Functionalization of soluble polymers

Summary The synthesis of di-(4-formylphenyloxyethyl) poly(oxyethylene) and the corresponding oxime derivative are described. Kinetic aspects of the reaction of the dichloro telechelic with 4-hydroxy benzaldehyde are investigated and discussed.     

HACCP在紫菜米果生产中的应用研究

在分析和研究紫菜米果的生产工艺的基础上,探讨了危害分析与关键点控制(HACCP)质量管理体系在其生产中的应用,以求确保产品的安全卫生,保证消费者的健康,使产品达到出口标准.     

换填法建筑地基处理的工程实录

结合某工程的地基处理，对换填法的应用作了较详细的阐述。     

美孚油回收利用的可行性实验研究

本文针对美孚油回收液与兰炼8#油混合利用进行可行性实验研究，经过重度、粘度、可燃性等方面的实验研究，表明美孚油回收液与兰炼8#油混合可以用在电动轮上并且获得良好的效果。     

用于生产甲基丙烯酸的杂多酸催化剂的研究

以异丁烯为原料的两段直接氧化生产甲基丙烯酸最新工艺有许多优点。其技术关键在于研制出高效的甲基丙烯醛选择性氧化催化剂。本文报道P-Mo-As-Cu杂多化合物催化剂的组成、制备条件对催化剂活性的影响。经优化后获得高选择性、高活性的二段氧化催化剂，其甲基丙烯酸收率达60％以上。     

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本文通过对在用钻机井架的现场实际测试,建立数据库、测评模型,对实测的数据用计算机技术进行分析,提出了初始弯曲应力;数据正态分布检验——x～2检验;建立回归方程;在给定置信度下测评当前承载能力的技术概念。解决了在用钻机A型井架的安全性评估问题,是一种较为合理、可靠、科学的测评技术和方法。     

Inter- and intra-molecular ionic interactions of polyampholyte: Carboxymethyl-2-diethylaminoethylcellulose

Carboxymethyl-2-diethylaminoethylcellulose (CM-DEAE cellulose) was prepared by etherification of carboxymethylcellulose with diethylaminoethyl chloride in a NaOH solution. The behaviour of CM-DEAE cellulose in aqueous solution was studied by viscosity and GPC measurements. The degree of substitution (DS) and existing states of DEAE substituents were examined by the use of proton NMR, and those of the CM substituents were observed with FT-IR. The results reveal that the reduced viscosity and apparent molecular size of CM-DEAE cellulose vary with the concentration of sodium chloride and changes in pH and DS. These phenomena can be explained in terms of inter- and intra-molecular ionic interactions.     

Crystallization behaviour of Ni-Co-base metallic glasses by isochronal and isothermal annealing

The crystallization behaviour of three amorphous alloys, Co₅₀Ni₂₅Si₁₅B₁₀, Ni₅₀Co₂₅Si₁₅B₁₀ and Ni₅₀Co₂₅P₁₅B₁₀, was studied by means of differential thermal analysis in conjunction with scanning transmission electron microscopy. Isochronal annealing showed a strong dependence of crystallization on scan rate over the range of 1.99 to 20.70 K min^–1. At high Co/Ni ratios, a sequential two-stage crystallization process involving primary MS-I phase followed by MS-II phase precipitation was observed. At low Co/Ni ratios MS-I and MS-II crystallization were concurrent and inseparable. Replacement of the metalloid Si with P as the glass-former dramatically reduced the activation energy for crystallization as well as the crystallization temperature. A mechanistic understanding of these findings was pursued in light of TEM/STEM microanalysis