相转移催化合成癸二酸二甲酯

使用相转移催化剂BTEAC(氯化三乙基苄胺 )合成癸二酸二甲酯。条件为 :10g癸二酸 ,80mL甲醇 ,0 .5mL硫酸 ( 98% )和 0 .0 5gBTEAC。癸二酸二甲酯产率达到 90 .4 %     

光化学反应中的磁场效应 Ⅱ.电子转移光敏化1,2-二苯乙烯的顺反异构化反应

前文报道了外加磁场对吸附在硅胶表面上的芳砜光解反应的影响,本文报道外加磁场影响光化学反应的另一个例子——电子转移光敏化1,2-二苯乙烯的异构化。 近年来电子转移光敏化反应引起了有机光化学家们的极大注意。一些异构化、重排、裂解、氧化反应都可以通过电子转移机理敏化。电子转移光敏化的机理可以用(1)描述。图中A和D分别代表电子的受体和给体。     

基于不完全信道信息的D2D功率分配算法

针对蜂窝与终端直通(Device-to-device,D2D)混合网络中的不完全信道状态信息(Channel state information,CSI),提出了一种基于不完全CSI的最优功率分配算法。利用拉格朗日乘数法推导出了最优功率分配解的闭式表达式。相对于传统的最大发送功率分配方案,该最优解受信道信息误差的影响较小,具有较好的鲁棒性。仿真结果表明,本文算法可以节约发送功率,并得到更大的接收信噪比。     

企业创新积累不足对温州产业升级的影响与启示

分析了在经济高速发展的2000-2009年10年间,温州企业和产业在创新资金、技术和人才等方面的投入情况.结果显示:除了正泰等少数企业外,温州多数企业没有为转型升级做好技术、人才和观念上的准备,企业家群体转型升级意识落后,企业创新能力提升缓慢.温州案例说明:企业建立基于创新的新竞争优势是一个长期过程,必须未雨绸缪,持续投入.在这一过程中,政府可以通过支持企业家学习和培训、提高标准和加强监管等措施促进产品质量提升,以及在加快改革以消除不合理暴利空间等方面发挥积极作用.     

电控柴油机分缸均衡控制算法及试验

柴油机各个气缸的进气量、喷油量、燃烧等存在差异,导致气缸间存在做功差异,直接影响柴油机转速的平稳性以及排放性能等。针对位置式电控柴油机,采用PI闭环控制,通过瞬时转速信号识别并计算各缸的工作差异,利用分缸均衡控制算法对油量进行补偿修正。试验结果显示低转速稳态工况转速波动由7 r/min降至3 r/min,各缸工作不均匀度由±5 r/min降至±2 r/min,在瞬态过程和高转速3 400 r/min时该算法仍然适用有效。     

从女性主义角度浅析《傲慢与偏见》两译本

从女性主义的角度对简·奥斯丁的作品《傲慢与偏见》的两个中文译本——孙致礼和张玲、张扬的译本进行比较。分析女性主义意识对翻译过程以及最终译本的影响。     

Robust lane recognition for structured road based on monocular vision

A robust lane detection and tracking system based on monocular vision is presented in this paper.First,the lane detection algorithm can transform raw images into top view images by inverse perspective mapping(IPM),and detect both inner sides of the lane accurately from the top view images.Then the system will turn to lane tracking procedures to extract the lane according to the information of last frame.If it fails to track the lane,lane detection will be triggered again until the true lane is found.In this system,θ-oriented Hough transform is applied to extract candidate lane markers,and a geometrical analysis of the lane candidates is proposed to remove the outliers.Additionally,vanishing point and region of interest(ROI)dynamically planning are used to enhance the accuracy and efficiency.The system was tested under various road conditions,and the result turned out to be robust and reliable.     

Oxidation Performance of Fe-Al/WC Composite Coatings Produced by High Velocity Arc Sprayed at 650 ℃

Fe-Al intermetallics with remarkable high-temperatureintensity and excellent erosion,high-temperatureoxidation and sulfuration resistance are potential lowcost high-temperature structural material.ProducingFe-Al/WC composite coating by high velocity arcspraying(HVAS)on structural materials would notonly obviate the problems faced in fabrication of thesealloys into useful shapes,but also allow the effectiveuse of their outstanding high-temperature performance,which might thus promisingly mak…     

不锈钢GTAW焊焊接中的氧化试验研究

对于不锈钢的焊接，在NDT检测中仅对夹渣、未熔合、未焊透、气孔等缺陷均有评定标准，而对菜花状缺陷、树瘤状氧化缺陷、蓝脆现象、氧化现象等却没有评定方法及标准。为此，以不锈钢管的焊接试验为主鲒合不锈钢板的焊接，针对不锈钢在GTAW焊焊接中氧化缺陷的防止方法、氧化评定及检测标准提出几点看法，供行业界借鉴与批评指证。     

Formation and thermal stability of amorphous Ni-Mo-P alloys

The experimental researches on the chemical deposition of Ni-Mo-P amorphous alloys were carried out by adding Na2 MoO4 into acidic solutions. The optimum technology conditions were obtained by orthogonal design experiments. The structures and the relationship between compositions and their thermal stability were studied by energy spectrum (EC), scanning electron micrograph and X-ray diffraction spectrum. Compared with Ni-P amorphous alloys, the Ni-Mo-P amorphous alloys have high crystallization temperature and thermal stability, and the hardness reaches its peak when the annealing temperature is 500 ℃. With the increase of the heat treatment temperature, the surface morphology of the alloys changes.