砷、氟污染地下水净化技术进展

砷、氟污染水体及其共存问题是环境领域的热点问题,长期暴露其中对公众的身体健康存在巨大威胁.文章梳理了砷、氟污染物的来源,及砷、氟污染水体的分布与危害,并按吸附、离子交换、反渗透、电絮凝、膜法等分析了用于砷、氟处理的各类技术手段的利弊,以期为后续水体中砷、氟污染物的高效去除提供参考.     

TiO2/MOFs的制备及污染物降解现状

TiO2是较为成熟的半导体光催化材料,但因TiO2分散性差、量子利用率低、比表面积小、难回收等问题难以工业化.多孔金属有机框架(MOFs)的引入可增强TiO2/MOFs复合材料的光吸收性能,提高电子-空穴对分离效率和提高回收率.基于TiO2/MOFs制备时前驱体添加顺序不同,综述了TiO2/MOFs的3种制备方法(即Ship-in-a-bottle法、Bottle-around-ship法、One-pot法)及TiO2/MOFs光催化机理与性能影响因素,并探讨不同MOFs与TiO2结合的作用机理.最后,对TiO2/MOFs存在的问题提出建议.     

热处理工艺对BT9合金疲劳和高温持久性能的影响

本文研究了不同的热处理工艺对BT9钛合金的疲劳寿命和高温持久强度的影响,并对其组织、断口进行了光学和电子金相分析。指出了获得良好的综合机械性能的热处理工艺,并讨论了在不同区域内疲劳裂纹扩展的方式。     

Effect of ultrasonic power and bonding force on the bonding strength of copper ball bonds

Copper wire, serving as a cost-saving alternative to gold wire, has been used in many high-end thermosonic ball bonding applications. In this paper, the bond shear force, bond shear strength, and the ball bond diameter are adopted to evaluate the bonding quality. It is concluded that the ef/~cient ultrasonic power is needed to soften the ball to form the copper bonds with high bonding strength. However, excessive ultrasonic power would serve as a fatigue loading to weaken the bonding. Excessive or less bonding force would cause cratering in the silicon.     

Synthesis of LaF3 superfine powder by microwave heating method

LaF3 superfine powder was synthesized from La(CH3COO)3 and NH4 F by microwave heating method,using ethanol or pure water as dispersants respectively. The results of XRD and SEM indicate that the superfine powder has high purity, regular particle shape and narrow distribution of granularity. The granularity of the best sample is in the range of 100 -200 nm. The influence of different dispersants on the crystal degree and microstructure was discussed. After the superfine powder was formed into a slice at pressure of 25 - 60 MPa, its electrochemical impedance spectroscopy was tested by electrochemical impedance spectroscopy (EIS) measurement. The result shows that the grain refining of LaF3 powder increases its ionic conductivity. Compared with traditional preparation methods of LaF3 powder, the advantages of microwave heating method were summarized.     

34CrNiMo钢齿轮轴开裂原因分析

对34CrNiMo钢齿轮轴的化学成分、金相组织及断口分析表明，其淬火开裂的主要原因是由于锻造温度过高，导致过热缺陷所致。     

肥皂冒霜的成因探讨

本文讨论了肥皂冒白霜的主要原因,即肥皂中无机盐含量和油脂皂化后的有机酸败。生产实践证明,皂基含NaOH≤0．3%,NaCl≤0.2%,SiO2≥3%为宜;有机酸中含低分子酸和不饱和酸,必须控制油脂的酸价和严格控制工艺操作。     

长化恩德炉运行中的问题及对策

我公司为了降低成本，提高企业的竞争能力，于2003年把煤气化工艺由富氧连续气化改为恩德粉煤气化。针对恩德炉实际生产过程中出现的一系列问题，公司及时采取相应措施，取得了较好的效果。下面简要介绍我公司恩德炉运行中出现的问题及应对措施。