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41.
Ternary oxide mixtures of lime, alumina, and silica were premelted and quenched to produce glassy cylinders. A diffusion couple was selected from the mixtures of six different compositions in such a way that the average composition could be 40 wt pct CaO-20 wt pct A12O3 = 40 wt pct SiO2. Penetration curves of the components were measured with a X-ray microprobe analyzer. The interdiffusivities matrix defined with the Matano interface has been obtained from 52 successful diffusion runs at 1723 K to 1823 K as follows; 1 $$\begin{gathered} \tilde D_{10 - 10}^{30} = 8.9 \times 10^{ - 11} \exp ( - \frac{{253,700}}{{RT}})(m^2 /s) \hfill \\ \tilde D_{10 - 20}^{30} = - 2.5 \times 10^{ - 11} \exp ( - \frac{{194,300}}{{RT}})(m^2 /s) \hfill \\ \end{gathered} $$ 2 $$\begin{gathered} \tilde D_{20 - 10}^{30} = - 4.0 \times 10^{ - 11} \exp ( - \frac{{177,600}}{{RT}})(m^2 /s) \hfill \\ \tilde D_{20 - 20}^{30} = 6.12 \times 10^{ - 11} \exp ( - \frac{{318,400}}{{RT}})(m^2 /s) \hfill \\ \end{gathered} $$ where symbols, 10, 20, and 30 mean CaO, A12O3, and SiO2, respectively, and the activation energies are in Joules per mole. The diffusion composition paths obtained are discussed in relation to Cooper’s parallelogram. The composition dependency of the above interdiffusivities is estimated from the quasibinary interdiffusivities in all composition ranges of the present oxide system in liquid state. 相似文献
42.
43.
T. Goto N. Wakamatsu H. Kamemizu M. Iijima Y. Doi Y. Moriwaki 《Journal of materials science. Materials in medicine》1991,2(3):149-152
The sintering mechanism of hydroxyapatite (HAp) by addition of lithium phosphate (Li3PO4) has been investigated. Using the X-ray diffraction method, HAp was confirmed to decompose into -Ca3(PO4)2 (-TCP) by addition of Li3PO4. The measurement of shrinkage rate by the isothermal firing made it clear that the densification process at the initial stage of sintering took place in the presence of liquid phase. Furthermore, the examination of the phase diagram on the binary system -TCP-Li3PO4 revealed that there was an eutectic point at 1010°C in the composition of 60 wt% Li3PO4. From these evidences, we concluded that -TCP produced by the decomposition of a part of HAp has formed the liquid phase by reacting with Li3PO4 above 1010°C, and that this liquid phase has largely promoted the densification by the rearrangement of HAp particles at the initial stage of sintering. 相似文献
44.
Allinson M Kageyama S Nakajima D Kamata R Shiraishi F Goto S Salzman SA Allinson G 《Water science and technology》2012,66(4):768-774
In 2007, samples of treated effluent were collected at point of discharge to the environment from 39 wastewater treatment plants (WWTPs) located across Victoria, Australia grouped by treatment type. Sample genotoxicity was assessed with a high-throughput luminescent umu test method using Salmonella typhimurium TL210 strain, with and without addition of a commercially available metabolic activation system. Samples were also screened using a gas chromatographic-mass spectrometric mass-structure database recognition method. A genotoxic response was observed in half of the samples tested without metabolic activation system (相似文献
45.
Hydrothermal vapor treatment method was applied for preparation of ceramic biomaterials. Hydroxyapatite (Ca10(PO4)6(OH)2; HA) ceramics prepared by sintering with random crystal surface have already been used as bone-repairing materials which
can directly bond to natural bones. If materials of HA could have the tailored specific crystal surface, they should have
the advantage of adsorptive activity and osteoconductivity in comparison with the sintered HA. In the present study, porous
HA sheets of about 50 μm to 1 mm in thickness and porous HA granules of about 50 μm to 1 mm in size with tailored crystal
surface were prepared by the hydrothermal vapor exposure method at temperatures below 200°C. Porous sheets and porous granules
of HA with controlled crystal surface should be suitable for scaffold of cultured bone, for bone graft material and for drug
delivery system (DDS). 相似文献
46.
Toshihiko Hirama Masashi Goto Keiji Shiba Toshio Kobayashi Ryozo Tanaka Shizuo Tsurumaki Katsuki Takiguchi Hiroshi Akiyama 《Nuclear Engineering and Design》2005,235(13):7
A 1/8-scale model was constructed of a reinforced concrete containment vessel (RCCV) used in the latest advanced boiling water reactors (ABWR). Shaking table tests were conducted on it with input motions corresponding to or exceeding a design earthquake assumed for a real Nuclear Power Plant.The objectives of the tests were to verify the structural integrity and the leak-proof functional soundness of the RCCV subjected to design earthquakes, and to determine the ultimate strength and seismic margin by an excitation that led to the model's collapse. The model, the test sequence and the pressure and leak test results were addressed in Part 1. The shaking table test method, the input motions and the test results, including the transition of the model's stiffness, natural frequencies and damping factors and the effects of vertical input motions and internal pressure on the model's characteristics and behavior, the load–deformation, the ultimate strength, the failure mode of the reinforced concrete portion and the liner plate are described here. The seismic safety margin that was evaluated by the energy input during the failure test to a design basis earthquake will be described in Part 3. The analytical results of simulation using the multi-lumped mass model will be described in Part 4. 相似文献
47.
NA Pablant M Bitter L Delgado-Aparicio M Goto KW Hill S Lazerson S Morita AL Roquemore D Gates D Monticello H Nielson A Reiman M Reinke JE Rice H Yamada 《The Review of scientific instruments》2012,83(8):083506
First results of ion and electron temperature profile measurements from the x-ray imaging crystal spectrometer (XICS) diagnostic on the Large Helical Device (LHD) are presented. This diagnostic system has been operational since the beginning of the 2011 LHD experimental campaign and is the first application of the XICS diagnostic technique to helical plasma geometry. The XICS diagnostic provides measurements of ion and electron temperature profiles in LHD with a spatial resolution of 2 cm and a maximum time resolution of 5 ms (typically 20 ms). Ion temperature profiles from the XICS diagnostic are possible under conditions where charge exchange recombination spectroscopy (CXRS) is not possible (high density) or is perturbative to the plasma (low density or radio frequency heated plasmas). Measurements are made by using a spherically bent crystal to provide a spectrally resolved 1D image of the plasma from line integrated emission of helium-like Ar(16 +). The final hardware design and configuration are detailed along with the calibration procedures. Line-integrated ion and electron temperature measurements are presented, and the measurement accuracy is discussed. Finally central temperature measurements from the XICS system are compared to measurements from the Thomson scattering and CXRS systems, showing excellent agreement. 相似文献
48.
Void-free β-SiC films were deposited on Si(001) substrates by laser chemical vapor deposition using hexamethyldisilane (HMDS) as the precursor. The effect of the time of introducing HMDS, i e, the substrate temperature when HMDS introduced (Tin), on the preferred orientation, surface microstructure and void was investigated. The orientation of the deposited SiC films changed from <001> to random to <111> with increasing Tin. The surface showed a layer-by-layer microstructure with voids above Tin ? 773 K, and then transformed into mosaic structure without voids at Tin= 298 K. The mechanism of the elimination of voids was discussed. At Tin =298 K, Si surface can be covered by an ultrathin SiC film, which inhibits the out-diffusion of Si atoms from substrate and prohibites the formation of the voids. 相似文献
49.
50.
Hiroo Hasebe Hiromichi Ryuto Nobuhisa Fukunishi Akira Goto Masayuki Kase Yasushige Yano 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》2008,590(1-3):13
The problem of handling the fragile carbon foils (mounting on the frame, placing in the stripper changer) that easily break when self-supporting has been solved by coating carbon foils with poly-monochloro-para-xylylene. It was found that the polymer-coating method could also be used to produce carbon foils thicker than 100 μg/cm2 by alternated deposition of carbon and poly-monochloro-para-xylylene layers. Carbon foil of 500 μg/cm2 thick and 10 cm in diameter was produced by this method and mounted to a foil holder. Results of lifetime measurement for singly coated foils are also presented. 相似文献