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1.
Raman spectra of Graphon carbon black 总被引:1,自引:0,他引:1
The Raman spectrum of Graphon carbon black has been recorded using rotating cell techniques. Angular dependence of scattering at 1360, 1580 and 2700 cm?1 are reported and these data suggest that the 1360 cm?1 line is associated with non-planar microstructure distortions. The excitation frequency dependence of the intensity ratio of the bands at 1360 (D) and 1580 cm?1 (G) is interpreted in terms of resonance (vibronic) interaction. This dependence is primarily the result of an increase in the intensity of the 1360 cm ?1 line. The disorder-associated line (D) exhibits a significant excitation-dependent shift from 1378 cmi?1 (457.9 nm Ar+) to 1330 cm?1 (647.1 nm Kr+). The “graphite” (G) line position is less sensitive to changes in excitation frequency. The spectral features are discussed in terms of factor group, C6v4, and layer site symmetry, C3v. Also the possible role of localized alkene-like structure in zones of structural distortion is considered. 相似文献
2.
This paper presents a rational method (based on Bayes' Theorem) for transferring information on parameter values from one experiment to another, in situations where the mathematical models for the two experiments share some parameters in common. The uncertainty in the estimates of the parameters, which reflects the experimental error in the initial experiment, is properly transferred as well. The use of the method is demonstrated by applying it to a fairly complicated system, typical in chemical reaction engineering, in which the kinetic parameters in a model for the hydrogenolysis of butane reaction were estimated using data obtained from a bench-scale, integral packed-bed reactor. These parameter estimates were then transferred to a model for a fluidized bed reactor in which the same chemical reaction occurred. Using the fluidized bed data they were updated and two additional parameters in the fluidized bed model were also estimated. This procedure allows a more realistic estimate of the uncertainty in all parameter values in the model for the fluidized bed reactor. 相似文献
3.
Supercritical Carbon Dioxide (SC CO2) is used as a reaction/processing medium in the fabrication of fiber‐reinforced composite materials. SC CO2 allows resin (reactive monomer), to penetrate inside the fibers themselves, partitioning into the amorphous regions of the fiber. The crystal structure then templates polymerization of matrix within the fiber. This process produces a composite that exhibits ultralong‐range order from the nanoscale reinforcement of crystals to the macroscale fiber reinforcement of matrix. In addition, SC CO2 lowers resin viscosity and aids in wetting out Nylon 6,6 fiber reinforcement in a process similar to reaction injection molding (RIM) or resin transfer molding (RTM). This article will discuss the fabrication technique in detail, including process parameters and the structure of resulting composites and morphology of modified fibers. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 1600–1607, 2003 相似文献
4.
Kevin A. Masser Joshua A. Orlicki Eugene Napadensky Terrence Taylor Doug Harris 《应用聚合物科学杂志》2021,138(3):49703
A series of transparent methacrylate-based crosslinked polymer networks are prepared in which the crosslinker length is controlled as a means to investigate the effects of network ductility on mechanical and ballistic properties. In each network the optical clarity of pure poly(methyl methacrylate) (PMMA) is retained, as well as a low value of haze. Both the glass transition temperature (Tg) and the tensile modulus of the networks are highly tunable, with network values both above and well below that of pure PMMA or the pure crosslinker network. The ballistic performance is likewise affected, with performance values of up to 400% greater than neat PMMA. We examine the effects of the crosslinker molecular weight on the impact performance, finding that, in these systems, the molecular weight between crosslinks is not a driving factor for the impact performance, and this may broadly translate to polymer networks in general. We find that improvements in ballistic performance can be realized at low molecular weight between crosslinks, provided the crosslinking agent is of sufficient ductility. 相似文献
5.
Vehicle Teleoperation Interfaces 总被引:1,自引:1,他引:0
Despite advances in autonomy, there will always be a need for human involvement in vehicle teleoperation. In particular, tasks such as exploration, reconnaissance and surveillance will continue to require human supervision, if not guidance and direct control. Thus, it is critical that the operator interface be as efficient and as capable as possible. In this paper, we provide an overview of vehicle teleoperation and present a summary of interfaces currently in use. 相似文献
6.
7.
Hard disk drives have to be designed to sustain operational and non-operational shock. There are many analytical models and numerical schemes proposed and many experiments conducted for analyzing the transient impact responses of hard disk drives. The existing researches have been focused on the slider-suspension responses at the head-disk interface in which the linear models have been used and the effects of spindle motor have been ignored. In this study, the complex vibrations of disk of 3.5 in. hard disk drive (HDD) under shock are experimentally investigated. The hammer impact test and linear drop test are conducted for the HDD to study the effect of shock on the disk responses. The results show that the nonlinear rock modes substantially contribute to the vibrations of disk when HDD is under shock impact. The nonlinear properties of the disk responses and the mode damping ratio are evaluated by using empirical mode decomposition approach. 相似文献
8.
9.
It is well known that the dynamic response rate of the Severinghaus-type CO2 electrode is improved significantly in some cases by addition of the enzyme carbonic anhydrase to the electrode assembly. Hysteresis in the response rate also is reduced. Experimental data and modelling results indicate that catalysis of the CO2 hydration reaction in the bulk of the bicarbonate layer (the Nernst film) is not responsible for the improved response behavior, Evidence is presented to show that catalysis in the electrostatic double layer region at the glass electrode surface is a possible explanation. This proposed phenomenon may have widespread implications for the optimal design of analytical devices, commercial processes involving electrochemical phenomena, and may also provide insight into electrobiologi-cal processes. 相似文献
10.
Terrence B. Lindemer Theodore M. Besmann Carl E. Johnson 《Journal of Nuclear Materials》1981,100(1-3):178-226
This paper considers the phase equilibria of alkali metal oxides and their combinations with other oxides relevant to nuclear fuels, fission products, and structural materials. The other oxides include those of the lanthanides, the actinides, iron, nickel, aluminum, silicon, as well as those of periodic table groups IIA, IVB, VB, VIB, and VIA. The alkali metal halides, chalcogenides, and hydroxides are also included. Techniques are developed to permit calculation of phase equilibria and Ellingham diagrams in ternary and higher-order systems. These techniques include estimation of previously unknown 298.15 K values of the enthalpies of formation and the entropies of many compounds. 相似文献