噻吩在镍基非晶态合金上的吸附和脱附

应用静态吸附、动态吸附、程序升温脱附和程序升温还原等实验方法，考察了噻吩在Ni基非晶态合金上的吸附和脱附行为。常温下，噻吩分子首先吸附在清洁的Ni表面，并立刻被活化，发生氢解反应，C-S键断裂，释放出烃类部分，S留在Ni原子上。噻吩可以在Ni基非晶态合金表面发生强度不同的化学吸附。弱化学吸附的噻吩可以脱附；强化学吸附的噻吩不会脱附，而在高温下发生氢解反应。     

环境保护地理信息系统的设计

本文主要介绍基于计算机网络的通用型环境保护地理信息系统的功能和实现方法。     

JOINING MECHANISMS OF β''''-Al2O3 CERAMIC AND PYREX GLASS TO Al MATRIX COMPOSITE

The bonding of β'-Al2O3 and pyrex glass to Al matrix composites by anodic bonding process is achieved. The microstructure of the bonded interface and the joining mechanisms are analyzed with scanning electron microscope (SEM), energy dispersive X-ray fluorescence spectrometer (EDX). It is observed that the bonding region across the interface consists of the metal layer, oxide transitional layer and the ceramic layer, with the transitional layer composed of surface region and sub-surface region. The bonding process can mainly be categorized into anodic bonding process and solid state diffusing process. The pile-up of the ions and its drift in the interface area are the main reasons for anode oxidation and joining of the interface. The temperature, voltage and the drift ions in the ceramic or glass during the bonding process are the essential conditions to solid state diffusing and oxide bonding at the interface. The voltages, temperature, pressure as well as the surface state are the main factors that influence the anodic bonding.     

兰州重离子加速器大型真空室

已建成的兰州重离子加速器的真空室是一个大型整体结构的超高真空容器,直径约10m,高4.5m,重65000kg,内表面积211m~2,容积100m~3,工作真空度为5×10~(-5)Pa。采用有限单元法在计算机上用SAP-5C程序对真空室受力分析进行了计算。真空室结构材料选用瑞典Uddeholm钢厂生产的316 L 超低碳不锈钢。承制此大型容器的是航天工业部风华机器厂。由于结构庞大,首先将真空室分成八大块和几小块在工厂制造,然后运至现场焊制成一整体容器并进行机械加工。所有密封焊缝均用着色渗透液,X-射线探伤和氦质谱探漏仪进行检查和探漏。     

提高开卷线纵剪机精度的研究

通过对纵剪机右立柱轴承间隙测量方法和左立柱导向结构的改进，保证了加工精度，易于操作，提高了生产效率。     

试论QC小组活动与企业文化建设相结合

本文分析了QC小组活动与企业文化的特点与共同点,提出开展QC小组活动与企业文化建设是互相促进,互相补充的,两者可以互相结合。     

Dielectric and piezoelectric properties of Pb(Ni1/3Nb2/3)O3–PbTiO3–PbZrO3 ceramics modified with bismuth and zinc substitutions

The dielectric and piezoelectric properties of the (Pb_0.985Bi_0.01)(Ni_1/4Zn_1/12Nb_2/3)_x- (Zr_σTi_1-σ)_1-xO₃ piezoelectric ceramic system (0.2 ≤ x ≤ 0.7, 0.1 ≤ σ ≤ 0.9) were systematically investigated. The results showed that, after poling, the dielectric constant, ε ₃₃ ^T , increased for the tetragonal compositions but decreased for the rhombohedral compositions. Furthermore, high values of ε ₃₃ ^T and piezoelectric modulus, d ₃₁ were found for the compositions along the extension of the morphotropic phase boundary. The highest values of the planar electromechanical coupling factor, K _p, and the piezoelectric modulus, d ₃₁, were found to be 0.70 and − 274 × 10^-12 C N^-1, respectively. The Curie temperature, remanent polarization, coercive field and the lattice constants of the a and c axes in relation to the Pb(Ni_1/3Nb_2/3)O₃ content and the Zr/Zr + Ti ratio were also determined. This revised version was published online in November 2006 with corrections to the Cover Date.     

贝利阀在氨厂运行情况简介

介绍贝利阀在试车及试生产期间出现的问题及解决办法，指出维护过程中应注意的事项。     

聚苯乙烯溴代并接技聚二甲基硅氧烷

聚苯乙烯（PS）在苯溶液中与溴代丁二酰亚胺（NBS）反应，经分离提纯得到了固体溴代聚苯乙烯（PSB）。将所得PSB溶于苯并与低分子量的聚二甲基硅氧烷硅醇锂（PDMSOLi）反应，经分离提纯得到固体的溴代聚苯乙烯接枝聚二甲基硅氧烷（PSB－g-PDMSO),所得PSB-g-PDMSO的结构经^1H-NMR、IR及TEM表征。     

油气井射孔器用炸药及其安全性

介绍了中国和美国射孔器所用的单质和混合炸药43种.根据耐热性,射孔器可分为普通型、高温型和超高温型三类.射孔器和炸药的耐热性与其受热时间有关,最后文中叙述了射孔器的安全性能.