The preparation and magnetic properties of Fe-Ag granular solid using a sol-gel method

The Fe-Ag granular metal solid samples with 10% and 30% weight iron have been successfully fabricated using a sol-gel method, which are characterized by X-ray diffraction and transmission electron micrography. The average diameters of iron particles are from about a few nanometres to a few tens of nanometres controlled by the reducing temperature. The evolution of magnetic properties and microstructure during heat treating are described in detail and explained by using the superparamagnetism, single domain and multi domain theories. The magnetic anisotropy of the Fe-Ag granular solid is studied by using the law of approach to saturation. It is found that the magnetic anisotropy constant is in the order of 10⁵ J m^–3 which is higher than the value of the bulk iron and increases with the increase of reducing temperature.     

高校大学生计算机应用能力培养的研究

随着我国的教育体制改革和信息化建设的开展,应用型人才培养模式越来越得到国家的重视,计算机专业作为高校基础应用学科,必须改变培养模式以满足社会需求,本文分析了当前高校计算机应用能力的培养现状,提出从转变教学理念、改善教学方法,建设信息化学习资源,加强学科整合,提升大学生信息素养以增进创新力和竞争力四个方面进行计算机应用能力的培养,并反思可能遇到的问题以便为后续的相关研究提供借鉴和参考。     

防锈油膜在5% Na2SO4溶液中的半导体导电行为

采用电位—电容法及Mott-Schottky分析技术研究了自腐蚀电位条件下防锈油膜在5% Na2SO4溶液中失效过程的导电机制转变行为.防锈油膜在5% Na2SO4溶液中的失效过程存在半导体导电特征，随着浸泡时间的延长，防锈油膜从浸泡初期的p型半导体转变为n型半导体，转变过程中，防锈油膜中出现两个空间电荷过渡层.随着浸泡时间的延长，防锈油膜中的空间电荷层厚度皆逐渐减小，载流子密度则逐渐增加，并且计算了不同转变时期防锈油膜中的电子给体（ND）和电子受体（NA）密度大小.     

Properties of Er3+-doped phosphate glasses and glass fibres and efficient infrared to visible upconversion

Some thermomechanical properties such as expansion, transition temperature and high-temperature viscosity of phosphate glasses with different P₂O₅ and BaO compositions have been measured. Absorption and fluorescence spectra of the phosphate glasses with different Er³⁺ doping have also been measured. The Er³⁺ doping concentration with respect to the maximal fluorescence intensity is 0.75 mol %. The attenuation of the fibre at a wavelength of 1.53 m is 12.8 db m^–1. Upconversion of 1.064 m NdYAG laser pulses into intense green 547 and 667 nm light in the 0.75 mol % Er³⁺-doped phosphate glass fibre has been achieved. The output power of the two fluorescence signals of green 547 nm and red 667 nm are 178 and 42 W, respectively, with an upconversion efficiency of 1.78×10^–2% and 4.2×10^–3% respectively.     

基于软交换的集群媒体服务器的安全问题及其解决方案*

媒体服务器是NGN多媒体业务平台中的关键设备,NGN的安全至关重要。针对一种基于软交换集群媒体服务器的体系结构及其原型系统,详细分析了系统安全性,并给出了相应的解决方案。     

Effects of modified hyperbranched polyester as a curing agent on the morphology and properties of dynamically cured polypropylene/polyurethane blends

The dynamic vulcanization process, usually used for the preparation of thermoplastic elastomers, has been applied to prepare polypropylene (PP)/polyurethane (PU) blends. Boltorn^TM H20 (H20) hyperbranched polyester containing 16 hydroxyl end gropus and pentaerythritol are used as curing agents, respectively, for curing PU oligomer during blending with molten PP. To improve the compatibility of cured PU particles with PP matrix, H20 is partly functionalized with stearic acid. The morphology, mechanical properties, thermal properties and melt flow index (MFI) of the PP/PU blends with different curing agent are investigated. Compared with pentaerythritol, SEM photographs show that H20 partly functionalized with stearic acid effectively reduces the size and size distribution of cured PU particles in PP/PU blends which also is proved by MFI measurement. Consequently, the dynamically cured PP/PU blends with modified H20 have better mechanical properties than those cured with pentaerythritol. The shifts of crystallization peaks to higher temperatures for all PP/PU blends indicate that PU particles in the blends can act as effective nucleating agents. Moreover, due to the smaller size of PU particles PP/PU blends cured with modified H20 have higher crystallization temperatures than those blends cured with pentaerythritol at the same PU content.     

聚碳酸亚乙酯多元醇制备湿固化聚氨酯热熔胶及其性能研究

以聚碳酸亚乙酯多元醇(PEC)、二苯基甲烷4,4'-二异氰酸酯(MDI)和1,4-丁二醇(BDO)为主要原料,采用预聚物法合成了一种新型的湿固化聚氨酯热熔胶,并用聚四氢呋喃二醇(PTMG)型和聚己内酯二醇(PCL)型湿固化聚氨酯热熔胶进行性能比较.结果表明,热熔胶中多元醇种类、催化剂及异氰酸根(-NCO)含量对热熔胶的性能有较大的影响.用预聚物法合成的PEC型聚氨酯热熔胶具有较好的拉伸强度、粘接强度、耐水性能和可生物降解性,是一种新型环保粘接材料.     

高强耐候钢加工成形性能分析及改善措施

高强耐候钢的加工成形性能要求高,使用过程中易出现冲压开裂现象。通过分析高强耐候钢的剪切形貌和冲压工艺原理,解析了高强耐候钢产生冲压开裂现象的原因,采取成分优化和工艺调整等措施,避免了冲压开裂现象,从而得到了加工成形性能优异的高强耐候钢。     

甚宽带PBG滤波器结构

研究了光子带隙结构作为微带电路衬底的情况,分析其阻带特性的形成以及对电路性能的影响.提出了利用级联与混合并联结构设计具有很宽频带的滤波器形式.实验测量了其传输特性,验证了频率阻带的存在和作为宽带滤波器结构的可行性.