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排序方式: 共有1761条查询结果,搜索用时 156 毫秒
91.
92.
N. Kawamoto T. Horikoshi K. Nomura H. Yokota Y. Negishi E. Tobita M. Terano 《应用聚合物科学杂志》2006,99(4):1350-1358
The aluminum aryloxide was prepared via the reaction of phenolic antioxidant, 3‐(3,5‐di‐t‐butyl‐4‐hydroxyphenyl)‐N‐octadecylpropionamide, with triethyl aluminum. Propylene polymerization using supported Ziegler–Natta catalyst systems was carried out in the presence of the antioxidant or its aluminum aryloxide. Although the antioxidant gave rise to decrease in catalyst yield and change in hydrogen response, the aluminum aryloxide had no influence on the catalytic polymerization behavior, and thus the obtained polymer characteristics such as molecular weight, polydispersity, and meso pentad as a stereoregularity were comparable to that polymerized without the antioxidant and the aluminum aryloxide. Polypropylene obtained in the presence of the aluminum aryloxide was well stabilized for oxidation and its stability was over 1000 h at 100°C (estimated to be over 30 years at room temperature). © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 99: 1350–1358, 2006 相似文献
93.
Guanghui Cui Masamichi Fujikawa Shusaku Nagano Masami Sano Hiroshi Takase Tsukasa Miyazaki Shinichi Sakurai Katsuhiro Yamamoto 《Polymer》2014
Polystyrene-b-poly(methyl acrylate) (PS-b-PMA) block copolymer with PS volume fraction of 25.2 vol% was synthesized by atom transfer radical polymerization. Non-pretreated silicon wafers were used as the substrates to prepare perpendicular oriented PS cylinders in PMA matrix via solvent annealing which could induce the transformation of spheres to vertically oriented and hexagonally packed cylinders. The spherical microdomains were formed after the evaporation of solvents from the solutions of the block copolymer in selective solvents mixed from methanol, acetone and dichloromethane. The thickness of films could be as thick as 1000 nm, which were much thicker than usual cases and the cylinders came from the directional coalescence of the spheres, thus any pre-treatments of the substrates were not required for perpendicular orientation. The structures were characterized by small angle X-ray scattering (SAXS), transmission electron microscope (TEM), atom force microscopy (AFM) and grazing incidence small angle X-ray scattering (GISAXS). 相似文献
94.
J. Yamamatsu N. Kawano T. Arashi A. Sato Y. Nakano T. Nomura 《Journal of power sources》1996,60(2):199-203
The reliability of multilayer ceramic capacitors (MLCCs) with Ni internal electrodes has been studied trom the viewpoint of partial oxygen pressure (PO2) during firing. It is shown that the load-life time of the insulation resistance (1R) was prolonged by firing under low Po2 annealing after firing, and the addition of dopants. It is also shown that the generation of oxygen vacancies led to the degradation of IR. Annealing treatment for the oxidation of the dielectric body accelerates the dielectric aging of MLCCs. It is found that the appropriate control of the PO2 during firing can improve the reliability of MLCCs with Ni electrodes to a level as high as that of MLCCs with precious metal electrodes. Thus, we have developed an MLCC with Ni electrodes that features high reliability and a large capacitance of 10 μF for the Y5V characteristic and 4.7 μF for the X7R characteristic, both in the case of the C3216 (3.2 mm × 1.6 mm × 1.4 mm) form. 相似文献
95.
Shinobu Mukasa Tsunehiro Maehara Shinfuku Nomura Hiromichi Toyota Ayato Kawashima Yoshiaki Hattori Yukio Hashimoto Hiroshi Yamashita 《International Journal of Heat and Mass Transfer》2010,53(15-16):3067-3074
Plasma was generated in water by irradiation at high frequency of 13.56 MHz, and the behavior of bubbles including the plasma was observed by a high-speed camera. The generation pattern of the bubbles was classified into four types according to liquid temperature and supplied power. Conducting the simulation, the maximum temperature in the bubble was found to be from 3500 K to 4300 K, and the decomposition of water molecule occurred. The gas in the bubble was found to become high ratio of hydrogen. The phenomenon can be regarded as a film boiling of exceptionally high heat flux. 相似文献
96.
Keiichi Miyamoto Ayaka Kawasaki Yuko Nagata Masanori Uraya Hisayoshi Kojima Takanori Ito Takashi Horiuchi Nagisa Asakawa Shinsuke Nomura 《Materials science & engineering. C, Materials for biological applications》2011,31(2):158-165
Immunoglobulin A1 (IgA1) concentration in the plasma of patients with IgA nephropathy (IgAN) as the cause of renal failure is higher than that in the plasma of normal controls. IgA1 with abnormal sugars is considered to deposit in the glomerular mesangium, aggravating nephritis in IgAN. Jacalin is a lectin that recognizes sugars on IgA1. However, its selective-recognition for normal-type (ST type, NeuAc-α(2,3)-Gal-β(1,3)-GalNAc) and abnormal-type (T type, Gal-β(1,3)-GalNAc; Tn type, GalNAc; STn type, NeuAc-α(2,6)-GalNAc) sugars α-O-linked to serine/threonine in IgA1 is weak. Therefore, jacalin cannot be used for recognizing specific sugar types on IgA1. We attempted to develop a new recognition method for specific sugar types on IgA1 by utilizing the multirecognition capability of jacalin. Its binding abilities were regulated by heat denaturation with suitable template sugar (galactose or N-acetylgalactosamine). Further, we successfully prepared denatured-jacalin derivatives, which recognized ST-/T-type sugars on IgA1, by sugar-immobilized affinity chromatography. Enzyme-linked immunosorbent assay of denatured-jacalin derivatives, showed the ratios of abnormal sugars on IgA1 in the plasma of IgAN patients and normal controls to be approximately 60% and 20%, respectively. The results proved that profiling of sugar types in IgAN can successfully be performed by solely using jacalin derivatives. 相似文献
97.
R. Kondo Y. Tsutsumi H. Doi N. Nomura T. Hanawa 《Materials science & engineering. C, Materials for biological applications》2011,31(5):900-905
The effects of Pt and Pd addition to a Zr-20Nb alloy on its microstructure and mechanical property, as well as the elution of metals from the alloys in lactic acid solution, were investigated. The microstructure was characterized with an X-ray diffractometer (XRD), an optical microscope (OM), and a transmission electron microscope (TEM). The mechanical properties were evaluated by a tensile test. The β phase is dominantly observed in the Zr-20Nb as well as in the Pt-added and Pd-added Zr-20Nb alloys. Needle-like microstructures are observed in equiaxed grains in all alloys. Pd addition to the Zr-20Nb alloy suppresses ω phase formation more than Pt addition does. The 0.2% offset yield strength and the ultimate tensile strength of the Pt-added and Pd-added Zr-20Nb alloys increase with the Pt and Pd concentrations. XRD analysis revealed that the lattice parameter of β-Zr in the Pt-added and Pd-added Zr-20Nb alloys decreases with the Pt and Pd concentrations. Pt and Pd solute in β-Zr as a substitutional element and contribute to the increase in the strength by solid solution hardening. The addition of 2Pt and 2Pd to the Zr-20Nb alloy also improves metal elution from the alloys in lactic acid solution. 相似文献
98.
Takuya Takahashi Motoya Suzuki Ryuji Nomura Yuichi Okuda Koji Kamiya Takenori Numazawa Peter Shirron 《Microgravity science and technology》2011,23(4):365-372
Superfluid 4He was produced on a small jet plane for the first time using a small GM-refrigerator to condense the liquid and a scroll
pump to get the superfluid by evaporation. The surface wave on superfluid under 0.5g
E, 0.1g
E and 0.05g
E, together with 2g
E and 1g
E, was successfully examined by an optical method utilizing parabolic flight. Here, g
E is the gravitational constant on the ground. Assuming that only the fundamental mode was excited as determined by the sample
cell width, the resonance peak in the frequency domain was well reproduced by the gravity wave with corresponding gravity
constant. 相似文献
99.
Katsunori Takeda Tetsuo Hattori Tetsuya Izumi Hiromichi Kawano Shinichi Masuda 《Artificial Life and Robotics》2010,15(4):421-424
Recently, remote monitoring camera systems have been widely used for security. In such systems, one important function is
that the system automatically detects any change in the scenes from the monitoring cameras. In wireless remote monitoring
camera systems, the images of the scenes are generally transmitted as compressed data (e.g., JPEG file), because of the capacity
of the wireless channel. This article shows the automated detection of the change point in time-series data of compressed
JPEG file quantity (Kbytes) from the monitoring camera by applying the sequential probabilistic ratio test (SPRT) and the
Chow test, which is well known as a standard method for detecting structural change in time-series data. 相似文献
100.
Weixiao Huang Chow T.P. Niiyama Y. Nomura T. Yoshida S. 《Electron Device Letters, IEEE》2009,30(10):1018-1020
We report on the experimental demonstration of a novel n-channel GaN epilayer RESURF GaN MOSFET with good tradeoff between breakdown voltage and specific on-resistance for the first time. Device with 4-mum channel length and 16-mum RESURF length has breakdown voltage up to 730 V with specific on-resistance 34 mOmegamiddotcm2 (VG - VT = 20 V), best reported to date. 相似文献