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排序方式: 共有324条查询结果,搜索用时 15 毫秒
1.
Titipong Issariyakul Mangesh G. KulkarniAjay K. Dalai Narendra N. Bakhshi 《Fuel Processing Technology》2007
Transesterification of waste fryer grease (WFG) containing 5–6 wt.% free fatty acid (FFA) was carried out with methanol, ethanol, and mixtures of methanol/ethanol maintaining the oil to alcohol molar ratio of 1:6, and initially with KOH as a catalyst. Mixtures of methanol and ethanol were used for transesterification in order to use the better solvent property of ethanol and rapid equilibrium using methanol. Formation of soap by reaction of FFA present in WFG with KOH instigated difficulty in the separation of glycerol from biodiesel ester. To untangle this problem, two-stage (acid and alkali catalyzed) method was used for biodiesel synthesis. More than 90% ester was obtained when two-stage method was used compared to ∼ 50% ester in single stage alkaline catalyst. In the case of mixed alcohol, a relatively smaller amount of ethyl esters was formed along with methyl esters. Acid value, viscosity, and cetane number of all the esters prepared from WFG were within the range of the ASTM standard. Esters obtained from WFG showed good performance as a lubricity additive. 相似文献
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4.
Marco Dalai Author Vitae 《Automatica》2007,43(8):1418-1425
In this paper we consider the problem of constructing confidence regions for the parameters of nonlinear dynamical systems. The proposed method uses higher order statistics and extends the LSCR (leave-out sign-dominant correlation regions) algorithm for linear systems introduced in Campi and Weyer [2005, Guaranteed non-asymptotic confidence regions in system identification. Automatica 41(10), 1751-1764. Extended version available at 〈http://www.ing.unibs.it/∼campi〉]. The confidence regions contain the true parameter value with a guaranteed probability for any finite number of data points. Moreover, the confidence regions shrink around the true parameter value as the number of data points increases. The usefulness of the proposed approach is illustrated on some simple examples. 相似文献
5.
分析在虚拟环境平台上(虚拟机上),采用原有的和新的方法来裁减Linux系统,得到的效果和意义。 相似文献
6.
高分子量聚氯乙烯树脂增塑,填充体系的物理力学性能研究 总被引:6,自引:1,他引:6
本文研究聚合度及增塑剂、填充剂用量对高分子量聚氯乙烯(HMWPVC)树脂物理力学性能的影响规律,并将国内外HMWPVC树脂以及HMWPVC与通用型PVC树脂进行了性能对比。结果表明,HMWPVC增塑、填充体系的拉什强度、撕裂强度冲击回弹性及压缩永久形变等物理力学性能均随聚合度的提高而有所增加,而且各项性能均优于通用型PVC树脂,可有效地用作橡胶代用品。分子量相同的国内外HMWPVC树脂物理力学性能基本相同。但是,后者随着增塑剂用量的增加,弹性比前者有所提高;随着填充剂用量的增加,性能变化比前者缓慢.增加填充剂用量以降低制品的体积成本。笔者还时两者物理力学性能的差异与颗粒形态之间的关系进行了探讨。 相似文献
7.
In this work, a systematic study has been conducted to optimize the process conditions and to evaluate kinetic parameters for hydrodenitrogenation (HDN) and hydrodesulphurization (HDS) of heavy gas oil derived from Athabasca bitumen using NiMo/Al2O3 catalysts containing phosphorus (P). In the catalyst, the concentration of phosphorus was maintained at 2.7 wt%. Experiments were performed in a tickle‐bed reactor at the temperature, pressure and liquid hourly space velocity (LHSV) of 340‐420°C, 6.1‐10.2 MPa and 0.5‐2 h?1, respectively. H2 flow rate and catalyst weight were maintained constant at 50 mL/min and 4 g, respectively in all cases. Statistical analysis of all experimental data was carried out using ANOVA to optimize the process conditions for HDN and HDS reactions. Kinetic studies for HDN and HDS reactions were studied within the temperature range of 340‐400°C using the power law model as well as the Langmuir‐Hinshelhood model. The power law model showed that HDN and HDS of heavy gas oil follow first order kinetics. The activation energies for HDN and HDS reactions from the power law and Langmuir‐Hinshelwood models were 94 and 96 kJ/mol and 113 and 137 kJ/mol, respectively. 相似文献
8.
Amanda D’Cruz Mangesh G. Kulkarni Lekha Charan Meher Ajay K. Dalai 《Journal of the American Oil Chemists' Society》2007,84(10):937-943
A series of alkali metal (Li, Na, K) promoted alkali earth oxides (CaO, BaO, MgO), as well as K2CO3 supported on alumina (Al2O3), were prepared and used as catalysts for transesterification of canola oil with methanol. Four catalysts such as K2CO3/Al2O3 and alkali metal (Li, Na, K) promoted BaO were effective for transesterification with >85 wt% of methyl esters. ICP-MS analysis
revealed that leaching of barium in ester phase was too high (~1,000 ppm) when BaO based catalysts were used. As barium is
highly toxic, these catalysts were not used further for transesterification of canola oil. Optimization of reaction conditions
such as molar ratio of alcohol to oil (6:1–12:1), reaction temperature (40–60 °C) and catalyst loading (1–3 wt%) was performed
for most efficient and environmentally friendly K2CO3/Al2O3 catalyst to maximize ester yield using response surface methodology (RSM). The RSM suggested that a molar ratio of alcohol
to oil 11.48:1, a reaction temperature of 60 °C, and catalyst loading 3.16 wt% were optimum for the production of ester from
canola oil. The predicted value of ester yield was 96.3 wt% in 2 h, which was in agreement with the experimental results within
1.28%. 相似文献
9.
Algebraic immunity for cryptographically significant Boolean functions: analysis and construction 总被引:13,自引:0,他引:13
Carlet C. Dalai D.K. Gupta K.C. Maitra S. 《IEEE transactions on information theory / Professional Technical Group on Information Theory》2006,52(7):3105-3121
Recently, algebraic attacks have received a lot of attention in the cryptographic literature. It has been observed that a Boolean function f used as a cryptographic primitive, and interpreted as a multivariate polynomial over F/sub 2/, should not have low degree multiples obtained by multiplication with low degree nonzero functions. In this paper, we show that a Boolean function having low nonlinearity is (also) weak against algebraic attacks, and we extend this result to higher order nonlinearities. Next, we present enumeration results on linearly independent annihilators. We also study certain classes of highly nonlinear resilient Boolean functions for their algebraic immunity. We identify that functions having low-degree subfunctions are weak in terms of algebraic immunity, and we analyze some existing constructions from this viewpoint. Further, we present a construction method to generate Boolean functions on n variables with highest possible algebraic immunity /spl lceil/n/2/spl rceil/ (this construction, first presented at the 2005 Workshop on Fast Software Encryption (FSE 2005), has been the first one producing such functions). These functions are obtained through a doubly indexed recursive relation. We calculate their Hamming weights and deduce their nonlinearities; we show that they have very high algebraic degrees. We express them as the sums of two functions which can be obtained from simple symmetric functions by a transformation which can be implemented with an algorithm whose complexity is linear in the number of variables. We deduce a very fast way of computing the output to these functions, given their input. 相似文献
10.
《元朝秘史》电子文本检索系统的研制 总被引:2,自引:0,他引:2
本文概要地介绍13世纪《元朝秘史》的文献背景及原文所独有的复杂文本形式,通过对文本的内涵分析和版面分析,设计了关于《元朝秘史》电子检索系统的研制方案。其中主要解决了原文三行一体显示格式的还原问题,而且系统可以分别对原文汉字音写、汉语译文、汉字旁译、语音语法标注等不同部分进行检索和统计。检索输出结果包括研究者最重视的传统学术章节号、卷页码、在电子文本出现的具体位置。另外,系统对检索词采用了上下文检索技术,输出文本包括检索词的部分上下文内容。本系统基本满足历史、文学和语言研究的应用需求。 相似文献