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51.
Paola Fabbri Massimo Messori Monica Montecchi Francesco Pilati Rosa Taurino Claudio Tonelli Maurizio Toselli 《应用聚合物科学杂志》2006,102(2):1483-1488
A commercial perfluoropolyether containing alkoxysilane functionalities was employed to prepare organic–inorganic hybrid coatings by using the sol‐gel process in the presence of tetraethoxysilane. Contact angle analysis revealed a strong hydrophobic and oleophobic character of the coatings almost independently from the molecular weight of the starting fluorinated oligomer. Surface tension values were in the range of 14–16 mN/m, suggesting a preferential segregation of fluorinated segments onto the surface of the coating. Atomic force microscopy showed the presence very smooth surfaces permitting to neglect the contribution of the surface roughness to wettability. Friction coefficient values were markedly lower with respect to the value of uncoated glass substrate. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 1483–1488, 2006 相似文献
52.
Summary New types of comb-shaped polyesters have been prepared by transesterification of 2,2-dioctadecyl-1,3-propanediol and the three isomeric diphenyl phthalates. Intrinsic viscosity and SEC analyses allowed determination of DPs (60–89) and molar masses; results compare well with absolute average weight molar masses (56,000–118,000) determined by low-angle laser light scattering. High-resolution 13C NMR reveals the characteristic aromatic and glycol polyester patterns; it resolves many side-chain methylene carbons, but shows no evidence of end-groups. All the polyesters are crystalline as shown by X-ray diffractometry and DSC, the crystallinity being exclusively due to the octadecyl side-group crystallization in the hexagonal form. The results indicate that the crystallinity decreases substantially when going from the ortho- to the terephthalate polyester. 相似文献
53.
The vulcanization of natural rubber was studied with the sulfurating agents dipentamethylene thiuram tetrasulfide (DPTT) and tetramethylene thiuram disulfide (TMTD) in the presence of tetramethyl thiuram monosulfide (TMTM). This last accelerant affects the rate and efficiency of the vulcanization as well as the structures of crosslinks formed by the two sulphur donors. It may give rise to a polymerization between adjacent double bonds and generate a inhomogeneous crosslink distribution with an adverse effect on physical properties. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 491–499, 2002 相似文献
54.
Guadalupe Del C. Pizarro Oscar G. Marambio Manuel Jeria O Margarita Huerta Bernab L. Rivas 《应用聚合物科学杂志》2006,100(1):178-185
The free‐radical copolymerization of water‐soluble poly(1‐vinyl‐2‐pyrrolidone‐co‐hydroxyethylmethacrylate) was carried out with a feed monomer ratio of 75:25 mol %, and the total monomer concentration was 2.67M. The synthesis of the copolymer was carried out in dioxane at 70°C with benzoyl peroxide as the initiator. The copolymer composition was obtained with elemental analysis and 1H‐NMR spectroscopy. The water‐soluble polymer was characterized with elemental analysis, Fourier transform infrared, 1H‐ and 13C‐NMR spectroscopy, and thermal analysis. Additionally, viscosimetric measurements of the copolymer were performed. The thermal behavior of the copolymer and its complexes were investigated with differential scanning calorimetry (DSC) and thermogravimetry techniques under a nitrogen atmosphere. The copolymer showed high thermal stability and a glass transition in the DSC curves. The separation of various metal ions by the water‐soluble poly(1‐vinyl‐2‐pyrrolidone‐co‐hydroxyethylmethacrylate) reagent in the aqueous phase with liquid‐phase polymer‐based retention was investigated. The method was based on the retention of inorganic ions by this polymer in a membrane filtration cell and subsequent separation of low‐molar‐mass species from the polymer/metal‐ion complex formed. Poly(1‐vinyl‐2‐pyrrolidone‐co‐hydroxyethylmethacrylate) could bind metal ions such as Cr(III), Co(II), Zn(II), Ni(II), Cu(II), Cd(II), and Fe(III) in aqueous solutions at pHs 3, 5, and 7. The retention percentage for all the metal ions in the polymer was increased at pH 7, at which the maximum retention capacity could be observed. The interaction of inorganic ions with the hydrophilic polymer was determined as a function of the pH and filtration factor. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 178–185, 2006 相似文献
55.
Bonaventura Focher Annamaria Marzetti Cataldo Santoro Virginio Sarto Luigi D'Angiuro 《大分子材料与工程》1982,102(1):187-197
Textile cotton wastes were irradiated with γ-rays at different doses and solubilized with 10% NaOH solutions. The regenerated products underwent enzymatic hydrolysis and their degradation pattern was compared with that of the cotton celluloses untreated or treated only with γ-rays. The different samples were characterized by measurements of X-ray diffraction, degree of polymerization, moisture regain and water retention. The structural and morphological modifications induced by the pretreatments were correlated with the variations of kinetic parameters, particularly the Vmax/Km ratio, defined as specificity constant. Only the combination of irradiation with dissolution pretreatments gave a considerable increase of hydrolysis reaction effectiveness. 相似文献
56.
Claudio Baecchi Tiberio Uricchio Marco Bertini Alberto Del Bimbo 《Multimedia Tools and Applications》2016,75(5):2507-2525
In this paper we investigate the use of a multimodal feature learning approach, using neural network based models such as Skip-gram and Denoising Autoencoders, to address sentiment analysis of micro-blogging content, such as Twitter short messages, that are composed by a short text and, possibly, an image. The approach used in this work is motivated by the recent advances in: i) training language models based on neural networks that have proved to be extremely efficient when dealing with web-scale text corpora, and have shown very good performances when dealing with syntactic and semantic word similarities; ii) unsupervised learning, with neural networks, of robust visual features, that are recoverable from partial observations that may be due to occlusions or noisy and heavily modified images. We propose a novel architecture that incorporates these neural networks, testing it on several standard Twitter datasets, and showing that the approach is efficient and obtains good classification results. 相似文献
57.
Most of the literature on innovation management highlights the fundamental role played by people in the innovation process and the need to fully develop the creative and innovative potential of organizations' members. This article offers the result of extensive research carried out among some of the most innovative companies in the Basque Country, a highly innovative region located in the north of Spain. It draws interesting conclusions about how these innovative companies combine strong leadership, human resource practices, and an organizational culture that enhances innovation capabilities among the company's employees. More specifically, it answers questions such as the following: Are human resources policies, leadership, and innovation culture implemented equally in Basque innovative companies? Do companies make the same effort in deploying these elements or routines and practices related to them? Can we see a pattern in the use of these elements among innovative firms? © 2012 Wiley Periodicals, Inc. 相似文献
58.
Arregui-Dalmases C Del Pozo E Stacey S Kindig M Lessley D Lopez-Valdes F Forman J Kent R 《Proceedings of the Institution of Mechanical Engineers. Part H, Journal of engineering in medicine》2011,225(7):688-695
While rupture of the aorta is a leading cause of sudden death following motor vehicle crashes, the specific mechanism that causes this injury is not currently well understood. Aortic ruptures occurring in the field are likely due to a complex combination of contributing factors such as acceleration, compression of the chest, and increased pressure within the aorta. The objective of the current study was to investigate one of these factors in more detail than has been done previously; specifically, to investigate the in situ intra-aortic pressure generated during isolated belt loading to the abdomen. Ten juvenile swine were subjected to dynamic belt loads applied to the abdomen. Intraaortic pressure was measured at multiple locations to assess the magnitude and propagation of the resulting blood pressure wave. The greatest average peak pressure (113.6 +/- 43.5 kPa) was measured in the abdominal aorta. Pressures measured in the thoracic aorta and aortic arch were 70 per cent and 50 per cent, respectively, that measured in the abdominal aorta. No macroscopic aortic trauma was observed. To the authors' knowledge the present study is the first one to document the presence, propagation, and attenuation of a transient pressure wave in the aorta generated by abdominal belt loading. The superiorly moving wave is sufficient to generate hydrostatic and intimal shear stress in the aorta, possibly contributing to the hypothesized mechanisms of traumatic aortic rupture. 相似文献
59.
Abstract. In this paper two problems on the class of k -trees, a subclass of the class of chordal graphs, are considered: the fast reordering problem and the isomorphism problem. An O(log
2
n) time parallel algorithm for the fast reordering problem is described that uses O(nk(n-k)/\kern -1ptlog n) processors on a CRCW PRAM proving membership in the class NC for fixed k . An O(nk(k+1)!) time sequential algorithm for the isomorphism problem is obtained representing an improvement over the O(n
2
k(k+1)!) algorithm of Sekharan (the second author) [10]. A parallel version of this sequential algorithm is presented that runs in
O(log
2
n) time using O((nk((k+1)!+n-k))/log n) processors improving on a parallel algorithm of Sekharan for the isomorphism problem [10]. Both the sequential and parallel
algorithms use a concept introduced in this paper called the kernel of a k -tree. 相似文献
60.
Antonio Coronato Massimo Esposito Giuseppe De Pietro 《Personal and Ubiquitous Computing》2009,13(7):527-538
This paper presents semantic models, mechanisms and a service to locate mobile entities in Smart and Intelligent Environments. The key feature of the service is the semantic integration of different positioning systems that not only enables the environment to handle transparently such physical positioning systems, but also to reason on location information coming from different systems and to combine it to obtain higher context information. Indeed, the service relies on the use of ontologies and rules to define a uniform, unambiguous and well-defined model for the location information, independently of the particular positioning system. Moreover, the location service performs logic and reasoning mechanisms to provide both physical and semantic locations of mobile objects and to infer the finest granularity in the case when a mobile object is located by more than one positioning system. Finally, we present an application of the proposed approach to the case of a Smart Hospital. 相似文献