云南滇黄精药渣中多糖含量的测定

以测定云南滇黄精药渣中多糖的含量为目的,采用热回流法提取总多糖,以葡萄糖为对照品制作标准曲线,采用苯酚-硫酸法和可见分光光度法测定多糖含量。研究结果表明该方法的线性关系良好,线性相关系数≥0.999,精密度良好,相对标准偏差≤3%,准确性良好,平均回收率为99.40%,测得6批滇黄精药渣中多糖的平均含量为4.47%,实验结果可为滇黄精的综合利用提供一定的参考。     

Rapid growth of angle-confined large-domain graphene bicrystals

In the chemical vapor deposition growth of large-area graphene polycrystalline thin films,the coalescence of randomly oriented graphene domains results in a high density of uncertain grain boundaries (GBs).The structures and properties of various GBs are highly dependent on the misorientation angles between the graphene domains,which can significantly affect the performance of the graphene films and impede their industrial applications.Graphene bicrystals with a specific type of GB can be synthesized via the controllable growth of graphene domains with a predefined lattice orientation.Although the bicrystal has been widely investigated for traditional bulk materials,no successful synthesis strategy has been presented for growing two-dimensional graphene bicrystals.In this study, we demonstrate a simple approach for growing well-aligned large-domain graphene bicrystals with a confined tilt angle of 30° on a facilely recrystallized single-crystal Cu (100) substrate.Control of the density of the GBs with a misorientation angle of 30° was realized via the controllable rapid growth of subcentimeter graphene domains with the assistance of a cooperative catalytic surface-passivation treatment.The large-area production of graphene bicrystals consisting of the sole specific GBs with a tunable density provides a new material platform for fundamental studies and practical applications.     

连续混炼过程比能耗分析

将连续混炼过程的有效比能耗分为升温、混炼、脱挥和建压比能耗,并提出了计算各项的一种方法。用该方法对不同机型、不同规格、不同加工对象的连续混炼机的比能耗进行了分析。结果表明,在多数连续混炼过程中,升温比能耗在总有效比能耗中所占比例都较大,建压比能耗所占比例都很小;原料热物性是影响有效比能耗及其构成的根本因素;当原料和混炼产物质量确定时,连续混炼机的螺杆与机筒结构、螺杆直径、产量、混炼工艺等都会影响有效比能耗及其构成。     

Growth and characterization of Pb0.97La0.02(Zr0.66Sn0.27Ti0.07)O3 antiferroelectric single crystals

Single crystals of Pb_0.97La_0.02(Zr_0.66Sn_0.27Ti_0.07)O₃ (PLZST) with the composition near the morphotropic phase boundary were grown by the flux method. The PbO–PbF₂–B₂O₃ system was used as a solvent. PLZST single crystals with the size of 4–6 mm are obtained and these crystals are slightly translucent after polishing. The splitting of (200) reflection peak indicates that the obtained crystals are of a single phase with tetragonal perovskite structure. The element contents of the grown crystals were measured by inductively coupled plasma atomic emission spectrometry. The chemical composition of the crystals is Pb_0.979La_0.014(Zr_0.666Sn_0.285Ti_0.049)O₃. Thermal properties and dielectric properties of PLZST single crystals were studied. The results show that flux-grown PLZST single crystals exhibit obvious endothermic processes and relaxor behaviors near the phase transition temperatures.     

关于细胞神经网络无性模板的设计

本文以连通片检测器无性模板的设计为例，给出了细胞神经网络中无性模板的设计方法及连通片检测器无性模板中各元素的数值范围。     

浅谈微生物实验室培养基制备

培养基的质量是微生物实验室检测工作的基础,事关检测工作的准确性、可靠性。因此,培养基的制备和使用是微生物实验室检测工作中的重要环节。本文针对培养基的储存、制备、灭菌后保存及灭菌效果检验进行分析,以便于保证检测结果的科学有效。     

A novel de-rusting method with molten salt precleaning and laser cleaning for the recycling of steel parts

Clean Technologies and Environmental Policy - Steel parts are a kind of high recovery value product for which de-rusting is the primary step in the recycling process. Laser cleaning is a popular...     

振动功率流方法诊断梁的损伤

利用振动功率流方法对无限直梁在集中力作用下的损伤进行了诊断研究。损伤部位模拟为转动弹簧,利用断裂力学的有关理论得到其转动刚度。研究了梁在集中载荷作用下的弯曲波运动以及振动功率流的输入和传播,分析了振动功率流与破损位置及其特征尺寸的关系。首先从理论上研究了破损诊断的具体步骤,然后进行了实验研究,结果证明了理论分析的准确性和可靠性。     

热声系统内交变流动特性的数值模拟

对热声系统中交变流动的声场与流场分布进行了数值模拟,得到了热声谐振管和回热器(板叠)内的压力和速度分布及二者之间的相位关系.数值模拟表明:在谐振管内,在模拟的边界条件下,径向速度分布出现"环形效应",流动分为核心区的完全湍流流动和湍流边界层内的粘性流动;对于水力半径和粘性渗透层深度相当的热声板叠,其内速度分布逐步出现"环形效应",流动介于层流和湍流的过渡区,为过渡态流动,在流道的大部分区域压力和速度振荡的相位差趋向于π/2;对于水力半径和粘性渗透层深度之比较小的热声回热器,其内交变流动的流动特性与稳态流动的相似,速度的径向分布为抛物线形,类似于定常流动的层流速度分布.