有减水作用的新型高效陶瓷助磨剂研制

利用曼尼奇反应原理 ,制备了多胺基磷酸钠陶瓷助磨剂 ,采用红外光谱、差热分析等对合成的助剂进行了表征 ;此外 ,通过对氧化铁以及石英滑石等原料的助磨应用测试表明 :合成的助剂是一种高效陶瓷助磨剂 ,同时还具有减水作用。     

高岭土改性聚酯纤维

介绍了高岭土在改性聚酯中的作用、纤维级高岭土的性质以及改性聚酯的制造方法．指出了我国开发高岭土改性聚酯纤维的的前景．     

聚氨酯防水涂料及其市场发展概况

聚氨酯防水涂料是当今最有效的柔性防水材料之一，介绍了聚氨酯防水涂料的发展状况，并对其市场前景进行了展望。     

分光光度法测定锌铁合金镀层及镀液中的铁

采用分光光度法，以磺基水杨酸为显色剂、双氧水为氧化剂，锌铁合金镀层用稀盐酸溶解，控制pH值为1.5～3，在等吸收点处测定吸光度，并根据比耳定律计算镀层及镀液中的铁含量。     

Medium-Term Hydro Generation Scheduling (MTHGS) with Chance Constrained Model (CCM) and Dynamic Control Model (DCM)

Medium-Term Hydro Generation Scheduling (MTHGS) plays an important role in the operation of hydropower systems. In the first place, this paper presents a Chance Constrained Model for solving the optimal MTHGS problem. The model recognizes the impact of inflow uncertainty and the constraints involving hydrologic parameters subjected to uncertainty are described as probabilistic statements. It aims at providing a more practical technique compared to the traditional deterministic approaches used for MTHGS. The stochastic inflow is expressed as a simple discrete-time Markov chain and Stochastic Dynamic Programming is adopted to solve the model. Then in order to use the information of long-term inflow forecast to improve dispatching decisions, a Dynamic Control Model is developed. Short-term forecast results of the current period and long-term forecast results of the remaining period are treated as inputs of the model. Finally, the two methods are applied to MTHGS of Xiluodu hydro plant in China. The results are compared to those obtained from Deterministic Dynamic Programming with hindsight and advantages and disadvantages of the two methods are analyzed.     

Effect of cobalt oxide on surface structure of alumina supported molybdena catalysts studied by in situ Raman spectroscopy

A set of Co promoted 10% Mo/Al₂O₃ samples have been characterized by means of Raman spectroscopy under ambient as well as in situ dehydrated conditions. Under ambient conditions, the degree of the polymerization of surface molybdenum oxide species decreases with increasing Co loading. Under dehydrated conditions, the polymeric molybdenum oxide species is absent with the addition of only 0.2% Co. At low Co loadings (2%), before the formation of CoMoO₄ compound, the spectral features are very similar under ambient conditions. Dehydration causes the upward shift of the Mo=O symmetric stretching mode. A broad band around 920–930 cm^–1 was thus observed. This band has been suggested to be associated with the Co-Mo interaction species. In contrast to crystalline CoMoO₄, this species shows a reversibility on H₂ reduction-O₂ reoxidation treatments. From the results obtained, it is proposed that cobalt oxide interacts with the most polymerized molybdenum oxide species to form Co-Mo interaction species and/or crystalline CoMoO₄; therefore, the amount of the surface molybdenum oxide species decreases with a change in the molecular structure as a function of the Co concentration.     

CSG-Ⅰ型抽油机综合诊断仪的研究与应用

针对中原油田各采油厂所用抽油井综合诊断仪所出现的各种问题 ,开发出一种准确、可靠、便携式新型抽油井综合诊断仪———CSG—Ⅰ型综合诊断仪。改进后的示功仪位移部分的光电增量编码器 ,用 5KΩ高灵敏度可调电位器代替 ,电位器的活动端随拉线盒的转动而旋转成不同角度 ,对应不同的电阻值 ,在电位器的两端供给 + 5V电压 ,随着电位器的阻值变化 ,自由端便可输出 0～ 5V的电压 ,电压的变化量与光杆的位移变化成正比。该仪器投入使用后操作方便、安全可靠、测试功能齐全、性能稳定、计算准确 ,深受广大测试人员的喜爱。     

我国烧碱市场分析与展望

回顾了2005年我国烧碱的生产与市场消费情况,分析了2006年国内烧碱市场形势,对“十一五”期间我国烧碱市场总体趋势进行了展望。     

TiO_2薄膜光催化降解甲基橙反应动力学研究

以甲基橙为模型污染物、TiO2薄膜为光催化剂,在自制的光催化反应器上进行了光催化降解反应实验,主要研究了甲基橙初始浓度(c0)和紫外光光照强度(I)对其光催化降解反应的影响。结果表明,该降解反应可用一级反应动力学方程进行描述,反应速率常数(k)与c0及光强I的关系分别为:k∝c0-1 4和k∝I0.65。     

以高活性度石灰为原料制备纳米碳酸钙的研究

采用间歇鼓泡碳化法，通过对碳化反应温度、灰乳体积质量、搅拌转速、气体分布器开孔直径、消化浆液陈化时间等影响因素的控制，得到了用高活性度石灰为原料制备纳米碳酸钙的优化工艺条件，制得了平均粒径为15～40nm的纳米碳酸钙产品。