3-甲基-7-二正丙氨基-1,4-氧氮杂萘-2-酮的合成

以间氨基酚为原料,经N 烷基化、亚硝化,制得2 亚硝基 5 二正丙氨基苯酚,其收率为91 6%。该化合物经还原、成环反应后,合成出3 甲基 7 二正丙氨基 1,4 氧氮杂萘 2 酮,其收率为80 3%。实验确定1 溴丙烷、亚硝酸钠及丙酮酸乙酯的最佳用量分别为70mL、11 5g和2mL(以15g间氨基酚为基准)。     

掺银对TIBaCaCuO系超导体性能的影响

本文研究了掺入适量的银对TlBaCaCuO系超导体超导性能的影响。实验结果表明,当银的掺入量不超过0.3mol时,有利于2223相的形成;在掺入0.3mol银的同时,适当提高组成中Tl或Cu的含量,可以降低烧结温度,并能获得T_(o0)=122K,T_(onset)=136K的TlBaCaCuO系超导体。     

浅谈涂布烘箱设计

探讨了涂布烘箱的设计方法,较系统地讨论了设计对流式涂布烘箱的內容、各种参数的确定等有关问题.     

基于面向对象技术的图书馆管理系统研究

基于面向对象技术在软件开发中得到了广泛的应用。图书馆管理系统需求的复杂性要求其采用面向对象方法进行系统分析和设计．基于此，本文对基于面向对象技术的网络化图书馆管理系统进行了研究；首先介绍了Browser／Server系统结构和面向对象的系统分析技术，结合图书馆的实际要求，对图书馆管理系统进行了需求分析、功能模块划分、数据库模式分析，然后对图书馆管理的相关内容进行了分析，最后研究了图书馆管理系统的框架结构以及主要模块．     

Determination of the modified effect of nano-SiO2 by titration in nonaqueous phase

The dispersion of nanosilica that was modified and original in organic solvents could be judged directly by using methyl red as the indicator, and the principle of color development was also discussed. A method has been developed for the determination of the acidity of solid surfaces, which consists of titration of the solid suspended in benzene with n-butyl amine, using neutral red as the indicator. Basic indicator forms a red color on acidic solids, and the end-point of the titration is the disappearance of the red color. The text was submitted by the authors in English.     

Experimental investigation on the detachable thermosiphon for conduction-cooled superconducting magnets

A detachable thermosiphon, as a transient thermal switch for conduction-cooled superconducting magnet, is designed, fabricated and tested. A thermosiphon between the first and second stages of a cryocooler can reduce the cool-down time of a conduction-cooled superconducting magnet by using the large cooling capacity of the first stage. The thermosiphon is a very efficient heat transfer device until all the working fluid in it freezes (off-state). After the working fluid freezes and the second stage temperature becomes lower than that of the first stage, however, the thermosiphon then becomes a conduction heat leak path between two stages of the cryocooler. Considering a very small cooling capacity of the second stage of the cryocooler around 4.2 K, the conduction heat loss is not negligible. Therefore, a detachable thermosiphon, made of a metal bellows, is considered to be able to eliminate such a conduction heat leak. The mock-up magnet is cooled down with the thermosiphon and the thermodynamic states of the thermosiphon and the mock-up magnet are precisely examined during the whole cool-down process. At off-state, the thermosiphon is detached mechanically from the magnet. In this way, the conduction heat leak path through the thermosiphon wall is completely eliminated. This paper describes the detailed transient operation of the detachable thermosiphon using nitrogen as the working fluid.     

大机组调峰对锅炉运行的影响及运行优化研究

利用炉膛断面温度场可视化监测系统、节能环保车、炉内三维数值模拟等先进的技术和设备对大机组调峰稳定性和运行方式优化进行试验和理论研究。     

风机动力型末端在变风量空调系统中的应用

通过对从低温送风技术中发展起来的变风量系统末端--风机动力箱的分析,在实际应用中对比两种型式的该种末端,分析其优缺点,认为这是一种值得在高级办公大楼中优先考虑和推广的系统形式.     

Automatic feature selection for unsupervised clustering of cycle-based signals in manufacturing processes

Recent developments in sensing and computer technology have resulted in most manufacturing processes becoming a data-rich environment. A cycle-based signal refers to an analog or digital signal that is obtained during each repetition of an operation cycle in a manufacturing process. It is a very important class of in-process sensing signals for manufacturing processes because it contains extensive information on the process condition and product quality (e.g., the forming force signal in forging processes). In contrast with currently available supervised classification approaches that heavily depend on the training dataset or engineering field knowledge, this paper aims to develop an automatic feature selection method for the unsupervised clustering of cycle-base signals. First, principal component analysis is applied to the raw signals. Then a new method is proposed to select information containing principal components to allow clustering to be performed. The dimension of the problem can be significantly reduced through the use of these two steps. Finally, a model-based clustering method is applied to the selected principal components to find the clusters in the cycle-based signals. A numerical example and a real-world example of a forging process are used to illustrate the effectiveness of the proposed method. The proposed technique is an important data pre-processing technique for the monitoring and diagnostic system development using cycle-based signals for manufacturing processes.