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21.
Rockwell hardness measurement at an elevated temperature has been proposed as an evaluation method for the curing characteristics of thermosetting molding compounds. This method is convenient and has a high accuracy over a wide range of curing, Using a cone indenter, the following advantages are brought about: a good correspondence with acetone extraction test, in showing the degree of cure of the internal part of a molding rather than that of the skin layer, and a higher sensitivity in measuring higher degrees of cure. On examining curing behavior of commercial phenolic molding compounds by this method, an inflection point was observed on a plot of the hardness vs log curing time. This critical point has been called “the minimum cure time”, beyond which the molding exhibits good physical properties. 相似文献
22.
Hiroshi Mori Noritaka Mizuno Masahiro Tajima Shuichi Kagawa Masakazu Iwamoto 《Catalysis Letters》1991,10(1-2):35-39
Proton exchanged ultrastable Y-type zeolite with silica/alumina = 40 showed a pronounced catalytic activity for the formation of ethyl methyl ketone directly from 1-butene and water. The formation rate of ethyl methyl ketone was much higher than those on MoO3-based catalysts in the oxidation of 1-butene by oxygen. It was suggested that the basic site necessary for the formation of ethyl ketone directly from 1-butene and water would be the pentacoordinated Al. 相似文献
23.
Yuko Kizu Ray Hasegawa Isao Amemiya Shuichi Uchikoga Hirofumi Wakemoto 《Journal of the Society for Information Display》2009,17(8):647-658
Abstract— A 9‐in. full‐color polymer‐stabilized OCB TFT‐LCD with stable bend alignment in the absence of an electric field was developed. The condition of the polymer stabilization, the characteristics of UV‐curable monomers, and their influence on the configurations of the polymer network in the cell were studied. Possible models of the configuration were proposed and their relationship to the electro‐optical properties was analyzed using a novel simulation method considering the distribution of anchoring effects from both alignment surfaces and the polymer network. It was suggested that a good performance such as high contrast ratio and fast response could be expected in the polymer network originating from newly developed monomers composed of multifunctional LC acrylates due to a relatively weak‐anchoring effect and presumably its localization near the alignment surfaces. By using the newly developed monomers under the optimized polymer‐stabilizing process, a high contrast ratio of 250:1 and fast response nearly equal to that of a conventional OCB cell were achieved. 相似文献
24.
M Nakada M Hasegawa K Sakuda N Muramatsu J Yamashita M Suzuki 《Canadian Metallurgical Quarterly》1998,140(7):647-650
The authors report two cases of multicentric osteolytic lesions in the occipital bone without any history of head trauma. The excisional biopsy of the first case revealed that the lesion was multicentric but a continuous cavity with the subarachnoid space through various sizes of dural defect, and the cavities were covered by arachnoid lining. Together with the previously reported similar 5 cases, the characteristic common feature is multicentric osteolytic lesions in the occipital bone at advanced age without marginal sclerosis. "The cluster of arachnoid diverticula in the occipital bone (CADOB)" is probably the most appropriate term for these non-traumatic lesions with the following characteristics: elderly patients, occipital bone, midline, multiple, intact outer table, nonsclerotic margin and without history of trauma. Operation may not be indicated because of its non-progressive and benign nature. 相似文献
25.
Koichi Hasegawa Hideki Nishimori Masahiro Tatsumisago Tsutomu Minami 《Journal of Materials Science》1998,33(4):1095-1098
Thick silica films were prepared by the electrophoretic sol–gel deposition technique in the presence of poly(acrylic acid) (PAA) using monodispersed silica particles; the particles were prepared by the sol–gel method, pre-heat treated and then re-dispersed in the mixture of H2O and ethanol. The weight of deposited silica films was maximized when 0.2 mass % of PAA against the whole amount of sol was added. The particles constructing the thick silica films were packed densely when the amount of added PAA was less than 0.2 mass%. The weight of the film increased with decrease in the content of H2O in the sol when a fixed amount of PAA was added. After the heat treatment of deposited films at 800 °C, crack-free silica films of about 30 m thickness were prepared. © 1998 Chapman & Hall 相似文献
26.
The electron spin susceptibility of (BEDT-TTF)(ClMeTCNQ) was measured by ESR under pressure. Analysis of the susceptibility
leads to the temperature dependence of the ionic fraction through the neutral-ionic phase transition, revealing that the transition
is broad and continuous. It is demonstrated that this transition is crossover-like between the two phases, which can be understood
by the unique double-well potential. 相似文献
27.
Y. Takano K. Hiraki T. Takahashi R. Kondo S. Kagoshima T. Hasegawa T. Mocihda Y. Iwasa 《Journal of Low Temperature Physics》2006,142(3-4):647-650
We carried out77Se NMR measurements on BETS2(Cl2TCNQ) under pressure in order to investigate the magnetic properties of the insulating state which appears above 0.6 GPa.
The relaxation rate 1/T1 at 0.7 GPa shows small peak-like anomaly at 20 K, indicating a spin density wave transition as observed in BETS2(Br2TCNQ). 相似文献
28.
In order to determine the activities of phosphorus and iron in liquid {Cu‐Fe‐P} alloys, the two coexisting phases of liquid {Cu‐Fe‐P} alloys + <Cu‐Fe‐P> solid solutions were brought into equilibrium with a mixture of Al2O3 + AlPO4 + FexAl2O4 at temperatures of 1416K and 1526K. The oxygen partial pressures were measured with the aid of a solid‐oxide galvanic cell of the type: (+)Mo / Mo + MoO2/ ZrO2(MgO) / {Cu‐Fe‐P} + <Cu‐Fe‐P> + <Al2O3> + <AlPO4> + <FeAl2O4> / Fe(‐) The equilibrium reactions underlying the experiments can be expressed by 2[P]cu + (5/2) (O2) + <Al2O3> = 2 <AlPO4> and x[Fe]Cu + (1/2) (O2) + <Al2O3> = <FexAl2O4> The Henrian activity coefficient referred to 1 wt pct solution in pure liquid copper could be well expressed by the formula log fP° = (4.46±0.40) ‐ (8.67±0.59)/(T/K). The iron activities referred to pure solid iron could be formulated as log aFe =‐ (0.37 ± 0.12) + (500 ±200) /(T/K). 相似文献
29.
S.K. Sharma H. Zushi I. Takagi Y. Hisano T. Shikama S. Morita T. Tanabe N. Yoshida M. Sakamoto Y. Higashizono K. Hanada M. Hasegawa K. Nakamura H. Idei K.N. Sato S. Kawasaki H. Nakashima A. Higashijima Y. Takase 《Journal of Nuclear Materials》2012,420(1-3):83-93
In order to investigate the overall atomic hydrogen background and the dynamic characteristics of wall pumping/fuelling phenomenon, a permeation probe system has been developed and applied in the spherical tokamak QUEST. Reliability of measurements, within ±3% accuracy and a positive correlation with the hydrogen line emission over three orders of magnitude have been demonstrated for more than 3000 various plasma discharges. By comparison of the experimental permeation (flux) curves with the numerically simulated curves, the net incident atomic hydrogen flux is evaluated in the range of 1 × 1019 H m?2 s?1 to 4 × 1020 H m?2 s?1. The atomic flux has been investigated as a function of various plasma operation parameters like RF power, gas pressure and magnetic configuration. Using the static particle balance and permeation measurements, the progress in wall conditioning has been investigated. An inverse correlation between the atomic hydrogen flux and improvement in wall pumping has been observed over the two campaigns. 相似文献
30.
Sota H Yoshimine H Whittier RF Gotoh M Shinohara Y Hasegawa Y Okahata Y 《Analytical chemistry》2002,74(15):3592-3598
Despite high theoretical sensitivity, low-cost manufacture, and compactness potentially amenable to lab-on-a-chip use, practical hurdles have stymied the application of the quartz crystal microbalance (QCM) for aqueous applications such as detection of biomolecular interactions. The chief difficulty lies in achieving a sufficiently stable resonance signal in the presence of even minute fluctuations in hydrostatic pressure. In this work, we present a novel versatile planar sensor chip design (QCM chip) for a microliter-scale on-line biosensor. By sealing the quartz resonator along its edges to a flat, solid support, we provide uniform support for the crystal face not exposed to solvent, greatly decreasing deformation of the crystal resonator under hydrostatic pressure. Furthermore, this cassette design obviates the need for direct handling when exchanging the delicate quartz crystal in the flow cell. A prototype 27-MHz sensor signal exhibited very low noise over a range of flow rates up to 100 microL/min. In contrast, signals obtained from a conventional QCM sensor employing an O-ring-based holder were less stable and deteriorated even further with increasing flow rate. Additional control designs with intermediate amounts of unsupported undersurface yielded intermediate levels of stability, consistent with the interpretation that deformation of the crystal resonator under fluctuating hydraulic pressure is the chief source of noise. As a practical demonstration of the design's high effective sensitivity, we readily detected interaction between myoglobin and surface-bound antibody. 相似文献