowledge, and personality traits. In addition, the authors address the relevance of the structure of diversity in cells. For each of the above‐mentioned groups of team characteristics, their potential impact on team functioning is worked out and discussed with simultaneous consideration of the characteristics of the team task. Three industrial examples are included to illustrate the importance of including worker, team, and work characteristics when designing manufacturing cells. © 2006 Wiley Periodicals, Inc. Hum Factors Man 16: 1–15, 2006. 相似文献