In-Situ observation on microfracture behavior ahead of the crack tip in 63Sn37Pb solder alloy

in-situ transmission electron microscopy (TEM) tensile tests on as-cast and aged 63Sn37Pb solder alloys were conducted, and the fracture behavior in nanometer scale ahead of the crack tip was inspected and discussed. Results show that the fracture was completed by connecting the discontinuous cracks or voids. Dislocation behavior was concentrated along the grain boundaries for as-cast samples, and displayed mainly as dislocation climb. The crack was intergranular dominated under the lower strain rate. While remarkable mutual dislocation emission was detected in the aged solder. Transgranular cracks were dominant in the fractured area, and they propagated by linking up with the nanometer scale cracks ahead of the crack tips under the effective promotion of the inverse dislocation emission. At the same time, the partial interphase or intergranular cracks in the thinned area were also found. Under this condition, a new critical stress intensity factor K _c ^′ to define the mutual dislocation emission was proposed.     

基于FLUENT软件的管式搅拌反应器流场的数值模拟

运用商业计算流体力学(CFD)软件FLUENT对一种新型管式搅拌反应器进行流场模拟,用GAMBIT建立流场实体模型,采用标准k-ε湍流模型以及多重参考系法(MRF)处理搅拌桨区.结果表明,计算所选模型能较准确地预测搅拌反应器的速度场、压力场及湍流动能分布,考察流量为1 m3/h时不同搅拌转速对反应器内部混合的影响,此时对应的最佳搅拌转速为50 rpm左右.模拟结果将为实验研究提供适当的操作参数,对搅拌反应器的优化和放大具有一定参考价值.     

印染废水处理工艺研究及实例

本文简要介绍了印染废水水质特征,提出了处理工艺,并利用两个工程实例说明了该工艺的可行性.     

PTA压力离心机转子的改造

介绍了PTA压力离心机的主要性能参数、工作原理、分离效果的影响因素。为了增大沉渣在过渡区及脱水区滞留的时问，同时为达到在过渡区及脱水区对沉渣加入纯净水进行再冲洗的目的，对螺旋送料转子、挡液环、进料管进行了改造。改造后，沉渣在脱水区的停留时间由0．44a增至0．72s，2．5～3t／h的冲洗水对脱水区的沉渣进行冲洗效果较好。产品中的杂质质量分数较改造前减少15％，产品优等品率提高到99％。     

Ionothermal synthesis of a three-dimensional zinc phosphate with DFT topology using unstable deep-eutectic solvent as template-delivery agent

A three-dimensional zinc phosphate compound with DFT topology, designated as ZnPO₄-EU1, has been synthesized by an ionothermal approach from the system HF-ZnO–P₂O₅-choline chloride-imidazolidone. Ethylenediamine, derived from decomposition of the imidazolidone component of the deep-eutectic solvent (DES) itself, is delivered to the synthesis and serves as an appropriate template for ZnPO₄-EU1. Experiments in which the synthesis conditions were varied showed that ZnPO₄-EU1 may be prepared over a wide molar ratio of P/Zn = 0.55–13.0. Powder X-ray diffraction patterns have been obtained at intervals to track the crystallization process of this material. The experimental data show that Zn₃(PO₄)₂ · 4H₂O (a dense phase) was first isolated from the DES after reaction for 1 h. Subsequently, the pure phase of ZnPO₄-EU1 was obtained with increasing crystallization time from 12 h to 72 h. The experimental results show that the nucleation and crystallization take place with relatively low levels of solvent degradation, demonstrating that zinc phosphate with a three-dimensional framework can be synthesized by in situ generation of an appropriate template using an unstable DES at high temperatures (150–200 °C).     

C语言学习方法与实践的探讨

针对C语言程序设计课程本身的特点，分析学习过程中存在的问题，强调实践的必要性。结合一些学校课程改革和实践的经验．提出面向应用的，科学的学习内容、方法和模式。同时提高学习者的专业动手能力。     

装配式基坑支护结构在广州地区的应用

装配式基坑支护结构是将基坑支护的围护结构部分在工厂预制成型,再在现场与撑或锚装配组成的支护结构。工程实践表明,此项技术可有效节省工程投资、缩短工期。     

裂齿矩形翅片板翅式换热器优化设计的分析

对裂齿矩形翅片板翅式换热器中的裂齿矩形翅片的传热效率作了分析,并以单位质量材耗的换热能力最大为目标函数,分析研究了在不同雷诺数(Re)的操作条件下裂齿矩形翅片间角度、翅片厚、长度、宽度及极厚之间的关系。结果表明:在气体换热的场合下,当Re在某一范围时翅片可有效地起到强化传热的作用。当板厚为5mm,翅片厚为3mm,翅片间夹角为45°～70°,Re为2×10~3～8×10~3,最佳翅片纵向间距与翅片长度和翅片厚度乘积的平方根的比为1.5～2.5,最佳翅片尺寸系数为3～5时,传热强化效果较好。     

计算机文化基础课程建设的探索与实践

"计算机文化基础"课程是面向非计算机专业大学生的公共基础课.它既是文化基础、公共基础、又是技术基础,并具有很强的应用性和工具性.它要完成的任务是:使学生掌握计算机软、硬件技术的基础知识,培养学生在本专业与相关领域中的计算机应用、开发能力,以及利用计算机分析问题、解决问题的意识.