制备2，4－二氯－5－氟苯甲酰乙酸甲酯的缩合剂及工艺研究

通过３种不同的碱来制备２，４－二氯－５－氟苯甲酰乙酸甲酯，优选得到了其最佳缩合剂甲醇钠；同时应用正交设计实验，研究了原料配比、反应时间、反应温度对收率的影响，在优选条件下收率为７８．５％。     

FAST MEASUREMENT OF ASH CONTENT IN COAL WASHING PLANT

The coal filter cake is a product of fine coal after floatation which has an ash content of 7-13%, water content of 30±2%, and a particle size of less than 1 mm. The ash content was measured by the intensity of the single backscattered gamma-ray, and its accuracy is mainly dependent on the energy of the gamma-ray. The 238Pu low energy photon source is selected in this work. The energy of its gamma-ray is 15 keV, which can result not only in the best sensitivity, but also in the lowest contribution to the environment radiation. The root mean square deviation of the ash measurement is±0.33% (±1σ).     

A new method for calculating loss coefficients [of power systems]

A method is proposed which avoids many limitations associated with traditional B-coefficient loss coefficient calculation. The proposed method, unlike the traditional B-coefficient method, is very fast and can handle line outages. The method utilizes network sensitivity factors which are established from DC load flow solutions, Line outage distribution factors (ODFs) are formulated using changes in network power generations to simulate the outaged line from the network. The method avoids the use of complicated reference frame transformations based upon Kron's tenser analysis. The necessity of data normalization used in least squares and the evaluation of the slope of &thetas;_j versus PG_n is not necessary with the proposed method. Using IEEE standard 14-bus and 30-bus systems, the method's results are compared against results obtained from an AC load flow program (LFED). The method's solution speed is compared to that of the LFED method, the base case database method and the conventional B-coefficient method based on A_jn-factor. The proposed method is easy to implement and, when compared to other methods, has exhibited good accuracy and rapid execution times. The method is well suited to online dispatch applications     

专家系统在化工中的应用进展

本文综述了近年来专家系统在化工领域的应用状况，并指出今后的发展趋势。     

石膏制品防水防潮剂的研制与开发

本文提出采用高分子有机材料配合，生产石膏制品防水防潮剂的生产方法和工艺。该剂还可以应用到氧化镁系列板材，同时提出开发珠光或彩色防水防潮剂，能达到满足的装饰效果，值提开发推广。     

����ѡ����ˮ��������ܴ���ѧģʽ���о���Ӧ�á�����̸TI��59����������ѧģʽŵģͼ

��Consulting the relevant documents at home and abroad,the author finisheid the derivation of quations about critical flow quantity,critical flow rate,contrast flow quantity,contrast flow rate which are necessary to the continuous water withdrawal through the flow string with different diameters and the rational flow string formula that should be selected when the contrust parameter1.The author also works out the solving programme for TI-59 computer and designs and draws up the nomograrn of mathematical mode.The evident economical results have been obtained from practice of optimizing the flow string for water withdrawal in gas production in Southern Sichuan and from studying the gas-water two-phase flow characteristics through vertical pipe.     

Fivefold symmetry in real and reciprocal spaces

Tetrahedrally close-packed structures with juxtaposed pentagonal antiprisms, such as the μ, C14 Laves and the newly found C phases, were studied by means of HREM and SAD. It was found that each bright spot in the structural image corresponds to an antiprism. Differently oriented domains of these phases intergrow frequently with a fairly good match at the interphase boundary. All diffraction patterns of these phases show a fivefold distribution of spot-pairs, and it is shown that this fivefold symmetry comes from the pentagons and spot-pairs from two pentagonal prisms superposed in antisymmetrical positions.     

鄱阳湖湖底沉积物放射性水平

本文报道了1985年鄱阳湖湖底沉积物放射性水平的调查结果。沉积物中 U、Th、~(226)Ra、~(40)(?)和~(137)Cs 的比活度分别为64.8、67.9,58.9、676.1和3.5Bq/kg;用~(137)Cs 测龄方法作了沉积物泥芯垂直深度的年代定位,由此得知1985—1958年对应深度沉积物中 U、Th、~(226)Ra 和~(40)K 的比活度与1957—1930年对应深度沉积物比较无显著性差异;U、Th 和~(226)Ra 的浓集因予分别为5.2×10~413.9×10~4和4.8×10~4L/kg。