H5N1亚型禽流感病毒免疫血清精制工艺的建立

目的建立马抗H5N1亚型禽流感病毒免疫血清的精制工艺。方法以硫酸铵盐析法提取免疫马血浆中的IgG抗体,以8～256μg/mgIgG胃蛋白酶(活性单位1:3000)进行消化,以阳离子交换层析柱纯化F(ab’)2抗体,并参照《中国药典》三部(2005版)要求,对试制的样品进行检定。结果经一步50%硫酸铵和多步33%硫酸铵盐析,获得了较为纯净的IgG抗体。8μg胃蛋白酶用量可完全消化1mgIgG抗体分子,阳离子交换方法分离F(ab’)2抗体纯度可达90%以上,高于常规工艺制备的抗体纯度。以此工艺试制的样品,各项质量指标均符合《中国药典》三部(2005版)质量标准。结论已初步建立了马抗H5N1亚型禽流感病毒免疫血清的精制工艺。     

Development of palm-based reference materials for the quantification of fatty acids composition

Characterisation of fatty acids composition of three palm-based reference materials was carried out through inter-laboratory proficiency tests. Twelve laboratories collaborated in these tests and the fatty acids compositions of palm oil, palm olein and palm stearin were determined by applying the MPOB Test Methods p3.4:2004 and p3.5:2004. Determination of consensus values and their uncertainties were based on the acceptable statistical agreement of results obtained from the collaborating laboratories. The consensus values and uncertainties (%) for each palm oil reference material produced are listed as follows : 0.20% (C12:0), 1.66+/-0.05% (C14:0), 43.39+/-0.39% (C16:0), 0.14+/-0.06% (C16:1), 3.90+/-0.11% (C18:0), 40.95+/-0.23% (C18:1), 9.68+/-0.21% (C18:2), 0.16+/-0.07% (C18:3) and 0.31+/-0.08% (C20:0) for fatty acids composition of palm oil; 0.23+/-0.04% (C12:0), 1.02+/-0.04% (C14:0), 39.66+/-0.19% (C16:0), 0.18+/-0.07% (C16:1), 3.81+/-0.04% (C18:0), 44.01+/-0.08% (C18:1), 10.73+/-0.08% (C18:2), 0.20+/-0.06% (C18:3) and 0.34+/-0.04% (C20:0) for fatty acids composition of palm olein; and 0.20% (C12:0), 1.14+/-0.05% (C14:0), 49.42+/-0.25% (C16:0), 0.16+/-0.08% (C16:1), 4.15+/-0.10% (C18:0), 36.14+/-0.77% (C18:1), 7.95+/-0.29% (C18:2), 0.11+/-0.07% (C18:3) and 0.30+/-0.08% (C20:0) for fatty acids composition of palm stearin.     

L-赖氨酸锌螯合物的研究

以L-赖氨酸盐酸盐和氢氧化锌为原料,按摩尔比为2∶1在70℃水浴中搅拌反应2 h,得到了产率为91.05%的赖氨酸锌螯合物。产品经纯化后通过IR,UV,TG-DTG,元素分析及X射线粉末衍射等分析手段进行了表征,推测出了螯合物的分子组成为Zn(lys)2.2H2O,测定了赖氨酸锌的稳定常数K=1.788×105。     

关于增加轧件外端改善无缝钢管变形的讨论

简述了变形体外端的含义及作用,介绍了几个轧钢生产中应用增加轧件外端方法来减少金属不均匀变形的实例,用外端理论解释了无缝钢管生产中在管坯尾部定心的原理和作用,提出了张力减径机轧制无缝钢管时采用半无头、无头轧制工艺的设想,并分析了采用半无头、无头轧制工艺生产时可能出现的问题。     

石家庄轴承设备有限公司顺利完成公司搬迁和企业改制

近日,石家庄轴承设备有限公司顺利完成了公司搬迁和企业改制工作,由原来的国有企业改制成为民营企业。改制后,石家庄轴承设备有限公司的经营管理团队拥有完全独立的经营自主权,灵活的营销机制,使原有的机械加工能力和科技研发能力优势更加突出,企业具有更大活力和发展空间。特别是公司的独立开发设计机构系河北省企业技术中心,公司科技研发的后盾,为公司生产科技含量更高的高频直缝焊管、冷弯型钢等系列生产线提供了保障,     

天津钢管集团股份有限公司φ720mm机组试制成功φ720mm×22mm气瓶用无缝钢管

日前,天津钢管集团股份有限公司根据用户要求,使用斜轧扩径工艺,按照ASMESA372标准,研制出当前市场急需的规格为φ720mm×22mm的气瓶用无缝钢管。该规格钢管是制作固定式天然气储气站用气瓶的重要原料。目前公司正在向国家相关部门申请对该产品进行型式试验。     

有限元模拟法分析斜轧扩管机变形特点

以Φ720mm斜轧扩管机为研究对象,应用三维有限元模拟仿真技术,对斜轧扩管过程进行了建模与仿真分析,获得了钢管的变形数据,在此基础上计算了斜轧扩管的主变形和附加变形,从变形的角度说明了辗轧角β和轧辊在垂直方向的调整距离h取值及相应工具设计的合理性。研究结果有助于了解斜轧扩管的工艺实质,提高产品质量。     

退火温度对(Pb_(0.5)Sr_(0.5))TiO_3薄膜光学性能的影响(英文)

以三水醋酸铅、醋酸锶、钛酸丁酯为原料,乙二醇甲醚、去离子水、乙酰丙酮做溶剂。用溶胶-凝胶法制备(Pb0.50Sr0.50)TiO3 (PST)前驱体溶液,通过旋涂工艺在石英玻璃基片上沉积 PST 薄膜。薄膜经 650 至 800 ℃退火 30 min,升温速率为 3℃/min。不同温度晶化的 PST 薄膜用 X 射线衍射测量其晶体结构,用原子力显微镜观测其表面形貌。不同温度退火薄膜的光学透射谱用双光束紫外-可见光分光光度计测量。薄膜的吸收边,即带隙能可以根据直接跃迁估计。650、700、 750 和 800℃退火的薄膜样品的直接带隙能分别为 3.74、3.75、3.76 和 3.75 eV。     

天津钢管集团有限公司PQF机组稳产高产

2005年上半年，天津钢管集团有限公司的φ160mm PQF机组充发挥出产品精度高、质量好、生产节奏快的优势。在试轧钻具管等新品种，部分产品根据用户要求按理论重量交货实行负偏差轧制，以及调试142孔型的情况下，     

Use of electronic probes for classifying lamb carcasses

Three commercially available electronic lamb carcass grading probes (Hennessy Grading Probe, AUS-Meat Sheep Probe, Swedish FTC Lamb Probe) and one developmental probe (Ruakura GR lamb probe) were assessed for accuracy and suitability for use on-line on the lamb dressing chain for objectively classifying lamb carcasses. GR is the total tissue thickness over the 12th rib taken at a distance 11 cm from the mid-line, used to define fatness in lamb carcass grading in New Zealand. Probe measurements were compared with manually measured GR (sometimes used at present) and Toland probe measurements (total tissue depth between the ribs) for accuracy of predicting both GR on the right side of the carcass and also carcass water (indicating muscle) and fat content. Probes were tested on six occasions, each having approximately 50 lambs. All probes combined with carcass weight accounted for over 70% of the variation (R(2)) of GR right, with GR left accounting for 92% of the variation of GR right. Inclusion of a quadratic probe term was not quite as useful as inclusion of carcass weight for predicting GR right. The three commercial electronic probes individually when combined with carcass weight could account for 36-49% of the variation in the percentage of water and fat in the carcass, with the manual GR probe (right) on the chilled carcass accounting for 55% of the variation in water and 58% of the variation in fat percentages. Chilled carcass measurements are expected to give better results than readings on hot carcasses. The use of a quadratic probe coefficient instead of carcass weight with the probe readings gave similar accuracy of prediction of carcass composition. There was little difference between the two sides in the accuracy of prediction. Small differences were found between regressions relating probe readings to GR and composition for the different probing occasions. The electronic probe results from this trial are consistent with overseas results where probes are in use for objectively grading the carcasses of meat animals.