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采用大试样高温热重分析仪研究了不烧Al-Si复合低碳Al2O3-β-SiAlON材料(MAC-F)的抗氧化性,并与Al-Si复合不烧铝碳滑板材料(MAC-S)进行了比较。结果表明(1)两种材料在250~1100℃氧化时的质量变化规律相似,在500℃以前均处于质量损失状态;从500℃开始试样处于质量增加状态,500~1100℃之间两种材料质量变化率的增加量差别不大;1100℃以上材料MAC-S的质量变化率的增加量明显提高,而材料MAC-F质量变化率的增加量稍有降低。(2)1500℃氧化后,材料MAC-F质量增加率明显低于材料MAC-S的,氧化层很薄,厚度仅0.5mm。材料MAC-F的氧化层中有较多的短柱状莫来石晶体,均匀地分布在刚玉骨架结构的空隙中,形成致密的结构,对氧气进入材料的内部起到了阻碍作用。其氧化层表面覆盖着一层由莫来石和少量玻璃相组成的光滑薄膜,更有效阻碍了氧气向内部的渗透。因此,材料MAC-F与材料MAC-S相比,抗氧化性能更为优异。 相似文献
96.
Xuejing Zhu Dan Gao Vittorio Albertazzi Jianyong Zhong Li-Jun Ma Liping Du Yu Shyr Valentina Kon Hai-Chun Yang Agnes B. Fogo 《International journal of molecular sciences》2022,23(11)
We previously found that short-term treatment (week 8 to 12 after injury) with high-dose angiotensin receptor blocker (ARB) induced the regression of existing glomerulosclerosis in 5/6 nephrectomy rats. We therefore assessed the effects of long-term intervention with ARB vs. nonspecific antihypertensives in this study. Adult rats underwent 5/6 nephrectomy and renal biopsy 8 weeks later. The rats were then divided into three groups with equivalent renal function and glomerular sclerosis and treated with high-dose losartan (ARB), nonspecific antihypertensive triple-therapy (TRX), or left untreated (Control) until week 30. We found that blood pressure, serum creatinine levels, and glomerulosclerosis were lower at sacrifice in ARB and TRX vs. Control. Only ARB reduced proteinuria and maintained the density of WT-1-positive podocytes. Glomerular tufts showed more double-positive cells for CD44, a marker of activated parietal epithelial cells, and synaptopodin after ARB vs. TRX or Control. ARB treatment reduced aldosterone levels. ARB-treated rats had significantly improved survival when compared with TRX or Control. We conclude that both long-term ARB and triple-therapy ameliorate progression, but do not sustain the regression of glomerulosclerosis. ARB resulted in the superior preservation of podocyte integrity and decreased proteinuria and aldosterone, linked to increased survival in the uremic environment. 相似文献
97.
Guixiang Tang Xuanbo Zhong Wei Hong Jianfei Li Yue Shu Lulu Liu 《International journal of molecular sciences》2022,23(12)
Soybean cyst nematode (SCN, Heterodera glycines Ichinohe) causes an estimated economic loss of about USD 3 billion each year in soybean (Glycine max L.) production worldwide. Overexpression of resistance genes against SCN provides a powerful approach to develop SCN resistance cultivars in soybean. The clarification of molecular characterization in transformation events is a prerequisite for ecological risk assessment, food safety, and commercial release of genetically modified crops. Here, we generated transgenic events harboring the BCN (beet cyst nematode) resistance Hs1pro−1 gene using the Agrobacterium-mediated method in soybean, evaluated their resistance to SCN infection, and clarified the molecular characterization of one of the transformation events. Five independent and stable inheritable transformation events were generated by an Agrobacterium-mediated transformation method. SCN resistance tests showed the average number of developed females per plant and female index (FI) in T4 ZHs1-1, ZHs1-2, ZHs1-3, ZHs1-4, and ZHs1-5 transformation events were significantly lower than that in the nontransgenic control. Among these, the ZHs1-2 transformation event had the lowest number of developed females per plant and FI. Southern hybridization showed the exogenous target Hs1pro−1 gene was inserted in one copy and the Bar gene was inserted two copies in the ZHs1-2 transformation event. The exogenous T-DNA fragment was integrated in the reverse position of Chr02: 5351566–5231578 (mainly the Bar gene expression cassette) and in the forward position of Chr03: 17083358–17083400 (intact T-DNA, including Hs1pro−1 and Bar gene expression cassette) using a whole genome sequencing method (WGS). The results of WGS method and Southern hybridization were consistent. All the functional elements of exogenous T-DNA fragments were verified by PCR using specific primer pairs in the T5 and T6 ZHs1-2 transformation events. These results demonstrated that the overexpression of Hs1pro−1 gene enhanced SCN resistance, and provide an important reference for the biosafety assessment and the labeling detection in transformation event ZHs1-2. 相似文献
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GR-3500型氧弹式量热计做燃烧焓的测定实验时间长,操作难度大,实验一次性成功率低.通过放宽对实验过程中夹层与量热容器的水温差值要求,实验结果表明夹层水温高于量热容器水温的0.5~3.0℃都是可行的,这样便于学生调节水温,缩短实验时间,取得良好的实验效果. 相似文献
100.
SO_4~(2-)/ZrO_2超强酸催化剂的结构表征 总被引:1,自引:0,他引:1
用BET法分析了制备条件对SO_4 ̄(2-)/ZrO_2超强酸催化剂的比表面和孔结构的影响,用SEM观察了催化剂的表面形貌。结果表明,引人SO_4 ̄(2-)后催化剂的比表面和比表面的热稳定性都增大了,在H_2SO_4浓度为1.0mol/1和焙烧温度约773K时催化剂的比表面较大。制备Zr(OH)_4时用浓氨水得到的催化剂的比表面、平均孔径和孔体积都较大。SO_4 ̄(2-)/ZrO_2催化剂的孔为平均孔径3-5nm的中孔。SEM结果表明,SO_4 ̄(2-)/ZrO_2催化剂的表面为很不平整的蜂窝状。 相似文献