化学还原法制备纳米铜粉的研究

本文采用KBH4在液相中化学还原CuSO4,并加入KOH和络合剂EDTA ,制得了纳米级的纯净的铜粉 ,通过调整反应物的浓度 ,可以消除Cu2 O等杂质。制备的纳米铜粉还存在一定程度的团聚 ,需试验加入分散剂来改善。     

Effect of dual-scale microstructure on the toughness of laminar zirconia composites

Numerical study by the finite element method (FEM) is performed to investigate the effect of dual-scale microstructure on the toughness of laminar zirconia composite. The computation is based on the micromechanics constitutive model of polycrystal transformation plasticity developed by Sun et al. [10] where both transformation induced shear and softening effects during autocatalytic transformation are taken into account. The numerical simulation presented in this paper successfully reproduced the experimentally observed two effects of the dual-scale microstructure on the toughness of laminar zirconia composite, i.e., the truncation of the elongated transformation frontal zone that forms in single phase Ce-ZrO₂ and the propagation of the transformation zone along the layers normal to the crack plane. Quantitative analysis on the role of microstructure in transformation toughening of laminar zirconia composite is first carried out in the present work which will provide a starting point for the microstructural design of this novel advanced composite in the future.Presented at the Far East Fracture Group (FEFG) International Symposium on Fracture and Strength of Solids. 4–7 July 1994 in Xi'an, China.     

无机膜的应用与展望

本文综述了无机膜的发展、制备方法和应用。     

自发参量下转换制备双光子纠缠态在量子信息学中的应用

叙述了自发参量下转换制备双光子纠缠态技术的发展历程、技术原理以及在量子信息学中的应用，并介绍了国内这一领域的进展。     

压电类智能层合结构的力学和计算模型综述

综述了压电类智能层合结构的力学和计算模型。基于大量国内外有关压电类智能层合结构的文献 ,根据各自采用的运动学假设、场变量的近似、压电层的表达法以及曲率和温度的影响 ,对压电层合结构的力学和计算模型进行了分类 ,阐述了各种理论的特点及一般形式。     

Comparison of Markov model and fault tree approach in determining initiating event frequency for systems with two train configurations

This study explores the use of Markov models in some areas of systems analysis in which time evolution of the system may be a significant factor in influencing the system reliability or availability. Comparisons are made between the Markov models and the time-averaged fault tree models for determining support system failure initiating event frequency in a nuclear power plant, for both power and shutdown conditions. Factors affecting consistency between the fault tree approach and the Markov model approach are studied for systems with common two train configurations. A correlation is developed to estimate the ratio between initiator frequencies through both approaches for a two parallel component system. Insights are developed as to when time averaged and simplified fault tree models support a good approximation to the more rigorous time-dependent Markov models.     

FE Simulation for Internal Inversion of Aluminium Alloy Tube

1 Introduction A double-walled invertube is difficult to fabricate other than applying inversion process. Such kind of invertube can be used as impact energy absorbing element in transport vehicles, like aircrafts and automobiles. Reddy T Y[1] did the analysis of Internal inversion and calculated the inversion load. Reid[2] et al. examined nosing and internal inversion of cold drawn steel tube by the finite element package ABAQUS. Recently, Rosa P A[3] et al. investigated Internal invers…     

下消化道出血DSA诊断及栓塞结合小剂量垂体后叶素灌注治疗

目的探讨不明原因下消化道出血的DSA诊断及介入栓塞治疗的临床应用价值.方法对32例不明原因下消化道出血患者行DSA检查,通过显示造影剂外溢、病理血管和肿瘤染色来确定出血原因及部位,对出血处行超选择性动脉栓塞治疗和留置导管灌注小剂量垂体后叶素维持12 h止血治疗.结果DSA诊断阳性率75%(24/32),其中肠伤寒2例,肠结核1例,血管性病变14例,肿瘤7例.阳性者介入手术成功20例,手术成功率83.3%,无一例严重并发症.结论DSA检查和介入治疗对诊断不明确或保守治疗无效的下消化道出血有着重要的诊断及治疗     

阳离子化多元醇防塌剂的研制

室内研究和现场应用表明,聚乙烯醇类防塌剂表现出较明显的增粘负效应,可引起钻井液粘度的急剧增加,严重影响其推广应用.通过金属盐催化降解和阳离子化反应,研制出了抑制性好且增粘负效应低的阳离子化改性多元醇防塌剂.考察了阳离子化试剂、反应温度、反应时间对取代度、反应效率和产品主要性能的影响,得出了阳离子化多元醇防塌剂最佳制备条件,即：PVA与阳离子化试剂物质的量比为1：1,反应温度为50℃,反应时间为4 h,阳离子度可达0.435.