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1.
Juan Chirinos Jose Arévalo Tamara Rajmankina Angel Morillo Darmenia Ibarra Ali Bahsas Alvaro Parada 《Polymer Bulletin》2004,51(5-6):381-387
Summary The complex
5-(C5H5)2Ti
(1-OC(O)C6H5)2
was synthesized and activated with MA0 for ethylene
polymerization. The resultant polymer is UHMW-PE with a
viscosimetric molecular weight of Mv = 6.8 x
106 to 0.7 x
106 g/mol dependent on the
temperature of the reaction. The effects of the Al/Ti molar
ratio and temperature of the reaction on the catalytic activity
and polymer properties were studied. 相似文献
2.
3.
An open-source software including an easy-to-use graphical user interface (GUI) has been developed for processing, modeling and mapping of gravity and magnetic data. The program, called Potensoft, is a set of functions written in MATLAB. The most common application of Potensoft is spatial and frequency domain filtering of gravity and magnetic data. The GUI helps the user easily change all the required parameters. One of the major advantages of the program is to display the input and processed maps in a preview window, thereby allowing the user to track the results during the ongoing process. Source codes can be modified depending on the users' goals. This paper discusses the main features of the program and its capabilities are demonstrated by means of illustrative examples. The main objective is to introduce and ensure usage of the developed package for academic, teaching and professional purposes. 相似文献
4.
A displacement interferometer is described for measuring gauge blocks, in which a spatial filter is used to combine a laser
beam with a white-light beam, and the length of the block is calculated from the phase differences of the laser signal corresponding
to the centers of gravity of the achromatic fringes from the gauge and from the reference plate.
__________
Translated from Izmeritel’naya Tekhnika, No. 9, pp. 3–5, September, 2006. 相似文献
5.
Ana C. Conti‐Silva Deborah H. M. Bastos José A. G. Arêas 《International Journal of Food Science & Technology》2012,47(9):1896-1902
Corn grits that were supplemented with isovaleraldehyde, ethyl butyrate, butyric acid and flavour enhancers were extruded under different processing conditions. Volatile compounds retained in the extrudates were isolated by dynamic headspace and analysed using gas chromatography–mass spectrometry. The expansion ratio, density and cut force to break down the extrudates were evaluated and aroma intensity was assessed using a multisample difference test. Butyric acid showed the greatest retention (96.4%), regardless of the extrusion conditions. All compounds were better retained when samples were extruded at 20% feed moisture and 90 °C processing temperature (2.9–81.0%), conditions that also resulted in greater aromatic intensity (moderate to moderate‐strong intensity). The addition of volatile compounds reduced the expansion ratio and cut force, whereas the addition of flavour enhancers increased the expansion ratio but reduced ethyl butyrate and butyric acid retention. 相似文献
6.
Fikret Kocabaş Özgür Kişi Mehmet Ardiçlioğlu 《Civil Engineering and Environmental Systems》2013,30(4):367-375
Density differences may occur because of temperature differentials, suspended sediments, dissolved salts or other chemicals. Most of the large surface reservoirs are stably stratified throughout most, or all, of the year. One of the means of assisting the management is to allow a selective withdrawal from the reservoir. And while an intake is used for withdrawal (from the lower layer), a maximum discharge is required not allowing the uptake of the upper layer fluids. The value of the intake's vertical distance from the upper layer elevation (submergence) when the upper layer fluids begin to be drawn into the intake is known as ‘critical submergence’. In this study, the critical submergence for a circular intake pipe in a stratified body (which has different layer thickness) is investigated. Experiments were conducted on a vertically flowing downward intake pipe in a still-water reservoir. Artificial neural network (ANN) models and formulas, which are found by the theoretical analysis of critical spherical sink surface (CSSS), are used for the analysis of experimental results. The CSSS has the same centre and discharge as the intake. The ANN model and CSSS results are compared with the experimental results. 相似文献
7.
J. Saúl García-Pérez Sara P. Cuéllar-Bermúdez Alejandra Arévalo-Gallegos José Rodríguez-Rodríguez Hafiz M. N. Iqbal Roberto Parra-Saldivar 《International journal of molecular sciences》2016,17(9)
Supercritical fluid extraction (SFE) is a sustainable technique used for the extraction of lipophilic metabolites such as pigments and fatty acids. Arnica plant is considered a potential candidate material with high antioxidant and antimicrobial activities. Therefore, in this study, a locally available Heterotheca inuloides, also known as Mexican arnica, was analyzed for the extraction of high-value compounds. Based on different pressure (P), temperature (T), and co-solvent (CoS), four treatments (T) were prepared. A maximum 7.13% yield was recovered from T2 (T = 60 °C, P = 10 MPa, CoS = 8 g/min), followed by 6.69% from T4 (T = 60 °C, P = 30 MPa, CoS = 4 g/min). Some bioactive sesquiterpenoids such as 7-hydroxycadalene, caryophyllene and δ-cadinene were identified in the extracts by GC/MS. The fatty acid profile revealed that the main components were palmitic acid (C16:0), followed by linoleic acid (C18:2ω6c), α-linolenic acid (C18:3ω3) and stearic acid (C18:0) differing in percent yield per treatment. Antibacterial activities were determined by the agar diffusion method, indicating that all the treatments exerted strong antibacterial activity against S. aureus, C. albicans, and E. coli strains. The antioxidant capacity of the extracts was also measured by three in vitro assays, DPPH, TEAC and FRAP, using Trolox as a standard. Results showed high antioxidant capacity enabling pharmaceutical applications of Mexican arnica. 相似文献
8.
Ozan Avinc Emine Bakan Aykut Demiral Grkem Gedik Fikret Karc 《Coloration Technology》2020,136(4):356-369
Poly(lactic acid) (PLA) is the first melt‐processable, renewable, sustainable and biodegradable natural‐based synthetic fibre. It has a broad range of uses and combines ecological advantages with outstanding performance in textiles. PLA fibre, as an aliphatic polyester, can be dyed with disperse dyes. Apart from the limited number of commercial disperse dyes, disperse dye exhaustion on PLA is generally lower than that on poly(ethylene terephthalate) (PET). In this study, new heterocyclic disazo disperse dyes, substituted with methyl, nitro and chloro groups at their ortho‐, meta‐ and para‐ positions, synthesised in our previous study, were applied to PLA and PET fibres to examine their dyeing performance, and colour fastness and dye exhaustion properties. Different shades of yellow, orange, reddish brown and brown were obtained. Most of the synthesised novel heterocyclic disazo disperse dyes exhibited good build‐up properties with high K/S levels on both fibres. Para‐ bonding substituent provided higher K/S values than meta‐ and ortho‐ positions for –NO2 and –Cl substituents for both fibres. Overall, the most synthesised novel heterocyclic disazo disperse dyes in this study exhibited good build‐up properties with high K/S, exhaustion and wet fastness levels on both PLA and PET fibres. 相似文献
9.
Fikret Yılmaz Semra Ergen Soon-Jik Hong Orhan Uzun 《International Journal of Hydrogen Energy》2018,43(44):20243-20251
The LaNi5 intermetallic compound is an AB5 type hydrogen storage alloy which exhibits low operating temperature, easy activation, low pressure and tolerance to impurities. In this study, LaNi4.7-x Al0.3Bix (x = 0.0, 0.1, 0.2, 0.3) alloys were produced by melt-spinning technique and the effects of Al and Bi additions on the microstructure, thermal and hydrogen storage properties of LaNi5 were investigated. The results showed that substitution of Ni with Al led to a desired decrease in absorption/desorption plateau pressure and hysteresis without a decrease in hydrogen storage capacity. In contrast, Bi substitution with Ni increased the absorption/desorption plateau pressure, reduced the hydrogen capacity and increased pulverization resistance of the alloy due to the formation of BiLa and AlNi3 intermetallic phases at the grain boundaries. 相似文献
10.
A decentralized control approach is presented for a network of robotic sensors to achieve the global coordination: group aggregation or consensus flocking. Each robotic sensor obeys three local interaction rules: group cohesion, collision avoidance and velocity alignment. Accordingly, the resultant control law for each robotic sensor is composed of three associated control components. The cohesion control component is based on geometry and additionally enables maintaining initial interconnection of network. The alignment control component ensures that all members in an interconnected network eventually reach to a common velocity. The control component for collision avoidance among members, as a passive role, is embedded in cohesion control. Simulation results demonstrate the capability of the proposed control approach in achieving the coordination behaviour with an initially interconnected network. However, we observed that an initially non-interconnected network may also achieve the coordination behaviour depending on the initial distribution and velocities. Initial interconnection of a network is only a sufficient but not essential condition for the network to achieve the coordination behaviour for our control approach. 相似文献