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81.
对甲基丙烯酸三氟乙酰氧乙酯(TFAOEMA)的阴离子聚合及原予转移自由基聚合进行了研究。常用的阴离于引发剂如丁基锂、1,1-二苯基已基锂等很难引发TFAOEMA的阴离子聚合,而碱性较弱的引发剂如三乙基铝却容易引发,且产率较高。以氯化亚铜、五甲基二乙基三胺、溴代丙酸乙酯为引发体系的TFAOEMA的本体原子转移自由基聚合符合活性聚合特征。但在四氢呋喃为溶剂的原子转移自由基聚合中却存在活性中心失活现象。以末端含卤素的聚甲基丙烯酸甲酯为大分子引发剂,引发TFAOEMA的原子转移自由基聚合,得到了含氟双嵌段聚合物。  相似文献   
82.
本文介绍了离子束混合工艺方法。与直接注入相比较,离子束混合所使用的设备造价低1/4—1/2,而生产效率可提高1—2个数量级,因而使生产成本大幅度降低,这无疑对离子束工艺的实际应用将产生巨大的促进作用。 通过对轴承材料(GCr15和Cr4Mo4V)经Cr、N、Ta不同元素的混合处理后,在0.5M H_2SO_4和0.1M NaCl的缓冲溶液中的阳极极化曲线表明经混合处理后的两种材料试样,其抗蚀能力和抗点蚀能力均大大提高,这与直接注入的试样效果是一致的。 通过俄歇谱仪和透射电镜的分析结果表明混合是成功的,且在一定的条件下,形成非晶组织。 本文的结论是,无论是离子的直接注入还是离子束混合,对提高轴承材料的抗腐蚀性能都是有效的方法,特别是离子束混合技术具有更大的应用前景。  相似文献   
83.
Using a linear voltage ramp method, ultraslow dielectric relaxation processes of La-doped BaTiO3 boundary layer (BL) capacitors are measured at room temperature. For the electric polarization model of a double-layer dielectric, a procedure to calculate the electrical parameters of grain and grain boundary has been developed. Calculated results suggest that there is a shell on the surface of the grain. TEM images of the BL capacitor also show a lot of microregions with minor structural modifications. Relaxation times are estimated from the equivalent circuit and are in agreement with fitted results.  相似文献   
84.
辛晋秋  李瑞山  莫庆 《铝加工》2003,26(4):11-13,16
本文论述了企业标准化工作的重要性及标准化工作需重视的几个方面。论述了采用国际先进标准及建全标准化管理体系的重要性。  相似文献   
85.
一种可切削玻璃陶瓷的压痕断裂特性   总被引:4,自引:2,他引:2  
将断裂韧性测试的压痕方法与压痕弯曲方法相结合,独立地分离出了压痕残余应力因子x,使其成为可测参量,并建立了压痕一压痕弯曲的断裂韧性测试方法.将这种方法应用于一种可切削玻璃陶瓷的测试,获得的K1c值为K1c=2.03MPa·m1/2,与单边切口法(SENB)获得的K1c值有较好的一致性.测得的残余应力因子X=0.093,符合Anstis经验公式的预测.  相似文献   
86.
A tennis novice watching a match for the first time might be surprised that the crowd erupts with cheers when a player wins one point, then barely applauds when he wins the next. The crowd is not necessarily fickle; some points are genuinely more important than others because a tennis match is hierarchically structured. One match consists of several sets. One set consists of several games. One game consists of several points. The match-winning point is the most important one. How can we make that importance visible? Our goal is to let a fan, a player, or a coach examine tennis data visually, extract the interesting parts, and jump from one item to another quickly and easily. The visualization tool should help parse the elements of a match. We developed an interactive system called TennisViewer to visualize the dynamic, tree-structured data representing a tennis match. It provides an interface for users to quickly explore tennis match information. The visualization tool reveals the overall structure of the match as well as the fine details in a single screen. It uses a 2D display of translucent layers, a design that contains elements of Tree-Maps and of the Visual Scheduler system, which was designed to help faculty and students identify mutually available (transparent) time slots when arranging group meetings. TennisViewer provides MagicLens filters to explore specialized views of the information and a time-varying display to animate all or part of a match  相似文献   
87.
张锦 《光电工程》1996,23(1):53-58
介绍了计算机光学零件图自动绘制软件系统的功能,给出了用该软件完成的光学零件图图样,对程序设计过程中的难点及处理方法也进行了详细阐述。  相似文献   
88.
Prostate development and disease are androgen dependent. However, the nature of hormonal effects on the prostate of healthy young men is not clear. We, therefore, measured prostate size in males chronically exposed to high doses of androgens (AS; habitual anabolic steroid abusers; n = 15) or estrogens (E; male to female transsexuals; n = 11) and compared the results with those in age-matched healthy eugonadal men without known prostate disorders. Prostate size was measured by planimetric ultrasound as cross-sectional areas and maximal dimensions in three orthogonal dimensions with a 7.5-megahertz B-mode sector scanner biplane in a transrectal transducer at 2.5 mm steps from the base to the apex of prostate. Total prostate volume (TPV) was reconstructed from planimetric sections, central prostate volume (CPV) was calculated by the ellipsoidal formula from the appropriate three maximum dimensions, and peripheral prostate volume was determined by the difference between TPV and CPV. Compared with age-matched controls, TPV was normal (-2%) in AS (P = 0.752) and reduced by 31% in E (P = 0.002), whereas CPV was increased by 20% in AS (P = 0.002) and reduced by 46% in E (P = 0.002), and the ratio of CPV/peripheral prostate volume was increased by 77% in AS (P < 0.001) and decreased by 33% in E (P = 0.047). Blood sex hormone-binding globulin was elevated by nearly 500% in E (P < 0.001), but was reduced by 47% in AS (P = 0.003). Prostate-specific antigen was normal (-6%) in AS (P = 0.799) and decreased by 86% in E (P = 0.002). Prostatic acid phosphatase was increased by 26% in AS (P = 0.007), but was unchanged (-28%) in E (P = 0.106). Total and free testosterone levels were reduced to castrate levels in E, whereas LH, FSH, and total testosterone levels were significantly reduced in AS. We conclude that in the human prostate of young men, CPV is more hormonally sensitive than TPV, and during high dose treatment, CPV is preferentially increased by chronic androgen treatment and decreased by chronic estrogen treatment. The reduction of TPV by estrogens was less than expected if solely attributable to inhibition of endogenous gonadotropin and testosterone secretion, suggesting that estrogens also have a positive effect on the normal human prostate. The reversibility and long term significance of androgen-induced stimulation of CPV and, in particular, its relationship to the onset and severity of benign prostatic hyperplasia remain to be clarified.  相似文献   
89.
本文对弹药内弹道性能检验的传统方法存在的问题进行了分析,提出了一种新的检验方法,重点对新的检验方法的数学模型的建立过程进行了论述。并对数学模型的精度进行了分析、检验和验证。  相似文献   
90.
富集孢粉化石的一种方法   总被引:2,自引:0,他引:2  
本论述了孢粉,沟鞭藻化石与矿物颗粒相互分离的方法,并与传统的氢氟酸冷处理方法进行实验对比。结果表明,该方法摒弃有毒重液,提高了化石收获率。  相似文献   
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