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121.
P. Meenakshi S. E. Noorjahan R. Rajini U. Venkateswarlu C. Rose T. P. Sastry 《Bulletin of Materials Science》2002,25(1):25-29
DriedMusa paradiciaca (banana) stem and veins of the leaves, which were hitherto discarded as a waste, were collected and used as starting material
for the preparation of cellulose and cellulose acetate. This cellulose acetate was mixed with polystyrene to form blend of
cellulose acetate-polystyrene in order to provide enhanced stability and extended utility to the end products. The films of
these composites or their individual partners were made separately and studied for their mechanical properties, chemical modification
and morphological changes. We report here that banana stem is good source of cellulose and that cellulose completely undergoes
modification upon esterification. 相似文献
122.
P.U. Sharma K.B. Modi V.K. Lakhani K.B. Zankat H.H. Joshi 《Ceramics International》2007,33(8):1543-1546
Compositional dependence of hyperfine parameters, determined through Mössbauer spectral analysis has been studied for Y3−xFe5+xO12 (x = 0.0, 0.1, 0.3 and 0.5) garnet system at 300 K. The Mössbauer spectra have been fitted with three sextets in the ferrimagnetic state corresponding to Fe3+ ions at tetrahedral (d), octahedral (a) and dodecahedral (c) sites of the crystal structure. It is observed that isormershift, quadrupole shift and hyperfine field of d-site show no significant variation with Fe3+ concentration. The change in hyperfine fields of a- and c-sites with composition (x) has been explained on the basis of strength of exchange integrals, change in isomershift can be understood due to s-electron charge distribution and asymmetric displacement of oxygen ions surrounding the a- and c-sites seems to be responsible for observable quadrupole shift. The magneton number values obtained from magnetization and Mossbauer data are in agreement to those calculated using Neel's three sublattice model of ferrimagnetism. 相似文献
123.
As part of the European Community research programme telluric, magnetotelluric and geomagnetic deep sounding measurements were undertaken at 40 sites within the geothermal area of Travale. In the period range of 6–10,000 s the telluric field inside the Travale graben is strongly polarized and directed, independent of the period, about parallel to the graben strike. The lateral variation of the telluric field amplitude is determined mainly by the distribution of the rocks (e.g. the central part of the geothermal anomaly inside the graben is correlated with a horst structure of resistive rocks) and an influence of the geothermal anomaly on the telluric field distribution cannot be observed. The apparent resistivity, as well as the phase curves, are rather similar at all sites within the graben, exhibiting 4–40 ohm · m for periods of 10 s and 50–500 ohm · m for periods of 10,000 s in E-polarization. In the period range of 10–100 s the E- and B-polarization of magnetotelluric measurements can be interpreted by the 2-D effect of the Travale graben, while with increasing period the induced current system becomes more and more 3-D below all sites. This limits the determination of the sedimentary cover thickness (max. 2500 m) by 1-D and 2-D model calculations to periods of less than 100 s. 相似文献
124.
F. -U. Gast P. S. Dittrich P. Schwille M. Weigel M. Mertig J. Opitz U. Queitsch S. Diez B. Lincoln F. Wottawah S. Schinkinger J. Guck J. Käs J. Smolinski K. Salchert C. Werner C. Duschl M. S. Jäger K. Uhlig P. Geggier S. Howitz 《Microfluidics and nanofluidics》2006,2(1):21-36
We describe a novel microfluidic perfusion system for high-resolution microscopes. Its modular design allows pre-coating of
the coverslip surface with reagents, biomolecules, or cells. A poly(dimethylsiloxane) (PDMS) layer is cast in a special molding
station, using masters made by photolithography and dry etching of silicon or by photoresist patterning on glass or silicon.
This channel system can be reused while the coverslip is exchanged between experiments. As normal fluidic connectors are used,
the link to external, computer-programmable syringe pumps is standardized and various fluidic channel networks can be used
in the same setup. The system can house hydrogel microvalves and microelectrodes close to the imaging area to control the
influx of reaction partners. We present a range of applications, including single-molecule analysis by fluorescence correlation
spectroscopy (FCS), manipulation of single molecules for nanostructuring by hydrodynamic flow fields or the action of motor
proteins, generation of concentration gradients, trapping and stretching of live cells using optical fibers precisely mounted
in the PDMS layer, and the integration of microelectrodes for actuation and sensing. 相似文献
125.
Antioxidative properties of sour (cottage) were evaluated with (thermized) and without (native) heat treatment (80°C for 30 min). A model system comprising a Tween 20 stabilized peanut oil in phosphate buffer (pH 7.0) emulsion containing lipid oxidation catalysts, FeCl 3, H2O2 and ascorbate was used. Native sour whey powder (SWP) was significantly better than thermized whey in terms of limiting the formation of thiobarbituric acid‐reactive substances and peroxide value. Antioxidative ability was best at pH 3.0 and decreased with increasing pH. SWP (20%, w/v) was significantly better than all commonly used antioxidants tested after 96 h of incubation at 40°C. 相似文献
126.
Lithium-ion batteries are becoming more and more important not only for portable electronic devices, but also in prevision of high power electric vehicles. In such an optic, deep studies regarding all the components of a secondary battery are in development. In this study, high voltage cathode materials have been selected. Crystals with spinel structure have a 3D vacancy pathway suitable for Li-ions transport. The material under study was LiNi0.5Mn1.5O4 doped with magnesium replacing the nickel. Various samples were synthesized via three different routes: a solid-state method, a modified sol–gel method and a xerogel method. The structure and morphology of the powders were analyzed with HRTEM and XRD. Electrochemical tests were also performed. A wide range of particle sizes (from micro to nanosize) was the result of the different synthesis routes. Unfortunately pure materials were not always obtained. The electrochemical tests showed improvement of the material's cyclability, by reducing the particle size. The electrochemical tests further confirmed the existence of a Li1+dMn2−dO4 impurity. The results are quite promising, however, further improvement of the purity of the electrode composition are needed. 相似文献
127.
U. Reimer
H. -J. Schek
《Data & Knowledge Engineering》1989,4(4):321-352The first part of this paper introduces the basic constructs of a frame representation model and gives a formal definition for them. Subsequently the nested relational model (NF2) is described as an extension of the classical relational model to support relation-valued attributes. In the second part of this paper both models are compared with each other and a mapping of frame representation structures to NF2 structures is specified. The structural similarities between frames and NF2 relations are made clear and it is shown that their main difference is due to the type polymorphism introduced by the concept hierarchy of the frame model. This causes type collisions to occur in the strictly typed NF2 model when frames are directly mapped to NF2 structures. Two solutions to this problem are suggested and compared. The paper concludes with a reformulation of query operations of the frame model in terms of NF2 algebra operations. 相似文献
128.
U. Amato G. Amodeo V. Brandi V. Cuomo D. Ruggi C. Serio V. Silvestrini G. C. Tosato 《国际能源研究杂志》1985,9(1):33-51
In Italy solar thermal energy and energy from biogas are two possible means of reducing dependence on energy imports. Using a multiperiod LP model (MARKAL) the authors assessed the likely potential of both technologies under various circumstances. The study covered the period 1980–2005, in five segments of five years. It focused only on the subsystem of the energy end-uses which can be substituted for by solar thermal and biogas technologies. The overall non-renewable sources which can be saved in 20 years by these technologies total 450 PJ (1 PJ = 101 5 J) if the fuel prices rise at 0 per cent average annual, 1450 PJ if the fuel prices rise at 4.2 per cent average annual, 1860 PJ if the fuel prices rise at 7.2 per cent average annual and 3780 PJ if the fuel prices rise at 15 per cent average annual. However the most competitive technologies appear to be solar water heaters used mainly in the private and commercial sectors and biogas systems used mainly in the agricultural sector. The study was carried out by APRE under ENEA (formerly CNEN) contract and was intended to serve as an analytical basis for establishing an overall development and demonstration strategy for end-use renewable technologies in Italy. 相似文献
129.
The reliability of a system is the probability that the system will perform its intended mission under given conditions. This
paper provides an overview of the approaches to reliability modelling and identifies their strengths and weaknesses. The models
discussed include structure models, simple stochastic models and decomposable stochastic models. Ignoring time-dependence,
structure models give reliability as a function of the topological structure of the system. Simple stochastic models make
direct use of the properties of underlying stochastic processes, while decomposable models consider more complex systems and
analyse them through subsystems. Petri nets and dataflow graphs facilitate the analysis of complex systems by providing a
convenient framework for reliability analysis. 相似文献
130.