微波电子回旋共振等离子体技术及其应用

微波电子回旋共振等离子体是淀积薄膜、微细加工和材料表面改性的一种重要手段。由于这种等离子体电离水平高,化学活性好,可以用来实现基片上薄膜的室温化学气相淀积和反应离子刻蚀,因此对于微电子学、光电子学和薄膜传感器件的发展,这种等离子体会具有重要的意义。此外,采用微波电子回旋共振等离子体原理,没有灯丝的离子源可以提高离子源的使用寿命,可以增加离子束的束流密度。可以确信,微波电子回旋共振等离子体的发展,将把离子源技术提高到一个新的水平。显然,这必将对材料表面改性工艺,包括离子注入掺杂等工艺的发展发挥作用。自从1985年以来,为了得到大容积等离子体而发展了微波电子回旋共振多磁极等离子体,这些技术在薄膜技术、微细加工以及材料表面改性中的应用前景是乐观的。我们将在本文中,介绍微波电子回旋共振等离子体的原理及其应用。     

湍流大气中光波闪烁的计算及实验测量比较

采用修正Rytov方法和近似理论计算了球面波在湍流大气中传播的闪烁指数，并与实验结果进行了比较，发现在弱起伏和中等湍流起伏区修正Rytov解与实验结果符合得良好，而在饱和区采用考虑内尺度效应下的近似理论结果更符合实验结果。     

内燃机车曲轴中频淬火过程的数值模拟

借助 ANSYS大型有限元分析软件 ,实现了 16 V2 4 0曲轴淬火过程的计算机模拟 ,模拟结果可直观地显示出任一时刻曲轴表面及内部的温度分布、冷却曲线以及淬火结束后的残余应力分布 ,并能预测淬硬层深度。同时对比了轴颈内圆角处进行淬火和不进行淬火两种工艺的效果 ,为现场提供了用虚拟现实方法详尽分析和研究淬火工艺的工具。     

Bright Blue Light—emitting Diodes Based on a Novel Fluorescent Dye Containing Heterocyclic Groups

Novel molecular material ,1-benzothiazoly-3-pheny1-pyrazoline (BTPP) was found to function as bright blue light emitting dye in organic electroluminescent device, and its optical and electric characteristics were investigated. This heterovyclic compound exhibited good characteristics of blue photoluminescence and electroluminescence,which had the emission peak at 450nm .The single layer light-emitting devices using BTPP as light -emitting material dispersed in poly(N-vinylcarbazole)(PVK) and double layer ones using PBD as hole block layer above the light-emitting layer were fabricated using conventional spin-casting and vaccum vapour deposition methods. The introduction of PBD has enhanced electron injection and luminance efficiency, compared with the single layer LEDs.     

用小波变换抑制SAR图像中的斑点噪声

抑制合成孔径雷达图像中的斑点噪声一直是处理图像并得到准确图像信息的难点，提出了一种基于小波变换抑制合成孔径雷达（SAR）图像中的斑点噪声的方法，对原有的小波变换方法作了改进，能更好地保留图像的边缘信息，并能简化计算量。在仿真实验中使用了合成的模拟图像和真实的合成孔径雷图像，并与以往的小波去噪滤波方法以及一些经典的斑点噪声滤波方法（包括中值滤波，Lee滤波，Frost滤波）进行比较，在综合考虑了滤波算法在均匀区域对斑点噪声的抑制能力以及保留边缘信息能力的情况下，提出的算法有更好的效果。     

四路激光跟踪测量系统最佳测量区域和系统自标定

研究了系统最佳布局下的最佳测量区域问题,给出了几何精度衰减因子PDOP在三维空间内的变化规律。通过计算机仿真研究了最佳测量布局对系统自标定的影响规律,指出最佳测量布局中的标称配置对系统自标定精度的影响最小,同时这种布局有着最小的几何精度衰减因子。     

Preparation and characterization of polyurethane microcapsules containing n‐octadecane with styrene‐maleic anhydride as a surfactant by interfacial polycondensation

A series of polyurethane microcapsules containing a phase change material (PCM) of n‐octadecane was successfully synthesized by an interfacial polymerization in aqueous styrene‐maleic anhydride (SMA) dispersion with diethylene triamine (DETA) as a chain extender reacting with toluene‐2,4‐diisocyanate (TDI). The average diameter of microPCMs is in the range of 5–10 μm under the stirring speed of 3000–4000 rpm. Optical and SEM morphologies of microPCMs had ensured that the shell was regularly fabricated with the influence of SMA. FTIR results confirmed that the shell material was polyurethane and the SMA chains associated on core material reacted with TDI forming a part of shell material. The shell thickness was decreasing in the range of 0.31–0.55 μm with the molar ratio of DETA/TDI from 0.84 to 1.35 and the weight of core material increasing from 40 to 80% (wt %). By controlling the weight ratio of PCM as 40, 50, 60, 70, and 80% in microPCMs, it was found using DSC that the T_m and T_c of microPCMs were in the range of 29.8–31.0^oC and 21.1–22.0°C and an obvious phase change had been achieved nearly the same temperature range of that of PCM. The results from release curves of microPCM samples prepared by 1.4, 1.7, and 2.0 g of SMA indicated the release properties were affected by the amount of the dispersant, which attributed to the emulsion effect and shell polymerization structure. The above results suggest that the shell structure of microPCMs can be controlled and the properties of microPCMs determined by shell will perform proper practical usage. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4996–5006, 2006     

纳米二氧化钛的表面修饰与应用的研究进展

介绍了纳米二氧化钛表面修饰的两种主要方法:无机和有机表面包覆,以及进行修饰后的纳米二氧化钛的应用.     

物理-化学复合解堵工艺技术在临11井的应用

在天然气勘探开发过程中的使用钻井液、压井液及暂堵剂造成裂缝系统产层堵塞，一直是困扰老井天然气生产的一大难题。综合运用物理一化学复合解堵工艺进行井下解堵是蜀南气矿一种新的技术尝试。结合临11井解堵实际，从该产层及井底堵塞物分析解堵药剂研制机理、现场应用情况、注意事项等多个方面，阐述了作者对物理-化学复合解堵工艺原理和应用的认识，对提高气井产能和老气田的开发水平有积极的指导意义。     

构皮滩水电站尾水隧洞特大断面软岩开挖支护

构皮滩水电站尾水隧洞软岩不良地质洞段占尾水隧洞全长的70%以上,确保软岩洞段的安全快速开挖是尾水隧洞施工的关键,尤其一次支护的强度对洞室稳定影响极大。为此,施工中根据软岩的地质特点及尾水隧洞开挖的断面尺寸,采取分层开挖和超前锚杆的施工方式和型钢拱架进行一次支护。根据监测结果,围岩变形很小,一次支护效果良好,表明构皮滩水电站尾水隧洞大断面软岩采取的开挖方式和一次支护方式是成功的。