高Bs的NiZn铁氧体材料的研制

以高纯度的NiO、ZnO、Fe2O3为原料,采用氧化物陶瓷工艺制备了高Bs NiZn铁氧体材料.通过岩崎B-H Analyzer SY-8232、Agilent 4285A和4284A多频LCR测试仪分析了NiO含量对材料的饱和磁感应强度、起始磁导率、Q值的影响;通过扫描电镜(SEM)观测样品的晶粒.结果表明,当NiO、ZnO、Fe2O3含量比为0.6:0.4:1、烧结温度为1140℃时,材料饱和磁感应强度大于480mT.     

退火工艺对射频磁控溅射Bi:YIG薄膜磁性能的影响

对于用射频磁控溅射技术在Si基片上制备的Bi:YIG系薄膜,用快速循环退火方法对其进行晶化处理,研究了退火温度对Bi:YIG薄膜结晶状态和形貌的影响,以及退火气氛和循环周期对薄膜性能的影响.结果表明,用快速循环退火可以在si单晶基片上得到磁性能优良的薄膜(饱和磁化强度139 kA/m,矫顽力6.37 kA/m)并使薄膜形貌有较大改善,在石英基片上制备的薄膜法拉第角比常规退火的薄膜增大了约一倍.     

Application of high-temperature permanent magnets Sm（Co,Fe, Cu,Zr）z in PPM focusing system

Rare earth permanent magnets Sm（Co, Fe, Cu, Zr）z with outstanding performance and high-temperature thermal stability were fabricated. Optimized by Fe content and process, Sm（Co0.72Fe0.15Cu0.1Zr0.03）7.5 magnet with B1〉0.75 T and Hci〉1300 kA/m at 300 ℃ can be obtained. According to the performance data of Sm（Co0.72Fe0.15Cu0.1Zr0.03）7.5, the magnetic field along central axis Bz in periodic permanent magnet （PPM） focusing system was simulated using electromagnetic field analysis software Maxwell 2D/3D. The Bz exhibited typical cosine curve along central axis, and the peak value of Bz was high enough to meet the demand of PPM focusing system at room temperature even at 200±20 ℃. Additionally, a kind of simple cooling structure for PPM focusing system was designed by setting cooling pipe between polepieces. Simulated results showed that smooth cosine curve of Bz was successfully achieved with good control of the thickness of cooling pipe.     

线性自旋阀读磁头的材料性能及结构参数优化（二）

优化材料性能参数和自旋阀巨磁电阻磁头的结构参数是磁器件实用化的关键。基于建立的物理计算模型,首先将自旋阀巨磁电阻磁头传感单元作为有源磁电阻放入前端放大电路,对输出电压,二次谐波及线性区间进行态模拟发现在宽ｇ１＋ｇ２≤０．７μｍ,线性偏电流１０－５０ｍＡ范围内,自旋阀磁头相对记录介质有线性信号输出。     

烧结温度对镍锌功率铁氧体磁性能的影响

为得到Zn含量不同时NiZn铁氧体材料的最佳烧结温度,用氧化物法制备了NiZn铁氧体材料,研究了烧结温度对材料起始磁导率、功耗、饱和磁感应强度和微结构的影响.结果表明,适宜的烧结温度对制备功耗低、饱和磁感应强度高和较优起始磁导率的NiZn铁氧体材料至关重要,而Zn含量不同时对应材料的最佳烧结温度也各不相同.     

Rare earth doped CaCu_3Ti_4O_(12) electronic ceramics for high frequency applications

Ca1-xRxCu3Ti4O12(R=La,Y,Gd;x=0,0.1,0.2,0.3) electronic ceramics were fabricated by conventional solid-state reaction method.The microstructure and dielectric properties as well as impedance behavior were carefully investigated.XRD results showed that the secondary phases with the general formula R2Ti2O7 existed at grain boundaries of rare earth doped ceramics,which inhibited abnormal grain growth.The dielectric constant decreased from 4×105 in pure CaCu3Ti4O12(CCTO) ceramics to 2×103 with rare earth doping.However,all samples showed high dielectric constant in broad frequency range(10 MHz).The cutoff frequency(f0) was remarkably shifted to higher frequency from 13 MHz(pure CCTO ceramics) to 80 MHz(Gd-doped CCTO ceramics).Meanwhile,the dielectric loss tangent rapidly decreased approximately 10 times.These improvements of dielectric properties by rare earth doping are very useful in wide frequency chip capacitor and LTCC devices.     

磁性微电子机械系统(MMEMS)中的关键问题

磁性微电子机械系统(MMEMS)是在传统的微电子机械系统(MEMS)基础上发展的,它在科学研究及应用领域中有着巨大的潜力.磁性材料和MEMS技术的兼容性问题此前已作为一个重要的问题论述过.本文就磁性MEMS技术中的线圈制作、软磁膜制备及硬磁膜制备等关键性问题加以概述.     

(Ba1-xSrx)3Co2Fe24O41材料的磁化处理与烧结特性

研究了采用固相法制备的(Ba1-xSrx)3Co2Fe24O41材料的烧结特性,讨论了预烧工艺、烧结温度、保温时间、降温方式等与材料显微结构及性能的关系。为了展宽频带,将永磁铁氧体制造中的磁化处理工艺“移植”到了该材料的制备中。结果显示：引入磁化处理措施有望改善材料性能。引入磁化处理后,优化的制备条件为配合料经1200℃预烧2h,升温速度为1℃／min;样品在1220～1240℃烧结1～3h,缓慢降温,所制得的样品共振频率高达1．8GHz以上,截止频率在1GHz附近,起始磁导率在5～13之间。介电常数ε低于30。     

乙二胺四乙酸含量对M型钡铁氧体薄膜磁性能和微波性能的影响

采用有机金属裂解法在Pt/TiO2/SiO2/Si基板上制备M型钡铁氧体(Ba M)薄膜,并着重研究了螯合剂乙二胺四乙酸(EDTA)含量对Ba M薄膜结构、磁性和微波性能的影响。研究发现,当EDTA∶(Ba2++Fe3+)=1(摩尔比)时,Ba M薄膜形成较多的六角形状晶粒,而且磁性能和微波性能较佳,沿c轴生长的取向度高达0.91,饱和磁化强度Ms为302k A/m(μ0Ms=0.38T),在50GHz时铁磁共振线宽ΔH为22k A/m(277Oe)。这是因为适量的EDTA不仅在溶液挥发时能够阻止金属离子的分离和间歇性的沉淀,并且能够促进成形成均匀的前驱液,从而在前驱液分解时能促进形成Ba M,在经过热处理后易形成沿c轴取向、具有六角形状晶粒的Ba M薄膜。     

磁阻传感器的多相滤波模型

提出了一种新颖的倾斜多相滤波(SMPF)磁阻器件设计模型,采用这种SMPF模型设计的磁阻传感器,可以滤去n(n=2,3,4…[V])次谐波;倾斜相角Δθ=2π/3时,波形畸变最小;具有正弦输出的编码器被研制,实验发现当倾角φ=5°[p=0.8mm,l=3mm,Δθ=2π/3]时输出为正弦波,与SMPF理论值φ=4.904°相吻合,这一结果可以广泛于磁阻传感器领域。