含氟聚酰亚胺的辐射交联及其交联度的XPS表征

含氟聚酰亚胺(FPI)是一种耐高温、耐水解的新型聚酰亚胺。到目前为止,尚未见文献报道它的辐射交联。本文发现它能在高温辐射下交联,交联后的含氟聚酰亚胺的玻璃化转变温度以及高温力学性能有明显提高。本文还首次用XPS方法做了它的交联度表征。用XPS方法求得FPI的凝胶化剂量为50Mrad。     

Fine-line conductor manufacturing using drop-on demand PZT printingtechnology

An emerging selective metallization process to fabricate fine-line conductors based on drop-on-demand (DOD) ink jet printing and novel nano-particle fluid suspensions (NPFS) was studied. The suspensions consist of 1-10 nm silver or gold particulates that are homogeneously suspended in an organic carrier. A piezo-electric droplet generator driven by a bipolar voltage signal is used to dispense 50-70 μm diameter droplets traveling at 1-3 m/s before impacting a compliant polyimide substrate. The deposit/substrate composite is subsequently processed at 300°C for 15 min to allow for complete evaporation of the carrier and for sintering of the nano-particles, thereby yielding a finished circuit interconnect. Test vehicles created using this technique exhibit features as fine as 120 μm wide and 1 μm thick with resistivities on the order of 3.5×10^-5 Ωcm. The circuitry performed well under environmental conditioning. As expected, repeatability of circuitry fabrication showed sensitivity to the generation of steady, satellite-free droplets. In an effort to generate droplets consistently, it is essential to develop a strong fundamental understanding of the correlation between device excitation parameters and dispensed fluid properties, and to resolve the microrheological behavior of the NPFS when flowing through the droplet generator     

智能小区中的网络和布线设计解决方案——智能建筑学术讨论系列文章之七

当前小区信息网络建设中存在多种实施方案。笔者分析比较了常用的几种典型方案的优劣。讨论了目前建设中的一些解决方法，提出了兼顾现状，适度超前的设计实施原则。     

Combined shape and sizing optimization of truss structures

 In this paper, an evolutionary optimization method is presented for weight minimum problem of a 3-dimensional truss structure in terms of nodal coordinates and element cross-sectional areas. The structure is subject to stress, local buckling and displacement constraints. Two types of design variables with different natures are optimized separately: (1) a fully stressed design (FSD) and scaling techniques are applied to sizing variables and (2) the evolutionary node shift method is applied to shape variables. Alternating procedure is utilized to couple the two types of variables and to combine the results. The optimum solution is achieved gradually from the initial configuration design. Two typical truss structures are examined to illustrate the validity of the method. Received: 22 October 2001 / Accepted: 04 June 2002 This research work is supported by the National Natural Science Foundation of China under the guarantees no. 10072050 and 10172072, respectively.     

油田放射性作业人员外周血淋巴细胞染色体畸变的观察

本文调查了油田212例受γ射线和中子混合辐射照射的作业人员和30例正常人的外周血淋巴细胞染色体畸变。作业人员受γ射线照射的人均年受照剂量为1.28mGy。调查结果表明,放射性测井人员与正常人相比染色体畸变率有显著差异。     

石油系油浆与煤系闪蒸油的焦化性能——I．热解条件的影响

通过偏光显微镜观察了石油系油浆（LH）与煤系闪蒸油（SN）焦化后所得焦块的光学结构。结果表明，在较宽条件下两种原料单独焦化均得不到取向度高的流线型结构。将两种原料以一定比例混合后先热解丙焦化所得焦块的光学结构明显好于二者混合后直接焦化所得焦块的光学结构，其中LH和SN以3：2的重量比混合后在440℃、1MPa下热解3．5h然后再在530℃、1MPa下焦化8h所得焦块为具有较高取向度的流线型结构，适合于作为针状焦的起始原料。