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951.
Summary: Soluble hyperbranched acrylate copolymers were prepared by the copolymerization of divinylbenzene (0.10 mol · L?1) and ethyl acrylate (0.50 mol · L?1) using dimethyl 2,2′‐azoisobutyrate of high concentrations (0.30–0.50 mol · L?1) as initiator at 70 and 80 °C in benzene. The copolymer formed at 80 °C for 1 h showed the weight‐average molecular weight of 2.5 × 105, the small radius of gyration of 10 nm, the low second virial coefficient of 5.7 × l0?7 mL · g?2 as shown by the MALLS measurements at 25 °C in tetrahydrofuran, and also the very low intrinsic viscosity of 0.10 dL · g?1 at 30 °C in benzene. The hyperbranched copolymer exhibited an upper critical solution temperature (35 °C on cooling) in an acetone‐water (60:11 v/v). The copolymer showed an ability to encapsulate and transfer Rhodamine 6G as a dye probe and could stabilize Ag nanoparticles. The porous film was prepared by simply casting an acetone solution of the hyperbranched copolymer on a cover glass. The copolymer molecules radially arranged on the surface layer of the spherical pores as observed by the polarized optical microscope. The hyperbranched acrylate copolymer was hydrolyzed by KOH to yield poly(carboxylic acid).
952.
Tabata S Takemura Y Kobayashi M Ikeda M Nishimura S Sato Y Tatsumi R Ikeuchi Y Iwamoto H 《Journal of electron microscopy》2006,55(5):265-271
The mechanism of intracellular calcium ions (Ca(2+)) increase in chicken myoblasts was studied using histological, immunohistochemical, immunoblotting and Ca(2+) imaging techniques. Mononuclear myoblasts at embryonic day 12 (E12) contained myofibrils in the peripheral cytoplasm, and the sarcoplasmic reticulum was observed in the cytoplasm. Several Ca(2+)-related receptors, namely acetylcholine (ACh) receptors, dihydropyridine receptors (DHPRs) and ryanodine receptors (RyRs), were detected in the tissue as early as E12. Western blotting analyses detected one band corresponding to RyR subtype 3 (RyR3) at E12 and two bands corresponding to RyR1 and RyR3 after E13. Ca(2+) imaging of mononuclear myoblasts in vitro revealed an intense Ca(2+)-increase response to ACh stimulation, and this effect was abolished after EGTA addition to the culture medium. Nifedipine treatment also led to a lack of Ca(2+) increase in response to ACh stimulation, while ryanodine treatment led to a weak Ca(2+)-increase response. On the other hand, multinuclear myoblasts showed a Ca(2+)-increase response to ACh stimulation in the presence of not only EGTA but also nifedipine, although ryanodine treatment led to a lack of Ca(2+) increase. These results suggest that the mechanism of Ca(2+) increase in mononuclear myoblasts involves extracellular Ca(2+) entry through DHPRs, which is amplified by Ca(2+) release from the cytoplasmic Ca(2+) store, while multinuclear myoblasts mainly depend on Ca(2+) release from the cytoplasmic Ca(2+) store. 相似文献
953.
Ohshima T. Kondo T. Kitajima N. Sato M. 《Industry Applications, IEEE Transactions on》2010,46(1):23-28
954.
Hiroki Mori Oleksandr Mikhyeyev Takuo Nagamine Mizue Mori Yuichi Sato 《Journal of Mechanical Science and Technology》2010,24(1):93-96
When a plate-like object is rubbed by rubber, friction-induced vibration is generated. To reduce the friction-induced vibration,
we experimentally investigate the characteristics of the vibration of a rectangular glass plate. The results show that the
frequency of the friction-induced vibration is almost the same as the natural frequency of a glass plate. The vibration is
generated when the natural frequency of a rubbing system is close to that of a glass plate. We then examine the effect of
a dynamic absorber mounted on the glass plate. The results demonstrate that the damping of a dynamic absorber is effective
for suppressing the friction-induced vibration. Numerical simulation is also performed using a simplified analytical model.
The calculated results agree qualitatively with the experimental ones. 相似文献
955.
Masanori Seki Masahiro Fujii Yuji Kobayashi Masaaki Sato Akira Yoshida 《Journal of Mechanical Science and Technology》2010,24(1):141-144
To investigate the influence of shot peening on the surface durability of powder-forged rollers, the case-hardened powder-forged
rollers with a forging density of 7.5 g/cm3 treated by the single shot peening and the double shot peening were fatigue-tested under a sliding-rolling contact condition.
The surface roughness, the surface hardness and the surface compressive residual stress of the rollers were increased by the
shot peening. In addition, the pores near the roller surface were deformed by the shot peening. The failure mode of all the
test rollers was spalling due to subsurface cracking. The fatigue lives of all the test rollers were improved by the shot
peening, and that of the test roller S08, which was shot-peened with the hardest steel shots in this experimental range, was
especially improved. The surface durability of the test roller S08 was also most improved by the shot peening. Cracks became
difficult to occur and propagate under the roller surface since the pores near the roller surface were deformed by the stronger
shot peening. In this study, double shot peening, which generally restrains the increase in surface roughness, was not particularly
effective for the improvement in the surface durability of the powder-forged rollers, because the influence of tangential
force on fatigue was not always great in a case of subsurface cracking. 相似文献
956.
V.P. de Souza D. Costa D. dos Santos A.G. Sato J.M.C. Bueno 《International Journal of Hydrogen Energy》2012
The effect of Pt addition on the oxi-reduction properties of α-Al2O3-supported Ni catalysts, with different degrees of interaction between NiO and the α-Al2O3 support, was studied using atmospheres of H2, H2/H2O, and CH4/H2O. The effect of Pt promotion on the reduction of NiO with H2 was significant for NiO species that interacted more strongly with the alumina surface, but was much lower when a NiAl2O4-like bulk phase was formed. For samples activated with H2, although metal dispersion decreased with increasing Pt content, the activity was maintained constant by the presence of Pt sites. For samples activated with a CH4/H2O mixture, the activity increased with increasing Pt content, due to the higher reducibility of Ni in the Pt-promoted catalysts. The Pt promotion effect was stable; there was no important decrease in the influence of Pt on NiO reduction, even after high temperature re-oxidation of the catalysts. 相似文献
957.
Yazan Al-ZainYosuke Sato Hee Young Kim Hideki HosodaTae Hyun Nam Shuichi Miyazaki 《Acta Materialia》2012,60(5):2437-2447
The effect of room temperature (RT) aging on the superelasticity of Ti-Nb-Mo-based superelastic alloys is investigated. The results show that annealing at relatively low temperatures such as 973 K after severe cold rolling results in poor resistance to the effect of RT aging. The transformation stress increases considerably due to the formation of an isothermal ω phase at RT. Addition of Sn is partially effective in suppressing the RT aging effect in the specimens annealed at 973 K. The RT aging effect is suppressed by increasing the annealing temperature, due to the annihilation of lattice defects or non-equilibrium vacancies introduced during cold rolling, which are responsible for accelerating the diffusion process, however, superelasticity is reduced by annealing at higher temperatures, due to a decrease in the critical stress for slip deformation (σCSS). The specimen annealed at 1173 K followed by aging at 773 K exhibits stable superelasticity with a high resistance to the effect of RT aging. Annealing at 1173 K causes the annihilation of lattice defects or non-equilibrium vacancies, while aging at 773 K induces precipitation of the α phase, which in turn causes an increase in σCSS, and further enhances the resistance to the RT aging effect by enriching the matrix with β-stabilizing elements. 相似文献
958.
In a previous study, we reported measurements of three-dimensional (3D) optical coherence tomography (OCT) images through a thinned skull by reducing temperatures from 28 °C to 18 °C in vivo in the rat brain to show negative correlation coefficients (CCs) between ratios of signal intensity (RSI) and temperature for applications to monitoring brain viability. In this study, using the same OCT system, we measured 3D OCT images of the rat brain by periodically changing tissue temperatures from 20 °C to 32 °C in vivo. In the evaluation of CCs among RSI, temperature, and heart rate, the largest number of periods was four, and the longest measurement time was 570 min. Averaged CCs between RSI and temperature, and between RSI and heart rate, were -0.42 to -0.50 and -0.48 to -0.64, respectively. RSI reversibly changed subsequent variations of temperatures and finally increased rapidly just before cardiac arrest. These results indicate that RSI could correspond to decreases in viability because of local ischemia and recovery. 相似文献
959.
Katsuhiro Narasaki Shoji Tsunematsu Kiyomi Ootsuka Kenichi Kanao Akinobu Okabayashi Kazuhisa Mitsuda Hiroshi Murakami Takao Nakagawa Kenichi Kikuchi Ryota Sato Hiroyuki Sugita Youichi Sato Masahide Murakami Masanori Kobayashi 《低温学》2012,52(4-6):188-195
This report describes the results and operating status of ground lifetime testing and achievements on orbit of coolers for space use. Ground lifetime tests of coolers of three types were conducted to demonstrate their long life and reliability. Three single-stage Stirling coolers were tested for 89,016, 71,871 and 68,273 h from 1998, a two-stage Stirling cooler was tested for 72,906 h, and a 4-K class cooler with a two-stage Stirling cooler and a Joule–Thomson cooler was tested for over 2.5 years. After lifetime tests were completed, a few coolers were investigated to determine the cause of the cooling performance degradation. Additionally, the filled gas of the coolers was analyzed. These coolers have shown good results on orbit. Three single-stage Stirling coolers were carried on the X-ray astronomical satellite “SUZAKU” (launched in July 2005), Japanese lunar polar orbiter “KAGUYA” (launched in September 2007), and the Japanese Venus Climate Orbiter “AKATSUKI” (launched in June 2010). Two units of a two-stage Stirling cooler were carried on the infrared astronomical satellite “AKARI” launched in February 2006. A 4-K class cooler was carried on the Superconducting Submillimeter-Wave Limb-Emission Sounder (SMILES) aboard the Japanese Experiment Module (JEM) of the International Space Station (ISS). SMILES was launched in September 2009. 相似文献
960.
Isao Saeki Yusuke Sugiyama Shigenari Hayashi Akira Yamauchi Takashi Doi Yoshitaka Nishiyama Shoji Kyo Shigeru Suzuki Masugu Sato Shinji Fujimoto 《Corrosion Science》2012
Changes in the crystal structure of type 430 stainless steel and the oxides on its surface were studied in situ at 1373 K using a high-intensity synchrotron X-ray source provided by SPring-8 in Japan. The surface of the steel was initially covered with Cr2O3, which was then converted to FeCr2O4, and finally Fe3O4 and Fe2O3 formed on it. These results indicated that the reason for the breakaway oxidation in type 430 stainless steel is Cr depletion beneath Cr2O3 layer and the subsequent ionisation of Fe, not the simple mechanical failure of Cr2O3. 相似文献