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排序方式: 共有161条查询结果,搜索用时 15 毫秒
1.
Jayaprakash Vandana Kaliyur Ravi Shri Aishvarya Vinni Novi Swaroopini Ramachandran Hridya Radhakrishnan Vaidyanathan Vinoth Kumar 《IET nanobiotechnology / IET》2017,11(6):690
The present study deals with the production of 5‐hydroxymethyl furfural (HMF) from fructose by chemo‐conversion method using chemical catalyst, conventionally achieved by microwave‐assisted dehydration process. Five different chemical catalysts, namely oxalic acid, phosphotungstic acid and mesoporous titanium dioxide nanoparticles (TNPs) were compared at constant conditions of which TNPs yielded a maxima of 33.95%. The optimum temperature and catalyst loading were found to be 200°C and 20%, respectively, at a 5% optimum substrate concentration during 15 min optimum reaction time to yield 61.53% HMF. The efficiency of synthesised TNPs was investigated further through reusability studies. TNPs were properly recycled and the catalytic activity recovery was good even after a 14 batch reactions. The specific surface area of the TNP obtained is about 105.46 m2 /g and its pore‐volume is about 0.42 cm3 /g according to single point adsorption. A large accessible surface area combined with a minimal pore size (15.92 nm) obtained with mesoporous TNPs is desirable for better catalyst loading, high‐yield HMF, retention and reduced diffusion constraints.Inspec keywords: mesoporous materials, recycling, production management, dissociation, nanoparticles, nanotechnologyOther keywords: mesoporous titanium dioxide nanocatalyst, recyclable approach, one‐pot synthesis, 5‐hydroxymethyl furfural production, HMF, chemo‐conversion method, chemical catalyst, microwave‐assisted dehydration process, oxalic acid, phosphotungstic acid, mesoporous titanium dioxide nanoparticles, TNP 相似文献
2.
Rewari Sonam Nath Vandana Haldar Subhasis Deswal S. S. Gupta R. S. 《Microsystem Technologies》2019,25(5):1537-1546
Microsystem Technologies - In this paper a cylindrical Dual Metal (DM) Dielectric Engineered (DE) Gate All Around (GAA) MOSFET has been proposed to resolve a big issue of Gate Inducted Drain... 相似文献
3.
Graph clustering is successfully applied in various applications for finding similar patterns. Recently, deep learning- based autoencoder has been used efficiently for detecting disjoint clusters. However, in real-world graphs, vertices may belong to multiple clusters. Thus, it is obligatory to analyze the membership of vertices toward clusters. Furthermore, existing approaches are centralized and are inefficient in handling large graphs. In this paper, a deep learning-based model ‘DFuzzy’ is proposed for finding fuzzy clusters from large graphs in distributed environment. It performs clustering in three phases. In first phase, pre-training is performed by initializing the candidate cluster centers. Then, fine tuning is performed to learn the latent representations by mining the local information and capturing the structure using PageRank. Further, modularity is used to redefine clusters. In last phase, reconstruction error is minimized and final cluster centers are updated. Experiments are performed over real-life graph data, and the performance of DFuzzy is compared with four state-of-the-art clustering algorithms. Results show that DFuzzy scales up linearly to handle large graphs and produces better quality of clusters when compared to state-of-the-art clustering algorithms. It is also observed that deep structures can help in getting better graph representations and provide improved clustering performance. 相似文献
4.
Saili Dharadhar Sagar Dhoble Vandana Patravale 《Drug development and industrial pharmacy》2019,45(2):188-201
Transdermal route has been explored for various agents due to its advantage of bypassing the first pass effect and sustained release of drug. Due to strong barrier properties of the skin, mainly stratum corneum (SC), the delivery of many therapeutic agents across the skin has become challenging. Few drugs with specific physicochemical properties (molecular weight <500?Da, adequate lipophilicity, and low melting point) can be effectively administered via transdermal route. However, delivery of hydrophilic drugs and macromolecular agents including peptides, DNA and small interfering RNA is challenging. Drug penetration through the SC may involve bypass or reversible disruption of SC layer by various means. Recently, the use of micron-scale needles has been proposed in increasing skin permeability and shown to dramatically increase permeation, especially for macromolecules. Microneedles (MNs) can penetrate through the SC layer of the skin into the viable epidermis, avoiding contact with nerve fibers and blood vessels that reside primarily in the dermal layer. This review summarizes the types of MNs and fabrication techniques of different types of MNs. The safety aspects of the materials used for fabrication have been discussed in detail. Biological applications and relevant phase III clinical trials are also highlighted. 相似文献
5.
Structural Characteristics and Electrical Conductivity of Spark Plasma Sintered Ytterbia Co‐doped Scandia Stabilized Zirconia 下载免费PDF全文
Vandana Shukla Ashutosh Kumar Ishamol Labbaveettil Basheer Kantesh Balani Anandh Subramaniam Shobit Omar 《Journal of the American Ceramic Society》2017,100(1):204-214
The effect of replacing Sc2O3 with Yb2O3 on the structural and electrical properties of xYb2O3–(12–x)Sc2O3–88ZrO2 has been investigated. Spark plasma sintering technique is employed to fabricate dense bulk samples from the nano‐sized powders. X‐ray diffraction and transmission electron microscopy performed on pellets indicate the existence of cubic and rhombohedral phases in 12ScSZ, and a single cubic phase in all the co‐doped compositions. However, Raman spectroscopic studies suggest the presence of a metastable tetragonal t″‐phase along with rhombohedral phases in 12ScSZ, whereas a single cubic phase in all the co‐doped compositions. Significant enhancement in the conductivity of grain and grain boundary is observed on replacing Sc2O3 with Yb2O3. In the intermediate temperature range, 1Yb11ScSZ exhibits the highest, while 12ScSZ shows the lowest conductivity values, which is attributed to corresponding phases present in that range. Through co‐doping with >1 mol% Yb2O3 leads to conductivity decrease, but the value remains higher than that of 12ScSZ. A sharp conductivity change is observed in 12ScSZ and 1Yb11ScSZ samples, which is attributed to partial phase transition as well to the formation of cation‐vacancy complexes. In this work, the beneficial effect of Yb2O3 co‐doping in 12ScSZ on the phase and conductivity has been highlighted. 相似文献
6.
Vandana Srivastava Petr Chýlek R G. Pinnick R. L. Dod T. Novakov 《Aerosol science and technology》2013,47(1):151-160
We collected several samples of fresh snow from the areas of southern New Mexico and western Texas. Samples were analyzed to determine graphitic carbon content of snow in rural and urban areas and to compare these present values with those obtained from deep ice core samples several thousand years old. To model the optical properties of snow grains containing carbon we used several different versions of effective medium approximations. Calculations are compared with microwave analog measurements to determine which of these approximations can reasonably well predict the properties of mixtures such as snow and carbon. Suggestions regarding which of the effective medium approximations that should not be used are presented. 相似文献
7.
Poly(acrylamide) functionalized chitosan: An efficient adsorbent for azo dyes from aqueous solutions
In the present communication we report on the optimization of persulfate/ascorbic acid initiated synthesis of chitosan-graft-poly(acrylamide) (Ch-g-PAM) and its application in the removal of azo dyes. The optimum yield of the copolymer was obtained using 16 × 10−2 M acrylamide, 3.0 × 10−2 M ascorbic acid, 2.4 × 10−3 M K2S2O8 and 0.1 g chitosan in 25 mL of 5% aqueous formic acid at 45 ± 0.2 °C. Ch-g-PAM remained water insoluble even under highly acidic conditions and could efficiently remove Remazol violet and Procion yellow dyes from the aqueous solutions over a pH range of 3–8 in contrast to chitosan (Ch) which showed pH dependent adsorption. The adsorption data of the Ch-g-PAM and Ch for both the dyes were modeled by Langmuir and Freundlich isotherms where the data fitted better to Langmuir isotherms. To understand the adsorption behavior of Ch-g-PAM, adsorption of Remazol violet on to the copolymer was optimized and the kinetic and thermodynamic studies were carried out taking Ch as reference. Both Ch-g-PAM and Ch followed pseudo-second-order adsorption kinetics. The thermodynamic study revealed a positive heat of adsorption (ΔH°), a positive ΔS° and a negative ΔG°, indicating spontaneous and endothermic nature of the adsorption of RV dye on to the Ch-g-PAM. The Ch-g-PAM was found to be very efficient in removing color from real industrial wastewater as well, though the interfering ions present in the wastewater slightly hindered its adsorption capacity. The data from regeneration efficiencies for ten cycles evidenced the high reusability of the copolymer in the treatment of waste water laden with even high concentrations of dye. 相似文献
8.
Temporal Process Discovery in Many Guises 总被引:1,自引:0,他引:1
9.
Sneh Punia Bangar Monica Trif Fatih Ozogul Manoj Kumar Vandana Chaudhary Milan Vukic Maharishi Tomar Sushil Changan 《Comprehensive Reviews in Food Science and Food Safety》2022,21(2):1958-1978
According to the Food and Agriculture Organization of United Nations reports, approximately half of the total harvested fruits and vegetables vanish before they reach the end consumer due to their perishable nature. Enzymatic browning is one of the most common problems faced by fruit and vegetable processing. The perishability of fruits and vegetables is contributed by the various browning enzymes (polyphenol oxidase, peroxidase, and phenylalanine ammonia-lyase) and ripening or cell wall degrading enzyme (pectin methyl-esterase). In contrast, antioxidant enzymes (superoxide dismutase and catalase) assist in reversing the damage caused by reactive oxygen species or free radicals. The cold plasma technique has emerged as a novel, economic, and environmentally friendly approach that reduces the expression of ripening and browning enzymes while increasing the activity of antioxidant enzymes; microorganisms are significantly inhibited, therefore improving the shelf life of fruits and vegetables. This review narrates the mechanism and principle involved in the use of cold plasma technique as a nonthermal agent and its application in impeding the activity of browning and ripening enzymes and increasing the expression of antioxidant enzymes for improving the shelf life and quality of fresh fruits and vegetables and preventing spoilage and pathogenic germs from growing. An overview of hurdles and sustainability advantages of cold plasma technology is presented. 相似文献
10.
Vandana Kumari Manoj Saxena R.S. Gupta Mridula Gupta 《Microelectronics Reliability》2012,52(8):1610-1612
This paper analyzes the effect of temperature variation on various device architectures i.e. Insulated Shallow Extension Silicon On Nothing (ISESON), ISE and SON MOSFET using ATLAS 3D device simulator for 45 nm gate length. The simulation results obtained with the ATLAS has been validated by comparing it with reported experimental data of SON MOSFET. The simulation results demonstrate that out of three device designs, the ISESON MOSFET is the most suitable device for high speed, low voltage and high temperature applications. The integration of ISE and SON onto the conventional bulk MOSFET leads to the enhancement in analog device performance in terms of device efficiency (gm/Ids), device gain (gm/gd), output resistance (Rout) and early voltage (Vea). 相似文献