星型聚合物中间体环硅氧烷核的合成研究

以甲基二氯硅烷、四甲基四乙烯基环四硅氧烷(DVi4)为原料,采用硅氢加成反应合成了星型聚合物的中问体环硅氧烷核,并用红外光谱和核磁共振谱进行了表征.反应的最佳条件是:采用预先活化、反应温度72℃、催化荆与DVi4的量之比为1.0×10-4,反应转化率可达95%,且选择性很好,产物主要为β-加成产物.     

浅谈在线配粉条件下专用粉质量控制

浅述了在线配粉条件下,通过严格生产管理及改良剂应用等相关措施,控制好专用粉质量的措施.包括落实ISO质量管理体系,加强原料的质量控制和预粉、粉路的测定,生产过程中要注意小麦清理与着水、生产设备和现场管理、员工的技术水平因素等.     

基于资源流分析的企业生态补偿机制研究

循环经济作为一种新型的经济范式,成为理论界和实业界共同关注的焦点问题.在循环经济模式下引入了投入产出的资源流管理模型,该模型反映各个过程中资源流的流向和流量,为建立生态补偿机制提供了详细的基础数据,并利用外部环境的完善,推动生态补偿机制在微观领域的实施,从而达到改善企业环境绩效,减少环境污染的目的.     

选煤厂跳汰工艺改造实践

针对选煤厂原有跳汰机技术落后、精煤捞坑跑粗及高灰细泥污染精煤等关键问题,采用SKT高效现代化跳汰机替换原有跳汰机,并用振动弧形筛回收粗煤泥的改造方案;实践证明,改造取得了良好效果。     

龙滩水电站尾水调压井桥机拆除

龙滩水电站尾水调压井施工桥机在完成其施工吊装使命后需要拆除，为保证其完好率，需采取无破坏法整机拆除。介绍了在狭小空间大型设备的整机拆除方法和天锚系统的设计、布局。     

Ultrasonic thin-walled tube wave structure for sensing devices

Theoretical and experimental investigations of thin-walled tube acoustic wave devices for gravimetric sensing applications are presented. Integrated sensor configurations have been demonstrated by employing a sol-gel processed thin piezoelectric lead zirconate titanate (PZT) film. This was coated coaxially on stainless steel tubes and interdigital transducers (IDT) fabricated as the transmitter and receiver on the curved tube surfaces. We have observed tube waves along both the axial and circumferential directions between 1 and 6.6 MHz. We have also analyzed the mass sensitivities of different modes propagating along the tubes and shown that high mass sensitivity can be achieved by keeping the tube wall thin     

Cast bulk ZrTiAlCuNi amorphous alloys

Cylindrical bulk amorphous samples with diameters up to 10 mm have been prepared by casting ZrTiAlCuNi alloys in a copper mould. In order to rank glass-forming ability as a function of alloy composition, alloys were also cast into wedge-shaped moulds; to a first approximation, the thickness of the amorphous region obtained can be taken as an indication of glass-forming ability. The compositions which lead to the production of bulk glasses all have reduced glass transition temperatures in excess of 0.65 and the extremely high glass-forming ability of these compositions is discussed. We suggest that both the Al and Ti contents are determining factors for the production of bulk amorphous samples and these are believed to reduce the driving force for, and hence the rate of, crystallisation. These amorphous alloys have been found to display high thermal stability and can be annealed for several minutes in the supercooled liquid region. They are ductile at room temperature and have a high value of yield stress.