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Samarium cobalt films were prepared on silicon substrates with and without a chromium buffer layer at room temperature and 600°C using direct current unbalanced magnetron sputtering. For obtaining ideal magnetic properties, the films should be free from impurities, such as O, Al and others. Rutherford backscattering spectrometry and heavy ion elastic recoil detection analysis were used to determine the composition and film thickness and to monitor the light element contamination across film thickness. X-ray diffractometer and superconducting quantum interference device were employed to characterize the structure and magnetic properties of the films, respectively. The results obtained led to an improved design of the ground shield and the use of a sorption pump to effectively minimize aluminium and oxygen concentration in the films, respectively. 相似文献
54.
Granulomas and cholestatic--hepatocellular injury associated with phenylbutazone. Report of two cases 总被引:1,自引:0,他引:1
A combined cholestatic-hepatocellular injury and noncaseating granulomas occurred in two patients 1 and 4 weeks after phenylbutazone therapy. Both patients were jaundiced, one had a macular rash, and both had peripheral blood eosinophilia. Symptoms and signs subsided, and abnormal findings from tests of hepatic function rapidly returned to normal following withdrawal of the drug. Sections of liver biopsy specimens 6 months later showed no granulomas or other pathologic changes. Previously reported cases are reviewed. 相似文献
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Ankur Sood Varun Arora Jyoti Shah R.K. Kotnala 《Journal of Experimental Nanoscience》2016,11(5):370-382
The current article reports on providing surface modification of magnetic nanoparticles with gold to provide stability against aggregation. Gold-coated magnetite nanoparticles were synthesised to combine both magnetic as well as surface plasma resonance (SPR) properties in a single moiety. The nanocomposites were produced by reduction (using ascorbic acid) of gold chloride on to the surface of iron oxide nanoparticles. Ascorbic acid not only acts as a reducing agent, but also the oxidised form of ascorbic acid i.e. Dehydro-ascorbic acid acts as a capping agent to impart stability to as synthesised gold-coated iron oxide nanocomposites. The synthesised nanocomposite was monodispersed with a mean particle size of around 16 nm and polydispersity index of 0.190. X-ray diffraction analysis confirms presence of gold on the surface of magnetite nanoparticles. The synthesised nanocomposites had a total organic content of around 3.2% w/w and also showed a shifted SPR peak at 546 nm as compared to gold nanoparticles (528 nm). Both uncoated and gold-coated magnetite exhibited superparamagnetic behaviour at room temperature. Upon coating with gold shell, saturation magnetisation of iron oxide nanoparticles decreases from 42.806 to 3.54 emu/gram. 相似文献
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Anil Kumar Mandeep Kaur Rajeev Kumar Pinaki Ranjan Sengupta Vasantha Raman Gopal Bhatia Kedar Nath Sood 《Journal of Materials Science》2010,45(5):1393-1400
Carbon–copper composites with varying copper to carbon ratio of 0.66–1.5 (by weight) were developed from coal-tar-pitch-derived
green coke (as such or modified with natural graphite) as carbon source and electrolytic grade copper powder at different
heat treatment temperatures (HTTs) of 1000–1400 °C. The physical, mechanical, and electrical properties differ depending upon
the HTT and also on copper to carbon ratio (Cu/C). The composites prepared at HTT of 1100 °C having Cu/C ratio of 0.66 and
0.9 exhibited a high bending strength of 150 and 140 MPa, bulk density of 2.63 and 2.81 gm/cm3, electrical resistivity of 1.6 and 0.96 m Ω cm and shore hardness of 88 and 84, respectively, in spite of well-known inadequate
wettability between copper and carbon. Increasing the temperature from 1100 °C for processing of the composites deteriorated
the properties mainly due to the loss of copper through melting above 1100 °C as revealed by X-ray, scanning electron microscopy,
thermal analysis and EDAX studies. 相似文献
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A case-control study, was carried out, which aimed to determine whether a relation exists between risk factors present in mother and the mode of delivery i.e., outcome. Cases were those mothers who had one or more risk factors present during pregnancy (namely, short stature, malpresentation, antepartum haemorrhage, pre-eclamptic toxaemia/eclampsia, anaemia-haemoglobin less than 10 g/dl, twins, bad obstetric history, prolonged pregnancy, history of previous caesarean section and instrumental delivery, pregnancy associated with general diseases, prolonged difficult labour and RH-iso-immunisation). Controls were those mothers who did not have any of the above mentioned risk factors. Total of 250 cases and 250 controls were taken. Results showed that surgical and instrumental deliveries were strongly associated with presence of risk factors (odd's ratio: 5.94; attributable risks: 72%). Out of risk factors among cases, most common indication of caesarean section, was previous caesarean section followed by malpresentation, prolonged difficult labour and short statured mothers in descending order. 相似文献
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AM Hodge RA Westerman MP de Courten GR Collier PZ Zimmet KG Alberti 《Canadian Metallurgical Quarterly》1997,21(1):50-53
We performed a case-control study to investigate the association of the poor metaboliser genotype of the cytochrome P450 2D6 gene with Parkinson's disease (PD). Genotyping was determined by the polymerase chain reaction followed by digestion with restriction enzymes. The poor metaboliser genotype was more frequent in 112 patients with PD than in 206 matched controls (odds ratio 1.7, 95% CI: 0.94-2.45). A meta-analysis of these results together with ten other published studies gave a pooled odds ratio for the poor metaboliser genotype of 1.47 (95% CI: 1.18-1.96, P=0.01). Thus, the poor metaboliser genotype has a small but highly significant association with PD which would be easily missed in small studies. Research now should focus on the mechanism of this association. 相似文献