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91.
A detailed elaboration of the transformations of iron species, present in natural and Fe(NO(3))(3) loaded montmorillonite, during carbon deposition and carbon nanotube growth is described. According to transmission electron microscopy results, deposited carbon atoms form fibres in the case of pristine montmorillonite and multiwalled carbon nanotubes in the case of Fe(III) loaded montmorillonite. M?ssbauer and x-ray diffraction analysis results point to an extensive reduction of structural and intercalated Fe(III) cations to Fe(II) with the latter migrating from the interlayer space to the vacant octahedral sites of the mineral's lattice. Such migration of the non-structural iron catalyst prohibits extensive contamination of the final composite with various metal catalyst impurities. The crucial role of the active catalytic centres in the formation of carbon nanotubes is ascribed to a minor quantity of iron, found entrapped in the carbon nanostructures, which, at the end of the reaction, is identified as iron carbide. The interesting formation of a nanometric γ-iron precipitate is also detected, which is probably stabilized through strong interactions with the lattice of montmorillonite. Finally, it is demonstrated that iron-rich natural clay minerals can serve as direct catalysts for carbon nanotube growth. 相似文献
92.
Panorgias A Kulikowski JJ Parry NR McKeefry DJ Murray IJ 《Journal of the Optical Society of America. A, Optics, image science, and vision》2012,29(2):A233-A239
A characteristic shift in hue and saturation occurs when colored targets are viewed peripherally compared with centrally. Four hues, one in each of the red, blue, green, and yellow regions of color space, remain unchanged when presented in the peripheral field. Apart from green, these peripherally invariant hues correspond almost exactly in color space with the unique hues. We explore this puzzling observation using asymmetric color-matching and color-naming experiments and computing cone contrasts for peripheral and central stimuli. We find that the difference between cone contrasts for the peripheral and central stimuli reaches a maximum at the chromatic axis corresponding to peripherally invariant green. We speculate that the effect is linked to a weakened signal from M-cones and probably associated with a reduced number of M-cones in peripheral retina. 相似文献
93.
Athanasios V. Papageorgiou Charis J. Gantes 《Canadian Metallurgical Quarterly》2010,136(10):1234-1247
The present work deals with the dynamic response of structures that are irregular in height, consisting of two parts, a lower part made of concrete and an upper part made of steel. Irregularity is due to different dynamic responses of the two parts, here expressed by their different damping ratios and inelastic material laws. The seismic design of such structures is not satisfactorily covered by current design codes, especially if a decoupled procedure is chosen for the analysis, where the lower part is excited first and its response is used as excitation for the upper part. The present paper aims at contributing toward better understanding of the interaction between the two parts and at proposing improved decoupling criteria for the seismic analysis of inelastic primary-secondary systems. Toward that goal, each part is modeled as a one-degree-of-freedom system, and the maximum responses of coupled and decoupled inelastic time history analyses are compared over a wide range of dynamic characteristics and strength levels of the two parts. The results are presented in the form of error levels between the two alternative analysis procedures. 相似文献
94.
Athanasios Batagiannis Michael Wübbenhorst Jürg Hulliger 《Current Opinion in Solid State & Materials Science》2010,14(5):107-115
In recent decades piezo- and pyroelectricity found application in yet another important field of research. A number of methods have been developed which employ these properties to investigate the micro- and macroscopic polarization of materials. Advances in piezo- and pyroelectric imaging enabled researchers to examine the polarization distribution of a sample with unprecedented detail. This review attempts to inform the general reader about some of those experimental techniques and their findings. 相似文献
95.
The current work presents a parametric study, which involves different generalized nonlinear mechanical formulations with different damping characteristics to account for the interaction between a monopile‐supported offshore wind turbine and the surrounding soil. The novelty of the study lies in the fact that recently developed nonlinear mechanical models used so far for the simulation of high‐damping rubber isolators are introduced to describe the nonlinear hysteretic soil behavior. More specifically, the first generalized mechanical model consists of a combination of elastoplastic and trilinear elastic elements (labeled as model 3), while the second model consists of trilinear hysteretic models connected in parallel with trilinear elastic springs and hysteretic dampers used to ensure that the unloading stiffness will be as close as possible to the initial stiffness of the system (labeled as model 4). These newly developed models are compared with well‐known models within the industry, namely, a model that comprises elastoplastic elements (labeled as model 1) and a model that comprises trilinear elastic springs (labeled as model 2). All these models provide exactly the same effective stiffness, but on the other hand different levels of damping are involved in each one of them. The goal of the present work is 3‐fold, introducing novel mechanical models for the simulation of soil behavior, to investigate the effect of different soil damping levels in the response of offshore wind turbines and to highlight the limitations of the commonly used models within the industry. To this end, the differences between the response due to different levels of damping characteristics and modeling approaches are shown, highlighting the importance of soil damping in the overall response of the system. 相似文献
96.
This paper presents an analytical multi-criterion analysis for the prioritisation of risks for the development of tidal energy projects. After a basic identification of risks throughout the project and relevant stakeholders in the UK, classified through a political, economic, social, technological, legal and environmental analysis, relevant questionnaires provided scores to each risk and corresponding weights for each of the different sectors. Employing an extended technique for order of preference by similarity to ideal solution as well as the weighted sum method based on the data obtained, the risks identified are ranked based on their criticality, drawing attention of the industry in mitigating the ones scoring higher. Both methods were modified to take averages at different stages of the analysis in order to observe the effects on the final risk ranking. A sensitivity analysis of the results was also carried out with regard to the weighting factors given to the perceived expertise of participants, with different results being obtained whether a linear, squared or square root regression is used. Results of the study show that academics and industry have conflicting opinions with regard to the perception of the most critical risks. 相似文献
97.
Wentao Wang José M. Herreros Athanasios Tsolakis Andrew P.E. York 《International Journal of Hydrogen Energy》2013
In this paper we show, for the first time, the feasibility of ammonia exhaust gas reforming as a strategy for hydrogen production used in transportation. The application of the reforming process and the impact of the product on diesel combustion and emissions were evaluated. The research was started with an initial study of ammonia autothermal reforming (NH3 – ATR) that combined selective oxidation of ammonia (into nitrogen and water) and ammonia thermal decomposition over a ruthenium catalyst using air as the oxygen source. The air was later replaced by real diesel engine exhaust gas to provide the oxygen needed for the exothermic reactions to raise the temperature and promote the NH3 decomposition. The main parameters varied in the reforming experiments are O2/NH3 ratios, NH3 concentration in feed gas and gas – hourly – space – velocity (GHSV). The O2/NH3 ratio and NH3 concentration were the key factors that dominated both the hydrogen production and the reforming process efficiencies: by applying an O2/NH3 ratio ranged from 0.04 to 0.175, 2.5–3.2 l/min of gaseous H2 production was achieved using a fixed NH3 feed flow of 3 l/min. The reforming reactor products at different concentrations (H2 and unconverted NH3) were then added into a diesel engine intake. The addition of considerably small amount of carbon – free reformate, i.e. represented by 5% of primary diesel replacement, reduced quite effectively the engine carbon emissions including CO2, CO and total hydrocarbons. 相似文献
98.
Athanasios Iliopoulos John G. Michopoulos 《International journal for numerical methods in engineering》2013,95(4):313-330
Full‐field strain measurement techniques are based on computing the spatial derivatives of numerical or functional approximations of the underlying displacement fields extracted from digital imaging methods. These methods implicitly assume that the medium satisfies the strain compatibility conditions, which are only true in the case of a continuum body that remains continuum throughout its deformation history. In the present work, we introduce a method that can be used to calculate the strain components directly from typical digital imaging data, without the need of the continuum hypothesis and the need for displacement field differentiation. Thus, it enables the measurement of strain fields from imaged surfaces that may or may not contain discontinuities. Numerical comparisons are performed on the basis synthetic data produced from an analytical solution for an elastically orthotropic open‐hole domain in tension. For performance comparison purposes, the mean absolute error distributions are calculated for the cases of both the traditional meshless random grid method, and the direct strain method introduced herein. It is established that the more refined representation of strain provided by our present approach is more accurate everywhere in the domain, but most importantly, near its boundaries. Published 2013. This article is a US Government work and is in the public domain in the USA. 相似文献
99.
Cyril Caliot Gilles Flamant Giorgos Patrianakos Margaritis Kostoglou Athanasios G. Konstandopoulos 《American Institute of Chemical Engineers》2012,58(8):2545-2556
A two‐dimensional model of methane thermal decomposition reactors is developed which accounts for coupled radiative heat and polydisperse carbon particle nucleation, growth, and transport. The model uses the Navier–Stokes equations for the fluid dynamics, the radiative transfer equation for methane and particle species radiation absorption, the advection–diffusion equation for gas and particle species transport, and a sectional method for particle species nucleation, heterogenous growth, and coagulation. The model is applied to a tubular laminar flow reactor. The simulation results indicate the development of a reaction boundary layer inside the reactor, which results in significant variation of the local particle size distribution across the reactor. © 2011 American Institute of Chemical Engineers AIChE J, 58: 2545–2556, 2012 相似文献
100.
Ioannis Sakaridis Ioannis Ganopoulos Nikolaos Soultos Panagiotis Madesis Athanasios Tsaftaris Anagnostis Argiriou 《European Food Research and Technology》2014,238(4):691-697
Lactic acid bacteria (LAB) are a complex group of Gram-positive bacteria belonging to different genera with common morphological, metabolic and physiological characteristics. Their classification was initially based on biochemical methods, but nowadays molecular methods are usually applied for the identification of LAB. Herein, real-time PCR assay coupled with high-resolution melting (HRM) analysis was developed for identifying and distinguishing LAB isolates coming from poultry carcasses. The 16S rRNA gene from these isolates was amplified using primers that annealed to conserved regions. The melting curve analysis of the amplicons classified all isolates into ten LAB species and generated ten distinct HRM curve profiles. The results from HRM analysis were compared to those produced by API 50 CH biochemical microkits and ribosomal DNA sequencing, suggesting the superiority of HRM against API. In conclusion, HRM was proven to be a fast, reliable and cost-effective method for identification of LAB isolates. HRM analysis could be used in order to reduce the time needed for the identification assay and the cost of sequencing the entire group of LAB isolates. The melting profile of known LAB species could be used as a reference for the rapid identification of unknown LAB isolates without the need of sequencing. 相似文献