Freestanding Alumina Membrane by Double-Layer Anodization

A novel method has been developed for fabricating full or partial freestanding anodic alumina. In our method a sacrificial metal layer is introduced between an Al film and a Si₃N₄ substrate. A freestanding alumina film at wafer scale is successfully achieved by anodizing the double metal layer, during which the alumina is spontaneously stripped off the Si₃N₄ substrate due to the anodic oxidation of the sacrificial layer. The barrier oxide of the alumina film is effectively removed either by H₃PO₄ dissolution or by CF₄ reactive ion etching. The freestanding alumina film is utilized as a contact mask to transfer its nanoporous pattern to a Si substrate. By patterning the sacrificial metal layer with contact lithography, a partial freestanding alumina film is successfully achieved on the silicon chip, producing a unique micro/nanofluidic channel. Compared with previous techniques, the method reported here is advantageous for its simplicity and flexibility     

A Microfluidic Device to Acquire Gaseous Samples Via Surface Tension Held Gas-Liquid Interface

We present a relatively simple and effective method for acquiring gaseous samples into microfluidic channels. Hydrophobic polymers are photopatterned on hydrophilic substrates. Due to surface tension, aqueous liquid is confined by the hydrophobic polymers, but not completely blocked by a physical wall, thus allowing an interface for gas-liquid interaction. Here, the mechanism is demonstrated by using hydrophobic (poly)iso-bornyl acrylate polymer patterns on hydrophilic glass substrates, and through a Nessler's reagent-ammonia reaction that exhibits changes in color and electrical resistance.     

泥土中微量六氯环戊二烯的气相色谱分析

采用SE 3 0为固定液进行色谱柱分离 ,用外标定量法测定泥土中的微量六氯环戊二烯 ,结果最小检知量为 0 .18× 10 - 6 ,相关系数为 0 .99992。     

Study on Adsorption Behavior of Rare Earth Complexes on Nanometer-Size Titanium Dioxide with ICP-AES

Inrecentyears ,rareearthelements (REEs)havebeenwidelyusedinfunctionalmaterials ,cata lystsandotherproductsinindustry ,diagnosisreagentsofmagneticresonanceimaging (MRI)inmedicineandsomefertilizersinagricultureespeciallyinChina .However,asaresultoftheirusage ,moreandmoreREEsaregettingintotheenvironment,andalsointohumanbodyviafoodchain[1,2 ] .Itisnotclearwhetherrareearthelementsareessentialforman ,soitisveryurgenttostudythebiologicaleffectofrareearthelementsinhumanhealthandenvironment .Inthes…     

国有施工企业走向市场应关注的几个问题

从辩证关系角度详细阐述了类似于北京燕化建筑工程公司这样的国有施工企业走向市场过程中应关注的企业定位、利益相关性、竞争策略与公平性、自我保护与內涵发展等问题,以促进国有施工企业的改革与发展。     

润滑油基础油的现状及发展趋势

叙述了内燃机油的发展对基础油的要求，并对传统工艺和加氢工艺生产的基础油质量状况进行了分析，指出润滑油加氢工艺是提高基础油质量的有效途径。加氢工艺生产基础油是润滑油的发展趋势。     

东营凹陷南斜坡储集层成岩作用及对储集性能的影响

东营凹陷南斜坡孔店组岩石类型以岩屑长石砂岩为主 ,长石砂岩和岩屑砂岩次之 ,其中岩屑长石砂岩含量超过 90 %。砂岩成岩作用包括压实作用、胶结作用、溶蚀作用、交代作用等 ,其中胶结作用使储层原生孔隙迅速变差 ,而溶蚀作用是次生空隙发育的主要因素。孔店组砂岩成岩作用进入晚成岩A期 ,期间经历了早成岩A期、B期。影响成岩作用的主要因素为构造演化背景、岩石成分、沉积环境、孔隙流体性质等。     

Measurement of gain spectrum for Fabry-Perot semiconductor lasers by the Fourier transform method with a deconvolution process

To improve the accuracy of measured gain spectra, which is usually limited by the resolution of the optical spectrum analyzer (OSA), a deconvolution process based on the measured spectrum of a narrow linewidth semiconductor laser is applied in the Fourier transform method. The numerical simulation shows that practical gain spectra can be resumed by the Fourier transform method with the deconvolution process. Taking the OSA resolution to be 0.06, 0.1, and 0.2 nm, the gain-reflectivity product spectra with the difference of about 2% are obtained for a 1550-nm semiconductor laser with the cavity length of 720 /spl mu/m. The spectra obtained by the Fourier transform method without the deconvolution process and the Hakki-Paoli method are presented and compared. The simulation also shows that the Fourier transform method has less sensitivity to noise than the Hakki-Paoli method.