Effects of tantalum on austenitic transformation kinetics of RAFM steel

The RAFM (reduced activation ferritic/martensitic) steels containing different tantalum contents (0 wt.％,0.027 wt.％,0.073 wt.％) were designed and cast.Differential scanning calorimetry and optical microscopy were employed to explore the influence of tantalum content on the austenitic transformation of RAFM steels.The austenitic transformation kinetics was described by a phase-transformation model.The model,involving site saturation nucleation,diffusion-controlled growth and impingement correction,was established based on the classical Johnson-Mehl-Avrami-Kolmogorov model.The phase-transformation kinetics parameters,including D0 (pre-exponential factor for diffusion) and Qd (activation energy for diffusion),were calculated by fitting the experimental data and the kinetic model.The results indicated that the average grain size is decreased with the increase of tantalum.The values of Ac1 and Ac3 (onset and finish temperature of austenitic transformation,respectively) are increased by increasing the tantalum content.The increase of tantalum caused the decrease of D0.However,Qd is increased with the increase of tantalum.In addition,as a carbides forming element,tantalum would reduce the carbon diffusion coefficient and slow down the austenitic transformation rate.     

A rapid method for simultaneous determination of triterpenoid saponins in Pulsatilla turczaninovii using microwave-assisted extraction and high performance liquid chromatography–tandem mass spectrometry

In the present study, a microwave-assisted extraction (MAE) and high performance liquid chromatography–tandem mass spectrometry (HPLC–MS/MS) method was developed for the simultaneous determination of seven triterpenoid saponins in Pulsatilla turczaninovii. Operational conditions of MAE were optimized using a central composite design. Multiple-reaction monitoring was employed for quantification while switching the electrospray ion source polarity between positive and negative modes. Full validation of the method was carried out (linearity, precision, accuracy, limit of detection and limit of quantification). The results indicated that the method was rapid, specific and reliable. The developed method was successfully applied to determine the investigated compounds in nine batches of P. turczaninovii. These samples were collected in different seasons from the Liaoning province and varied greatly. The total triterpenoid saponins content was the highest in April, the seedling stage, and decreased from May to August. The contents of total triterpenoid saponins decreased significantly after the blooming period.     

带式输送机空载功率计算方法探讨

带式输送机空载功率是鉴定制造、安装质量的重要指标。介绍一种比较准确和简便的空载功率计算方法。     

基于GSM-Hi技术的农村无线宽带建设方案及部署策略

当前宽带建设的重点集中在城市地区,而农村地区目前2G和3G仍作为农村无线数据业务的主要承载网络,宽带设施发展水平提升并不显著,不能适应农村互联网快速发展的需要.因此,如何实现农村宽带接入建设,解决农村区域上网难的问题显得尤为重要,GSM-Hi技术应运而生.     

基于三维非连续接触模型的管片接头静动力特性分析

基于非线性接触理论,考虑盾构隧道结构的非连续性,模拟管片接头结构和管片衬砌与围岩及道床之间的相互作用,建立了道床-管片-围岩的三维非连续接触模型,对盾构隧道管片接头在围岩静压、列车动载作用下的受力与变形进行了深入分析。研究结果表明,围岩静压下拱顶和隧底处的纵向接头部分向内张开,两侧拱腰处的接头部分向外张开,拱顶处的封顶块与邻接块错台较大,拱腰接头受压明显,拱顶接头受压最小,各环管片拱顶处的螺栓轴力最大,隧底处的其次,拱腰处的接头螺栓轴力最小,旋转了一定拼装角度后位于拱肩上部的接头螺栓,其剪力最大;列车动载作用下管片接头的张开错台、混凝土应力以及接头螺栓的内力均在动载施加初期迅速增加,然后明显减小,而后产生波动,其中浅埋地铁隧道拱顶接头的动力响应较隧底接头明显,螺栓剪力在列车动载作用下较螺栓轴力增加的多。     

掺钨类金刚石膜的制备与性能研究

采用无灯丝长条离子源结合非平衡磁控溅射的方法，在不同基体上制备了面积较大、光滑、均匀的掺钨类金刚石（W-DLC）膜层，用SEM、Raman、XPS、XRD、硬度计、划痕仪、摩擦磨损试验机等手段分析和研究了膜层的形貌、结构及部分性能．结果表明：膜／基硬度高，W—DLC／Si为Hv0.02515=3577；膜／基结合力在45-75N之间；摩擦系数小，抗磨损性能良好．     

GC-MS测定乌参中多环芳烃残留

建立了气相色谱-质谱法（GC-MS）同时测定乌参中20种多环芳烃残留的方法。样品经蒸馏水混合和二氯甲烷萃取,浓缩,硅胶层析柱净化,外标法定量。20种多环芳烃得到较好的分离,回收率为92.0%~103.0%,相对标准偏差（RSD）为1.86%~4.62%,检出限10μg/kg。实验结果表明,该方法简单、快速、重现性好,能满足乌参中多环芳烃残留的测定要求。     

基于模板热压法制备超疏水柱状结构表面

超疏水表面材料在生产生活中具有重要的应用价值,其制备的关键在于构建合适的表面微结构。以多孔阳极氧化铝表面为模板,高密度聚乙烯为压印热塑材料,进行常压工况下的热压印,制备出三维柱状结构表面,表面形貌规整有序,通过调节模板结构参数实现对柱状结构尺寸的精确调控。测试结果显示,制备的不同微结构尺寸的柱状结构表面接触角均在150°以上,具有优异的超疏水性能。     

Dolfi定理的Brauer形式

给定一个p-可解群G以及G的一个关于该素数p的不可约Brauer特征标x.证明了x在G的任意一个子群N上的限制的不可约分量的次数可被N及其在G中的正规化子满足的条件所控制,从而把Dolfi定理从复特征标推广到Brauer特征标情形,并得到了p-可解群中关于Brauer特征标的Clifford定理的某种推广.     

一种小型校园网的组网方案

提出一种小型校园网的组网方案,从逻辑上把校园网分成校务网、教学网、公共网等三个独立的业务网,使用MA5200F作为核心组网设备,使用Quidway○RS2026和Quidway○RS3026做为各逻辑组成的交换机,使用Eudemon 100为专用硬件防火墙设备,并通过S2026的端口的VLAN特性对其用户进行VLAN的划分和访问权限的控制,这使得构建出来的校园网具有性能高、扩展性高、安全性高和管理简单等特点.