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991.
自蔓延高温技术制备ZrC粉体(英文) 总被引:4,自引:0,他引:4
采用自蔓延高温合成(self-propagating high-temperature synthesis,SHS)技术,以 Zr+C 为反应体系合成了 ZrC 粉末。研究了实验参数对 SHS过程中点火电流、燃烧温度的影响。采用了 3 种碳源,研究了其对最终产物形貌及化学组成的影响。通过添加不同含量的 NaCl 作为 SHS 稀释剂,控制产物粒径及形貌。结果表明:炭黑是高温自蔓延法制备 ZrC 粉体的最佳碳源。由该体系制备的 ZrC 粉末粒径在 0.5~1 μm之间,氧含量为 0.38%。随稀释剂 NaCl 含量增加,体系燃烧温度降低,产物粒径减小。当 NaCl 含量为 30% (质量分数)时,体系燃烧温度下降至 1 810 K,产物 ZrC 粉末的粒径减小至 50 nm。 相似文献
992.
Chang-Min LEE Jun-Hyung LIM Soo-Min HWANG Eui-Cheol PARK Jong-Hyun SHIM Jin-Hyun PARK Jinho JOO Seung-Boo JUNG 《中国有色金属学会会刊》2009,19(4):965-969
Flexible copper clad laminates(FCCLs) were fabricated using the electro-plating process and the combined effect of the current density and plating time on their surface morphology, texture, hardness, electrical resistivity and folding behavior was evaluated. To achieve Cu layers with similar thicknesses, the current density was varied in the range of 0.2–3 A/dm2 and the plating time was controlled in the range of 0.5–7.5 h to compensate for the variation of the current density. The surface morphology, hardness, and folding behavior were characterized by atomic force microscopy, nanoindentation technique and Massachusett Institute of Technology folding endurance test, respectively. The X-ray diffraction patterns indicated that the Cu phase was formed without any secondary phases; however, the preferred orientation changed from (220) to (111) as the current density increased over 1 A/dm2. In addition, it was observed that the root-mean-square and hardness values decreased when the current density increased and the plating time decreased simultaneously. The electrical resistivity was as low as approximately 21 nΩ·m and the number of cycles without failure in the folding test was over 15 000, which were comparable to those of commercial FCCLs. 相似文献
993.
As-cast CC slabs of microalloyed steels are prone to surface and sub-surface cracking. Precipitation phenomena initiated during solidification reduce ductility at high temperature. The unidirectional solidification unit is employed to simulate the solidification process during continuous casting. Precipitation behavior and thermal stability are systematically investigated. Samples of adding titanium and niobium to steels have been examined using field emission scanning electron microscope (FE-SEM), electron probe X-ray microanalyzer (EPMA), and transmission electron microscope (TEM). It has been found that the addition of titanium and niobium to high-strength low-alloyed (HSLA) steel resulted in undesirable large precipitation in the steels, i. e. , precipitation of large precipitates with various morphologies. The composition of the large precipitates has been determined, The effect of cooling rate on (Ti, Nb)(C, N) precipitate formation is investigated. With increasing the cooling rate, titanium-rich (Ti,Nb)(C,N) precipitates are transformed to niobium-rich (Ti,Nb)(C,N) precipitates. The thermal stability of these large precipitates and oxides have been assessed by carrying out various heat treatments such as holding and quenching from temperature at 800 and 1 200℃. It has been found that titanium-rich (Ti,Nb)(C,N) precipitate is stable at about 1 200 ℃ and niobium-rich (Ti,Nb)(C,N) precipitate is stable at about 800 ℃. After reheating at 1 200℃ for 1 h, (Ca,Mn)S and TiN are precipitated from Ca-Al oxide. However, during reheating at 800 ℃ for l h, Ca-Al-Ti oxide in specimens was stable. The thermodynamic calculation of simulating the thermal process is employed. The calculation results are in good agreement with the experimental results. 相似文献
994.
HAN Sung-ho JUNG Gye-dong LEE Sangh-yuk HONG Yeong-pyo LEE Sang-hun 《中南工业大学学报(英文版)》2013,20(9):2407-2413
A new method for automatic salient object segmentation is presented.Salient object segmentation is an important research area in the field of object recognition,image retrieval,image editing,scene reconstruction,and 2D/3D conversion.In this work,salient object segmentation is performed using saliency map and color segmentation.Edge,color and intensity feature are extracted from mean shift segmentation (MSS) image,and saliency map is created using these features.First average saliency per segment image is calculated using the color information from MSS image and generated saliency map.Then,second average saliency per segment image is calculated by applying same procedure for the first image to the thresholding,labeling,and hole-filling applied image.Thresholding,labeling and hole-filling are applied to the mean image of the generated two images to get the final salient object segmentation.The effectiveness of proposed method is proved by showing 80%,89% and 80% of precision,recall and F-measure values from the generated salient object segmentation image and ground truth image. 相似文献
995.
996.
发现服务(Discovery Service, DS)通过提供一种查询服务,为用户提供物品射频识别(Radio Frequency Identification, RFID)标识与供应链中存储该物品信息的多个信息服务器地址之间的映射服务,以帮助用户获取物品在整个供应链中的信息。但是,当前已有的DS设计方案不能满足兼容不同的RFID编码标准、高效的系统性能和强大的抗拒绝服务(Denial of Service, DoS)攻击能力等需求。因此,针对已有DS研究的不足,基于结构化对等(Peer-to-Peer, P2P)网络和PCache主动缓存算法提出一种称为PCacheDS的DS设计方案。仿真实验的结果表明,与已有的DS研究相比,PCacheDS不仅能够兼容不同的RFID编码标准,而且具有更低的平均查询时延、更强的系统处理性能和强大的抗DoS攻击能力,能够更好的满足DS的应用需求。 相似文献
997.
MOK Young Sun JO Jin-Oh LEE Heon-Ju 《等离子体科学和技术》2008,10(1):100-105
The physicochemical processes of dielectric barrier discharge (DBD) such as insitu formation of chemically active species and emission of ultraviolet (UV)/visible light were utilized for the treatment of a simulated wastewater formed with Acid Red 4 as the model organic contaminant. The chemically active species (mostly ozone) produced in the DBD reactor were well distributed in the wastewater using a porous gas diffuser, thereby increasing the gas-liquid contact area. For the purpose of making the best use of the light emission, a titanium oxide-based photocatalyst was incorporated in the wastewater treating system. The experimental parameters chosen were the voltage applied to the DBD reactor, the initial pH of the wastewater, and the concentration of hydrogen peroxide added to the wastewater. The results have clearly shown that the present system capable of degrading organic contaminants in two ways (photocatalysis and ozonation) may be a promising wastewater treatment technology. 相似文献
998.
Linear time-varying systems and bilinear systems are analysed via shifted Chebyshev polynomials of the second kind. Using the operational matrix for integration and the product operational matrix, the dynamical equation of a linear time-varying system (or bilinear system) is reduced to a set of simultaneous linear algebraic equations. The coefficient vectors of shifted Chebyshev polynomials of the second kind can be determined by using the least-squares method. Illustrative examples show that shifted Chebyshev polynomials of the second kind having a finite number of terms are more accurate than either the Legendre or Laguerre methods. 相似文献
999.
S. E. MARSH J. L. WALSH C. T. LEE L. R. BECK C. F. HUTCHINSON 《International journal of remote sensing》2013,34(16):2997-3016
Abstract Multi-resolution and multi-temporal remote sensing data (SPOT-XS and AVHRR) were evaluated for mapping local land cover dynamics in the Sahel of West Africa. The aim of this research was to evaluate the agricultural information that could be derived from both high and low spatial resolution data in areas where there is very often limited ground information. A combination of raster-based image processing and vector-based geographical information system mapping was found to be effective for understanding both spatial and spectral land-cover dynamics. The SPOT data proved useful for mapping local land-cover classes in a dominantly recessive agricultural region. The AVHRR-LAC data could be used to map the dynamics of riparian vegetation, but not the changes associated with recession agriculture. In areas where there was a complex mixture of recession and irrigated agriculture, as well as riparian vegetation, the AVHRR data did not provide an accurate temporal assessment of vegetation dynamics. 相似文献
1000.
An investigation of the ventilated supercavitation for a supercavitating vehicle pitching up and down in the supercavity was carded out in a high-speed water tunnel. The emphasis is laid on the understanding of the interaction of the vehicle aft body with the cavity boundary. The flow characteristics were measured and the stability of supercaviting flow with different pitching frequencies and amplitudes was analyzed. In particular, the objectives of this study are to understand the effect of the impact upon the cavity distortion, and to quantify the impact process by investigating the evolution of the pressure inside the cavity and then the loads on the vehicle during the pitching motion. It is also shown that the evolution of the pressure detected in different,as inside the supercavity, is coherent and uniform during the periods of the pitching motion. This study is of direct relevance to reliable and accurate prediction of hydrodynamic loads associated with the slamming and impact on supercavitating vehicles. 相似文献