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11.
Palanisamy GomathiAuthor VitaeMin Kwan KimAuthor Vitae Jung Je ParkAuthor VitaeDhanusuraman RagupathyAuthor Vitae Annamalai RajendranAuthor VitaeSoo Chool LeeAuthor Vitae Jae Chang KimAuthor VitaeSang Hak LeeAuthor Vitae Han Do GhimAuthor Vitae 《Sensors and actuators. B, Chemical》2011,155(2):897-902
Multiwalled carbon nanotubes (MWNTs) grafted chitosan (CS) nanowire (NW) was prepared by phase separation method. Glucose oxidase (GOx) was sequentially immobilized into MWNT-CS-NW to obtain MWNT-CS-NW/GOx biosensor. Field emission scanning electron microscopy (FESEM) images of MWNT-CS-NW/GOx reveals the existence of MWNT and CS. Cyclic voltammetry and amperometry were used to evaluate the electrochemical determination of glucose. The MWNT-CS-NW/GOx biosensor shows an excellent performance for glucose at +0.34 V with a high sensitivity (5.03 μA/mM) and lower response time (3 s) in a wide concentration range of 1-10 mM (correlation coefficient of 0.9988). In addition, MWNT-CS-NW/GOx biosensor possesses better reproducibility, storage stability and there is negligible interference from other electroactive components. 相似文献
12.
Dhineshbabu Nattanmai Raman Karunakaran Gopalu Suriyaprabha Rangaraj Manivasakan Palanisamy Rajendran Venkatachalam 《纳微快报(英文)》2014,6(1):46-54
Nano-Micro Letters - Magnesia (MgO) nanoparticles were produced from magnesite ore (MgCO3) using ball mill. The crystalline size, morphology and specific SSA were characterized by X-ray diffraction... 相似文献
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Engineering components can be subjected to normal and/or rotational fretting wear with contacts that are intermittently exposed to the atmosphere. Exposure to the environment may lead to the alteration at the contact due to the changing role of third body particles such as hard oxides which can result in abrasion. The abrasion due to hard oxide particles differs for the closed contact and intermittently opened contact. In the former scenario, the oxides are compacted into tribo-film, while in the latter case they remain loose, leading to bigger role of abrasion. Standard fretting test setup employed to estimate the fretting wear characteristic operates with a constant load such that the contact remains closed between the counter surfaces and does not simulate the opening and closing of the contacts as observed in certain applications. The forceful interruptions to the experiments to simulate open and close condition of the contact require considerable amount of time and effort. In this paper, an accelerated test procedure is proposed and investigated to capture the effect of intermittent opening of the contact without stopping the experiments. A test rig is designed to simulate the opening and closing conditions, and tests were performed with abrasive diamond-like particles. Friction and wear results are compared with those of intermittently contact opening conditions along with operating wear mechanisms. Scanning electron microscope analysis showed that the wear mechanism observed in the case of fretting with intermittent opening of contact is similar to that of fretting with diamond-like abrasives at the contact. 相似文献
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Lavanya Thirugnanam Manikandan Palanisamy Satheesh Kaveri Sundara Ramaprabhu Vilas G. Pol Mrinal Dutta 《International Journal of Hydrogen Energy》2021,46(2):2464-2478
TiO2 nanoparticles decorated nitrogen (N) doped helical carbon nanofiber (CNF)-carbon nanotube (CNT) hybrid material is prepared by low-cost electrospinning technique followed by hydrothermal method. Morphological investigations establish helical structure of CNFs with hierarchical growth of CNTs around CNFs. The hybrid material shows a high specific surface area of 295.17 m2 g?1 with nanoporous structure. X-ray photoelectron spectroscopic studies establish Ti–O–C/Ti–C bond mediated charge transfer channel between TiO2 nanoparticles and carbon structures with the success of N doping in CNFs. The electrospun hybrid material delivered high reversible charge capacities of 316 mAh g?1 (100th cycle) and 244 mAh g?1 (100th cycle) at a current density of 75 mA g?1 and 186 mA g?1 respectively. The charge capacities obtained for different applied current densities are higher than the conventional graphitic microporous microbeads anode. Results indicate that the hybrid material reported here shows high performance compare to graphite for LIBs. 相似文献
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M. Gopiraman C. Sathya S. Vivekananthan D. Kesavan N. Sulochana 《Journal of Materials Engineering and Performance》2012,21(2):240-246
The inhibition effect of 2,3-dihydroxyflavone on the corrosion of mild steel in 100-600 ppm aqueous hydrochloric acid solution
has been investigated by weight loss and electrochemical impedance spectroscopy. The corrosion inhibition efficiency increases
with increasing concentration and time. The effect of temperature on the corrosion behavior of mild steel in 1 M HCl with
addition of inhibitor was studied at the temperature range of 300-330 K. UV-Vis, FTIR, and surface analysis (SEM) was also
carried out to establish the corrosion inhibitive property of this inhibitor in HCl solution. The adsorption of this inhibitor
on the mild steel surface obeys the Langmuir adsorption isotherm. Electrochemical studies reveal that the inhibitor is a cathodic
type. 相似文献
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The usage of hybrid natural composites has surged in almost all fields of engineering due to their advantage of possessing high strength to weight ratio and biodegradability. This paper deals with the fabrication and investigation of mechanical and thermal properties of banana-kenaf glass fiber reinforced epoxy composite which is relatively a newer hybrid composite. In this study, the composite is fabricated by a hand layup process with different fiber orientations and also with different volume fractions. The composites are prepared with five different proportions of banana-kenaf fibers. Various mechanical and thermal tests are conducted and the result shows that the hybrid composite in which fibers are arranged at 450 inclination has better properties than the others. Also, failure morphology analysis is done using a Scanning Electron Microscope (SEM) through which the internal structures of the tested specimen are analysed. 相似文献
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Jana S. Kesavan Jerold R. Bottiger Deborah R. Schepers Andrew R. McFarland 《Aerosol science and technology》2014,48(2):219-227
Aerodynamic particle sizer (APS) users typically calibrate the particle sizing capabilities, but not the counting efficiency upon which aerosol concentration results are based. Herein, comparisons were made between the counts provided by an ink jet aerosol generator (IJAG) with those measured by an APS. Near-monodisperse (geometric standard deviation of about 1.06) liquid or solid aerosols in the size range of 0.95 to 13.3 μm aerodynamic diameter (AD) generated with an IJAG were released into the inner inlet-tube of the APS in a manner that rendered APS wall and aspiration losses negligible. For most experiments, the IJAG generated 75 particles/s, which rate was maintained by the IJAG system through control of electrical pulses applied to its ink jet cartridge. For particles in the size range of 2–13.3 μm AD, the ratio of relative detection efficiency (ratio of the number of particles counted by the APS to the number reported as generated by the IJAG) was 99.3 ± 1.4%; however, for test particles between 0.95 and 2 μm AD, the relative detection efficiency was somewhat lower, but the drop off was less than about 2%. This slight drop off is likely associated with the light scattering detection approach and corresponding counting algorithm of the APS. Tests were conducted where the IJAG produced 7.0 μm AD particles at rates of 1 to 500 s-1 and the results showed essentially a 1:1 correspondence between IJAG and APS counts. The presence of smaller-sized background particles did not affect the measured APS counts of larger-sized challenge particles.
Copyright 2014 American Association for Aerosol Research 相似文献