带约束拉杆L形方钢管混凝土组合异形柱的受力研究

为研究对拉约束拉杆对组合柱性能的影响,针对L形组合异形柱设置不同类型的约束拉杆、不同强度材料等进行数值模拟,对比该类型下的相应试验结果,分析验证了对拉约束拉杆对L形组合异形柱的性能改善作用,得到了对拉约束在柱延性及承载力方面的积极影响效果。最后基于线性回归分析的理论计算方法表现出了和数值结果较高的一致性,建立了具有较高参考价值的带约束拉杆的组合异形柱承载力计算公式。     

高转化率SBR1712的合成和性能

分子量调节剂叔十二碳硫醇(TDM)采用分批加入方式,TDM补加量为0.35～0.45份;选用歧化松香酸钾和脂肪酸钠复合乳化剂,采用一次加入方式;在聚合速率为(7～8)%/h时,可制备出转化率达70%±2%的充油丁苯橡胶SBR 1712(充油量27.3%).在10L釜中进行扩大试验,所得试样的性能与JSR公司同类产品的性能相当.     

State estimation for complex systems with randomly occurring nonlinearities and randomly missing measurements

This paper is concerned with the state estimation problem for the complex networked systems with randomly occurring nonlinearities and randomly missing measurements. The nonlinearities are included to describe the phenomena of nonlinear disturbances which exist in the network and may occur in a probabilistic way. Considering the fact that probabilistic data missing may occur in the process of information transmission, we introduce the randomly data missing into the sensor measurements. The aim of this paper is to design a state estimator to estimate the true states of the considered complex network through the available output measurements. By using a Lyapunov functional and some stochastic analysis techniques, sufficient criteria are obtained in the form of linear matrix inequalities under which the estimation error dynamics is globally asymptotically stable in the mean square. Furthermore, the state estimator gain is also obtained. Finally, a numerical example is employed to illustrate the effectiveness of the proposed state estimation conditions.     

State space approximation for general fractional order dynamic systems

Approximations for general fractional order dynamic systems are of much theoretical and practical interest. In this paper, a new approximate method for fractional order integrator is proposed. The poles of the approximate model are unrelated to the order of integrator. This feature shows benefits on extending the algorithm to the systems containing various fractional orders. Then a unified approximate method is derived for general fractional order linear or nonlinear dynamic systems via combining the proposed new method with the distributed frequency model approach. Numerical examples are given to show the wide applicability of our method and to illustrate the acceptable accuracy for approximations as well.     

Feedback nonlinear discrete-time systems

In this paper, we design an adaptive iterative learning control method for a class of high-order nonlinear output feedback discrete-time systems with random initial conditions and iteration-varying desired trajectories. An n-step ahead predictor approach is employed to estimate future outputs. The discrete Nussbaum gain method is incorporated into the control design to deal with unknown control directions. The proposed control algorithm ensures that the tracking error converges to zero asymptotically along the iterative learning axis except for the beginning outputs affected by random initial conditions. A numerical simulation is carried out to demonstrate the efficacy of the presented control laws.     

Dynamics stability in wireless sensor networks active defense model

Wireless sensor networks, which are widely used in military, industrial and transportation fields, are vulnerable to various kinds of attacks, since they are mostly deployed in a relatively open environment. Based on the evolutionary game theory, this paper proposes a proactive defense model for wireless sensor networks, in which we emphasize that the node has a limited ability to learn the evolution of rationality from different attack strategies of the attacker, and can dynamically adjust their strategies to achieve the most effective defense. Following this approach, the cost (e.g., energy consumption and wastage of machinery) has been greatly saved and the life cycle of the nodes has been extended as well. By employing the proposed model, the whole wireless sensor network can be implemented in an effective way.     

A New Indole Synthesis Promoted by Metal Triflates

A new synthesis of 4- and 7-carbon-substituted indoles is described. The overall sequence involves the addition of a nitrile oxide to 1 carboethoxy-2-(or 3-) allylpyrrole, hydrogenation of the intermediate isoxazoline to β-hydroxy ketone and cyclization of the ketol using magnesium or zinc triflate to the substituted indole. This new indole-forming strategy can also accommodate the introduction of oxygen functionality into the indole 6-position. Possible mechanistic aspects of the reaction are detailed.     

Examining the role of perceived value in virtual communities continuance: its antecedents and the influence of experience

Although perceived value has long been recognised as an influential means of affecting continuance intention in information systems (IS), little attention has been devoted to explore its antecedents, which constitutes an important research issue. This study, building on prior literature on continued usage in IS as well as the resource-based view, proposed a model to address this gap. Our model suggests that perceived value, a major driving force for members’ satisfaction and continuance intention, is affected by four kinds of resources embedded in virtual communities, which are relationship resources, technology infrastructure, knowledge resources and human resources. To provide additional insights on the pivotal role of perceived value, we also postulate that experience moderates the link between perceived value and its antecedents. Data collected from 235 members of a professional virtual community provide strong support for the research model. It was found that perceived value exerts a great effect on both satisfaction and continuance intention. In addition, when different levels of experience are taken into consideration, relationship resources, knowledge resources and human resources were found to be more salient to high-experience members, whereas technology infrastructure was found to be more salient to low-experience members. Finally, this study discusses the implications of these findings and offers direction for future research.     

羧甲基淀粉的应用与合成

综述了羧甲基淀粉的发展、合成方法、合成过程中的影响因素以及应用现状。羧甲基淀粉的合成主要分三种类型 :干法、半干法、湿法。综合了反应过程中的影响因素 ,例如醚化剂和催化剂的影响 ,反应时间和温度的关系 ,溶剂、设备对反应的影响 ,以及在食品、医药、钻井、纺织、日化工业中的应用前景     

Intercalated PS/Na+‐MMT Nanocomposites Prepared by Ultrasonically Initiated In Situ Emulsion Polymerization

Summary: A new technique, ultrasonically initiated in situ emulsion polymerization, was employed to prepare intercalated polystyrene/Na⁺‐MMT nanocomposites. FTIR, XRD, and TEM results confirm that the hydrophobic PS can easily intercalate into the galleries of hydrophilic montmorillonite via ultrasonically initiated in situ emulsion polymerization, taking advantages of the multi‐effects of ultrasonic irradiation, such as dispersion, pulverization, activation, and initiation. Properly reducing SDS concentration is beneficial to widen the d‐spacing between clay layers. However, the Na⁺‐MMT amount has little effect on the d‐spacing of nanocomposites. The glass transition temperature of nanocomposites increased as the percentage of clay increased, although the average molecular weight of PS decreased, and the decomposition temperature of the 1obtained nanocomposites moves to higher temperature.

TEM of PS/Na⁺‐MMT nanocomposite prepared by ultrasonically initiated in situ emulsion polymerization.