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191.
H Soleimani Z Abbas N Yahya K Shameli H Soleimani P Shabanzadeh 《International journal of molecular sciences》2012,13(7):8540-8548
The sol-gel method was carried out to synthesize nanosized Yttrium Iron Garnet (YIG). The nanomaterials with ferrite structure were heat-treated at different temperatures from 500 to 1000 °C. The phase identification, morphology and functional groups of the prepared samples were characterized by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR), respectively. The YIG ferrite nanopowder was composited with polyvinylidene fluoride (PVDF) by a solution casting method. The magnitudes of reflection and transmission coefficients of PVDF/YIG containing 6, 10 and 13% YIG, respectively, were measured using rectangular waveguide in conjunction with a microwave vector network analyzer (VNA) in X-band frequencies. The results indicate that the presence of YIG in polymer composites causes an increase in reflection coefficient and decrease in transmission coefficient of the polymer. 相似文献
192.
Mohammad Razzaghi Afzal Karimi Hassan Aghdasinia Mohammad-Taghi Joghataei 《Korean Journal of Chemical Engineering》2017,34(11):2870-2878
Horseradish peroxidase (HRP) and glucose oxidase (GOx) were co-immobilized on polyurethane, and the resulting HRP/GOx/polyurethane biocatalyst was characterized using scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDAX) mapping techniques. The prepared biocatalyst was used for removal of acid orange 7 as model azo dye. The required H2O2 for activation of HRP was in-situ produced using GOx to prevent deactivation of HRP in the presence of excess chemical H2O2. Central composite design (CCD) was applied for modeling and optimization of parameters affecting the activity of prepared biocatalyst. Under the optimum conditions, removal efficiency of the azo dye was predicted to be 87.47%, which was in good agreement with the experimental value (89.69%). In addition, the performance of the prepared biocatalyst for removal of two other dyes with different structure was investigated at the optimum conditions, and a removal efficiency of 91.56% and 95.25% was obtained for removal of methylene blue and malachite green, respectively. The results demonstrated that the resultant HRP/GOx/Polyurethane biocatalyst was able to decrease the chemical oxygen demand (COD) of a textile effluent from 740mg/L to 96mg/L, indicating that the prepared biocatalyst is an effective enzymatic system for treatment of real wastewater. 相似文献
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194.
F. Hosseini Seyed Hassan Jafari Hossein-Ali Khonakdar Majid Abdouss 《Polymer-Plastics Technology and Engineering》2019,58(7):732-741
This paper deals with influence of chitosan nanoparticles (CNPs) loaded by tetracycline, as a drug, on the physico-mechanical and antibacterial properties as well as drug release behavior of poly(vinyl alcohol), PVA, hydrogels prepared by electron beam irradiation. The formation of spherical chitosan particles in nanoscale size prepared by an ionic gelation method was confirmed by FTIR and UV spectroscopy, and scanning electron microscopy analyses. The drug release kinetic studies from drug loaded chitosan nanoparticles (DLCNPs) at pH = 7.4 revealed a linear and steady release behavior over long period of time. The theoretical analysis of the swelling kinetic data, using Peppas’s model showed that the swelling kinetic is governed by Fickian diffusion for all the prepared hydrogels, however, the water diffusion coefficient, and therefore, the swelling content were lower for the hydrogels loaded with DLCNPs as compared to the ones with the neat drug. In agreement with these results, the hydrogels containing DLCNPs exhibited a more controlled drug release behavior with significantly stronger antibacterial activity. The tensile mechanical properties of the hydrogels not affected by the DLCNPs were found to be suitable for wound dressing applications. 相似文献
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197.
Zubair Butt Riffat Asim Pasha Faisal Qayyum Zeeshan Anjum Nasir Ahmad Hassan Elahi 《Journal of Mechanical Science and Technology》2016,30(8):3553-3558
Energy harvesting is the process of attaining energy from the external sources and transforming it into usable electrical energy. An analytical model of piezoelectric energy harvester has been developed to determine the output voltage across an electrical circuit when it is forced to undergo a base excitation. This model gives an easy approach to design and investigate the behavior of piezoelectric material. Numerical simulations have been carried out to determine the effect of frequency and loading on a Lead zirconate titanate (PZT-5A) piezoelectric material. It has been observed that the output voltage from the harvester increases when loading increases whereas its resonance frequency decreases. The analytical results were found to be in good agreement with the experimental and numerical simulation results. 相似文献
198.
Rasoul Safdarian Korouyeh Hassan Moslemi Naeini Gholamhosein Liaghat 《Journal of Materials Engineering and Performance》2012,21(10):2053-2061
The forming limit diagram (FLD) is a useful method for characterizing the formability of sheet metals. In this article, different numerical models were used to investigate the FLD of tailor-welded blank (TWB). TWBs were CO2 laser-welded samples of interstitial-free (IF) steel sheets with difference in thickness. The results of the numerical models were compared with the experimental FLD as well as with the empirical model proposed by the North American Deep Drawing Research Group. The emphasis of this investigation is to determine the performance of these different approaches in predicting the FLD. These numerical models for FLD are: second derivative of thinning (SDT), effective strain rate (ESR), major strain rate (MSR), thickness strain rate (TSR), and thickness gradient (TG). Results of this research show necking will be happened, when the value of MSR, TSR, ESR criteria is maximum, TG????0.78 and SDT criterion has the first peak in forming process time. The value of dome height of TWB samples at failure was predicted based on the numerical models for samples with different widths. These numerical predictions were compared with the experimental results. The SDT model indicates a better agreement with experimental results in prediction of both the FLD and the limit dome height (LDH) in comparison to the other numerical models. Both numerical and experimental results show that minimum of LDH is happened in plane strain condition. 相似文献
199.
Aziz UI Hassan Mohsan Zhanqiang Liu G. K. Padhy 《The International Journal of Advanced Manufacturing Technology》2017,88(1-4):107-113
Self-conditioning performance of polishing pad is an important characteristic to influence processing efficiency and service life in chemical mechanical polishing (CMP). The slurry can react with the pad surface, which affects its self-conditioning performance in fixed abrasive polishing process. Wear ratio of wafer material removal rate (MRR) and pad wear rate is introduced to evaluate self-conditioning performance of fixed abrasive pad (FAP). To clear the effect of chemical additive on FAP self-conditioning, wear ratio, FAP surface topography, friction coefficient, and acoustic emission signal of polishing process were investigated in fixed abrasive polishing of quartz glass with ferric nitrate, ethylenediamine (EDA), and triethanolamine (TEA) slurry, respectively. Results indicate that TEA slurry can provide excellent self-conditioning of FAP in fixed abrasive polishing of quartz glass. MRR and wear ratio maintain high levels during the whole polishing process. Friction coefficient and acoustic emission signal are more stable than that of the other two chemical additives. An appropriate amount of TEA, which is beneficial to enhance MRR and extends service life of FAP, is added in the polishing slurry to improve FAP self-conditioning in fixed abrasive polishing process. 相似文献
200.
Vahid Zal Hassan Moslemi Naeini Ahmad Reza Bahramian Jos Sinke 《The International Journal of Advanced Manufacturing Technology》2017,89(1-4):207-217
Semi-crystalline thermoplastic-based composite laminates and fiber metal laminates have a narrow forming temperature window, which limits formability of these products. The intention of this study was investigation of non-melting amorphous polyvinyl chloride as a proper matrix to increase the formability and forming temperature window of these products. For this, [45/?45] and [0/90] layups of polyvinyl chloride-based composite laminates and fiber metal laminates were produced using the film-stacking procedure and later press formed into channel sections at six temperatures in the range of 80 to 200 °C. The effects of the layups and forming temperatures on the forming loads and spring back of the formed profiles were measured, and their effects on the fiber buckling, wrinkling, and delamination of the profiles were evaluated using optical microscope images. The effects of layups and forming temperatures on the deformation mechanisms were also analyzed using the grid strain analysis method. Of the fiber metal laminates, 160 °C was found as the minimum forming temperature, and for the composite laminates, 120 and 160 °C were found as the minimum proper forming temperatures of [45/?45] and [0/90] layups, respectively. Finally, the forming temperature windows and formability of polyvinyl chloride matrix composite laminates and fiber metal laminates were found higher than semi-crystalline matrices. 相似文献