In situ polymerization and characterization of polyester‐based polyurethane/nano‐silica composites

Polyester‐based polyurethane/nano‐silica composites were obtained via in situ polymerization and investigated by Fourier‐transform infrared spectroscopy (FTIR), or FTIR coupled with attenuated total reflectance (FTIR‐ATR), Transmission electron microscopy (TEM), atomic force microscopy (AFM), an Instron testing machine, dynamic mechanical analysis (DMA) and ultraviolet‐visible spectrophotometry (UV‐vis). FTIR analysis showed that in situ polymerization provoked some chemical reactions between polyester molecules and nano‐silica particles. FTIR‐ATR, TEM and AFM analyses showed that both surface and interface contained nano‐silica particles. Instron testing and DMA data showed that introducing nano‐silica particles into polyurethane enhanced the hardness, glass temperature and adhesion strength of polyurethane to the substrate, but also increased the resin viscosity. UV‐vis spectrophotometry showed that nano‐silica obtained by the fumed method did not shield UV radiation in polyurethane films. Copyright © 2003 Society of Chemical Industry     

焊接史

本文追溯了19世纪末发明的电弧焊接的历史。当Oscar Kjellberg成立伊萨公司以探索他发明的涂层焊条时，伊萨从一开始就和电弧焊的发展结下了不解之缘。     

Multistage amplifier topologies with nested Gm-Ccompensation

This paper presents a multistage amplifier for low-voltage applications (<2 V). The amplifier consists of simple (noncascode) low gain stages and is stabilized using a nested transconductance-capacitance compensation (NGCC) scheme. The resulting topology is similar to the well known nested Miller compensation (NMC) multistage amplifier, except that the proposed topology contains extra G _m feedforward stages which are used to enhance the amplifier performance. The NGCC simplifies the transfer function of the proposed multistage amplifier which, in turn, simplifies its stability conditions. A comparison between the NGCC and NMC shows that the NGCC has wider bandwidth and is easier to stabilize. A four-stage NGCC amplifier has been fabricated using a 2-μm CMOS process and is tested using a ±1.0 V power supply. A dc gain of 100 dB has been measured. A gain bandwidth product of 1 MHz with 58° of phase margin and power of 1.4 mW can be achieved. The op amp occupies an active area of 0.22 mm². Step response shows that the op amp is stable     

Statistical analysis of decision threshold for parallel acquisitionwith reference filtering in Rician fading channel

Statistical analysis of the decision threshold for parallel PN code acquisition in a Rician fading channel is presented. It is shown that in the performance analysis of the acquisition system with reference filtering, the statistical evaluation of the decision threshold seems more appropriate than the approximation of the decision threshold     

我国明矾石的物化性质及其在水泥中的水化硬化

本文系统地介绍了我国明矾石的地质成因、化学成份和矿物组成及其在水泥中的水化硬化,提出了明矾石在碱-硫酸盐激发下形成钙矾石的水化机理,综述了我国利用明矾石作为特种水泥、外加剂的原料及作为普通水泥的混合材所取得的应用成果。     

新农村建设规划过程中的问题与对策探析——以都昌县新农村建设为例

建设社会主义新农村,要坚持规划先行,在当前新农村建设的过程中,合理地进行村庄建设规划具有重要的意义。本文就都昌县目前农村建设的现状及新农村建设规划过程中出现的相关问题进行探析,并对都昌县新农村建设提出了可行性的对策。     

循环经济在赣州矿产资源开发与管理中的研究

如何利用赣州矿产资源优势发展本地经济,节约资源开采,充分利用现有资源,实现资源的循环利用,保持生态环境的良好发展具有重要意义。本文分析介绍了循环经济、赣州矿产资源及开发利用现状,并提出了实现矿业循环经济的具体措施。     

Application of scanning tunnelling microscopy to the quality control of tungsten carbide (WC-Co) ball bearings

Scanning tunnelling microscopy (STM) has been applied to the topographical study of tungsten carbide (with 6% Co) ball bearings in air. It is shown that, for this material, scanning tunnelling microscopy can provide not only general topographical information on the surface microtexture with a resolution of nearly 0.1 nm if required, but also quantitative information for the measurement of surface roughness. Thus, scanning tunnelling microscopy has utility as a quality control tool of particular relevance in the submicron range. The STM topographical results from specific tungsten carbide ball bearings are presented, and the limitations and applicability of the STM technique when used as a quality control tool are discussed.