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991.
992.
铌酸对酯化反应催化性能的研究 总被引:1,自引:0,他引:1
研究了新型固体酸催化剂铌酸对乙醇及异戊醇与乙酸酯化反应的催化性能、研究表明热处理温度对水洗法制备的铌酸催化剂的催化活性有显著影响,在350℃处理时活性达到极大值.与HZSM-5相比,铌酸催化剂不仅在乙醇和乙酸的气相酯化反应中表现出良好的催比性能,而且在异戊醇和乙醇的液相酯化反应中亦表现出较好的催化活性和稳定性. 相似文献
993.
Statistical studies of branched ester latex and paint properties 总被引:3,自引:0,他引:3
R. A. Prior W. R. Hinson O. W. Smith D. R. Bassett 《Progress in Organic Coatings》1996,29(1-4):209-224
Vinyl versatate, butyl acrylate and 2-ethylhexyl acrylate were compared as comonomer, for colloid-stabilized vinyl acetate latex polymers to assess their impact on latex coating properties. Vinyl versatate afforded advantages in scrub resistance, gloss, hydrophobicity and higher glass transition temperatures. Butyl acrylate developed better wet adhesion efficiency, gel content and hiding efficiency. 2-Ethylhexyl acrylate offered performance comparable to butyl acrylate in hiding efficiency, lowering copolymer glass transition temperatures, and gloss development. Combinations of these monomers, in many instances, afforded a better balance of performance properties than individual monomers alone. In the subject study, a simplex-centroid design was utilized to statistically map polymer compositions for determining the effect of comonomer composition on latex and paint film properties. In addition to developing contour maps of polymer and paint properties as a function of composition, a technique for studying structure-property relationships is presented. 相似文献
994.
It is shown that steady-state kinetic data do not allow the discrimination between the redox and associated mechanisms of the partial oxidation reactions. A discrimination between these mechanisms was performed using transient experiments. The obtained rate expressions are in agreement with experimental kinetic data for catalytic partial oxidation of o-xylene.
An influence of the conjugate oxidation of a catalyst surface on dynamics and kinetics of the heterogeneous catalytic oxidative reactions is considered. Computing simulation of methane oxidative coupling of methane reaction at lowered temperature and elevated pressure has been performed. It showed that the reaction order with respect to oxygen exceeding unity is consistent with the chain branching mechanism of the reaction in the presence of TiSi2 and TiB2 and showed the important role of the branching chain cycles in the low-temperature OCM reaction at elevated pressure. 相似文献
995.
本文将奇异摄动系统看成是存在参数扰动的广义系统的一种特殊形式,然后利用广义系统特征结构配置来使广义系统的有限闭环极点尽可能接近奇异摄动系统的闭环主导极点,从而达到近似配置奇异摄动系统主导极点的目的。本文提供的算法是数值稳定的。 相似文献
996.
EuLisp has an integrated object system with reflective capabilities. We discuss some example applications which use these facilities to experiment with some advanced and powerful concepts, namely, finalization, virtual shared memory and persistence. A secondary goal is to attempt to illustrate the additional possibilities of metaobject programming over non-metalevel techniques. 相似文献
997.
In this paper the modelling, analysis and optimization of millimeter wave oscillatorsare investigated by using the a frequency-domain harmonic balance technique (FDHB), where theexternal-circuit impedances looking outside from the active device are calculated with a combinedtechnique of modes expansion, Galerkin, and collocation methods. The optimization results arein agreement with the experimental ones, which show the reliability of the presented model andoptimization. 相似文献
998.
分析和总结了飞机各种机动动作的内在因素,提出了目标机动规范模型,研究了模型的数学描述方式、控制参量的相互约束关系及其组织形式,并通过模拟导弹对目标的攻击过程对模型进行了验证。 相似文献
999.
1000.
Iron pyrite films prepared by sulfur vapor transport 总被引:4,自引:0,他引:4
Iron films deposited via thermal evaporation, with a thickness between 100 and 250 nm, were converted into FeS2 by open sulfur transport using nitrogen as a gas vector. The films thus obtained constituted a single pyrite phase and were optically highly absorbing. The sulfurization process was optimized. As a result, sample temperature and conversion time were found to be the major determining parameters. The films were characterized using several methods. The crystallinity and phase identification were determined by X-ray diffractometry. Scanning electron microscopy showed a homogeneous surface of both iron and pyrite layers. Optical transmission measurements confirmed the highly absorbing character of FeS2 and allowed the determination of direct (1.35 eV) and indirect (0.82 eV) transitions. 相似文献